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公开(公告)号：DE102004032488A1
公开(公告)日：2005-01-27
申请号：DE102004032488
申请日：2004-07-05
Applicant: KAO CORP TOKIO TOKYO
Inventor： AZUMA KOJI , TSUTSUMI TAKEHIRO , MIZUSHIMA RYUMA , TAKENO HIROTAKA , IWASAKI TOSHIYA
Abstract: The invention provides a process for producing a water dispersion for ink jet recording,which comprises the following steps 1 and 2: (Step 1) a step of obtaining a pigment treated with (a) a water-insoluble vinyl polymer particles by making a pigment and (a) a water-insoluble vinyl polymer particles present in an aqueous solvent and then removing the solvent; and (Step 2) a step of obtaining a water dispersion of a pigment-containing water-insoluble vinyl polymer particles by dispersing a mixture comprising the water-insoluble vinyl polymer particle (a)-treated pigment obtained in step 1, an organic solvent, (b) a water-insoluble vinyl polymer and water and then removing the organic solvent.
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公开(公告)号：DE102004032488B4
公开(公告)日：2013-05-23
申请号：DE102004032488
申请日：2004-07-05
Applicant: KAO CORP
Inventor： AZUMA KOJI , TSUTSUMI TAKEHIRO , MIZUSHIMA RYUMA , TAKENO HIROTAKA , IWASAKI TOSHIYA
Abstract: Verfahren zur Herstellung einer Wasserdispersion zur Tintenstrahlaufzeichnung, umfassend die folgenden Schritte 1 und 2: (Schritt 1) einen Schritt zum Herstellen eines mit wasserunlöslichen Vinylpolymerteilchen (a) behandelten Pigments durch Einbringen eines Pigments und wasserunlöslicher Vinylpolymerteilchen (a) in ein wässriges Lösungsmittel und dann Entfernen des Lösungsmittels; und (Schritt 2) einen Schritt zum Herstellen einer Wasserdispersion von Pigment enthaltenden, wasserunlöslichen Vinylpolymerteilchen durch Dispergieren eines Gemisches, umfassend das mit wasserunlöslichen Vinylpolymerteilchen (a) behandelte Pigment, das im Schritt 1 erhalten wird, ein organisches Lösungsmittel, ein wasserunlösliches Vinylpolymer (b) und Wasser, und dann Entfernen des organischen Lösungsmittels.
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3.发明公开PROCESS FOR PRODUCING AQUEOUS PIGMENT DISPERSION 有权VERFAHREN ZUR HERSTELLUNG EINERWÄSSRIGENPIGMENTDISPERSION
公开(公告)号：EP1935952A4
公开(公告)日：2014-01-22
申请号：EP06783184
申请日：2006-09-05
Applicant: KAO CORP
Inventor： MATSUMOTO TOSHIYUKI , ODA TSUYOSHI , KAMEI KOJI , IWASAKI TOSHIYA
CPC classification number: C09D17/001 , C09D11/322
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公开(公告)号：EP2360215A4
公开(公告)日：2014-01-22
申请号：EP09833480
申请日：2009-12-17
Applicant: KAO CORP
Inventor： YOSHIDA HIROYUKI , ODA TSUYOSHI , SATO TAKAHIRO , SHIMIZU YUSUKE , KAMEI KOJI , IWASAKI TOSHIYA
CPC classification number: C09D11/326 , C09B67/0097
Abstract: The first invention relates to a water-based ink for ink-jet printing which includes colorant-containing polymer particles (A) obtained by dispersing a colorant with a water-soluble polymer (x) and a water-insoluble polymer (y), a water-soluble organic solvent (B) and water, wherein a weight ratio of the water-insoluble polymer (y) to the water-soluble polymer (x) [(y)/(x)] is from 2.0 to 5.0, and a content of the water-soluble organic solvent (B) in the ink is from 10 to 70% by weight. The water-based ink for ink-jet printing according to the first invention is excellent in ejection property and optical density and exhibits a low viscosity. The second invention relates to a process for producing a water dispersion for ink-jet printing, which includes a step (I) of mixing a dispersion of a colorant with an emulsion of a water-insoluble polymer containing an organic solvent; a step (II) of subjecting the resulting mixture to dispersing treatment to obtain a dispersion of the colorant onto which the water-insoluble polymer is deposited; and a step (III) of removing the organic solvent from the resulting dispersion. The water dispersion produced by the process of the second invention is capable of exhibiting a high optical density suitable for high-speed printing.
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公开(公告)号：JP2010017654A
公开(公告)日：2010-01-28
申请号：JP2008180373
申请日：2008-07-10
Inventor： KAMEI KOJI , IWASAKI TOSHIYA , ODA HITOSHI
Abstract: PROBLEM TO BE SOLVED: To provide a method for smoothly starting a continuous bead mill packed with fine beads. SOLUTION: A starting method is disclosed for the continuous bead mill 10 which is provided with a stator 11 having a liquid feed port 13 at the bottom and an agitating rotor 12 provided in the stator 11, and which is packed with fine beads with an average particle size of 0.1 mm or less in 70 vol.% or more in an effective dispersion chamber space in the stator 11. In the starting method, liquid is fed into the stator 11 from the liquid feed port 13 at the bottom of the stator 11 to float the fine beads so that a stator cross area-based liquid average empty tower velocity expressed by expression (1) is 0.4×10 -3 m/s or more and a liquid pressing ratio expressed by expression (2) is 0.1 or more, and the agitating rotor 12 is rotationally driven while the fine beads are floated. COPYRIGHT: (C)2010,JPO&INPIT
Abstract translation: 要解决的问题：提供一种平滑起动填充有细小珠粒的连续珠磨机的方法。 解决方案：公开了一种连续珠磨机10的启动方法，该连续珠磨机设置有在底部具有液体供给口13的定子11和设置在定子11中的搅拌转子12，并且填充有细小珠 在定子11的有效分散室空间中的平均粒径为0.1mm以下，70体积％以上。在起动方法中，液体从液体供给口13的底部进入定子11 定子11使微细珠漂浮，使得由式（1）表示的定子横截面积的液体平均空塔速度为0.4×10 -3秒/秒以上，液压比 由表达式（2）表示为0.1以上，并且在细珠浮起的同时旋转驱动搅拌转子12。 版权所有（C）2010，JPO＆INPIT
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Patent Agency Ranking
公开(公告)号：JP2009062419A
公开(公告)日：2009-03-26
申请号：JP2007229328
申请日：2007-09-04
Inventor： IWASAKI TOSHIYA
IPC: C09D17/00 , B41J2/01 , B41M5/00 , C09D11/00 , C09D11/322 , C09D11/328
Abstract: PROBLEM TO BE SOLVED: To provide a method for producing an aqueous pigment dispersion excellent in dispersibility and dispersion stability, an aqueous pigment dispersion and inkjet recording aqueous ink reducing contamination by foreign matter even when hydrophobic silica is mixed.
SOLUTION: The method for producing the aqueous pigment dispersion comprises a process 1 for obtaining the dispersion A by dispersing a mixture containing a pigment, a water-insoluble polymer, a hydrophobic organic solvent and water, a process 2 for obtaining a dispersion B by mixing hydrophobic silica, a hydrophobic organic solvent, and a hydrophilic organic solvent in amount of 0.5-10 weight times of the hydrophobic silica, and a process 3 for obtaining a dispersion C by mixing the dispersion A and the dispersion B together.
COPYRIGHT: (C)2009,JPO&INPITAbstract translation: 要解决的问题：提供一种分散性和分散稳定性优异的水性颜料分散体的制造方法，水性颜料分散体和喷墨记录水性油墨，即使在疏水性二氧化硅混合的情况下还能减少异物污染。 解决方案：水性颜料分散体的制备方法包括通过分散含有颜料，水不溶性聚合物，疏水性有机溶剂和水的混合物获得分散体A的方法1，获得分散体的方法2 通过将疏水性二氧化硅，疏水性有机溶剂和亲水性有机溶剂以疏水性二氧化硅的0.5-10重量倍的量混合来制备B，以及通过将分散体A和分散体B混合在一起而获得分散体C的方法3。 版权所有（C）2009，JPO＆INPIT
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公开(公告)号：JP2007092059A
公开(公告)日：2007-04-12
申请号：JP2006239814
申请日：2006-09-05
Inventor： KAMEI KOJI , MATSUMOTO TOSHIYUKI , IWASAKI TOSHIYA , ODA HITOSHI
IPC: C09D17/00 , C09B67/40 , C09B67/46 , C09D11/00 , C09D11/322 , C09D11/324 , C09D11/326 , C09D11/328 , C09D11/38
Abstract: PROBLEM TO BE SOLVED: To provide a process for producing an aqueous pigment dispersion having a high color density, and is excellent in gloss and marring resistance when printed on specialized paper; and to provide an aqueous ink for inkjet recording. SOLUTION: The process for producing an aqueous pigment dispersion comprises: (1) a first step in which an emulsion composition (A) comprising a water-insoluble polymer having a specific weight-average molecular weight and a salt-forming group, an organic solvent having a specific water solubility, a neutralizing agent, and water is mixed with a pigment (B) to obtain a mixture as a predispersion having a nonvolatile content of 5-50% by weight and an organic solvent/water ratio of 0.1-0.9 by weight; (2) a second step in which the predispersion is continuously dispersed with a dispersing-medium type disperser and the resultant dispersion treated product is continuously separated from the medium particles; and (3) a third step in which the dispersion is treated with a homogenizer for further dispersing the pigment. Also provided is a water-based ink for inkjet recording containing the aqueous pigment dispersion obtained by the process. COPYRIGHT: (C)2007,JPO&INPIT
Abstract translation: 要解决的问题：提供一种具有高色密度的水性颜料分散体的制造方法，并且在印刷在专用纸上时的光泽和耐光泽性优异; 并提供用于喷墨记录的水性油墨。 水溶性颜料分散体的制备方法包括：（1）第一步，其中包含具有特定重均分子量的水不溶性聚合物和成盐基团的乳液组合物（A） 将具有特定水溶性的有机溶剂，中和剂和水与颜料（B）混合，得到作为不挥发成分为5-50重量％，有机溶剂/水比为0.1的预分散体的混合物 -0.9重量％ （2）第二步，其中预分散体用分散介质型分散机连续分散，得到的分散处理产物与介质颗粒连续分离; 和（3）第三步，其中分散体用均化器处理以进一步分散颜料。 还提供了一种用于喷墨记录的水性油墨，其包含通过该方法获得的水性颜料分散体。 版权所有（C）2007，JPO＆INPIT
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公开(公告)号：JP2002338563A
公开(公告)日：2002-11-27
申请号：JP2001148101
申请日：2001-05-17
Applicant: KAO CORP
Inventor： IWASAKI TOSHIYA , KIDA KIYOBUMI
IPC: C07D307/33
Abstract: PROBLEM TO BE SOLVED: To provide a method for producing the objective radical addition reaction product in high yield by simple operation. SOLUTION: This method for producing a radical addition reaction product from a polymerizable monomer and an organic compound A capable of making a radical addition reaction with the polymerizable monomer, comprises the steps of (A) extracting part of an organic compound A-containing liquid put into a reaction vessel and adjusting the temperature of the thus extracted liquid to a specified value and (B) mixing the extracted liquid and the polymerizable monomer together and putting the resultant mixture into the reaction vessel.
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公开(公告)号：JPH09249637A
公开(公告)日：1997-09-22
申请号：JP6226396
申请日：1996-03-19
Applicant: KAO CORP
Inventor： TSUYUTANI SHINJI , AIMONO KIYOSHI , IWASAKI TOSHIYA
IPC: C11D1/29 , C07C303/24 , C07C305/10
Abstract: PROBLEM TO BE SOLVED: To obtain the subject compound having excellent hue, etc., in high conversion and productivity with simple operability and easy removal of by- produced hydrochloric acid by sulfating an N-alkylamidoalkanol in the presence of a solvent at a low temperature and raising the temperature of the reaction system. SOLUTION: The objective N-alkylamidoalkanol sulfuric acid ester (salt) of formula II (M is H or a cation) is produced by sulfating an N- alkylamidoalkanol of formula I (R is a 6-22C straight or branched-chain alkyl, alkenyl, etc.; R is H or a 1-22C straight or branched-chain alkyl, etc.; R is a 1-5C straight or branched-chain alkylene; R is a 2-3C straight or branched- chain alkylene; (n) is an average addition molar number of alkylene oxide and is 0-50) with chlorosulfonic acid as a sulfating agent in the presence of a solvent at
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10.发明专利
公开(公告)号：JP2013124356A
公开(公告)日：2013-06-24
申请号：JP2011275594
申请日：2011-12-16
Inventor： WADA KOSUKE , IWASAKI TOSHIYA
Abstract: PROBLEM TO BE SOLVED: To provide a process for efficiently producing a dispersion for inkjet recording, wherein finely grained pigment is stably dispersed.SOLUTION: [1] The process includes: a step (A) for producing an aqueous pigment dispersion containing a treated pigment by the reaction of the pigment with a treating agent that can introduce a hydrophilic group into the pigment, while a mixture that contains the pigment and an aqueous medium is ground by means of a media mill, and a step (B) for adding a polymer having an acid value of 150 to 250 mg-KOH/g to an aqueous pigment dispersion that contains the treated pigment and dispersing the resulting material by using a high pressure homogenizer. [2] An aqueous ink for inkjet recording contains the aqueous pigment dispersion produced by the process described in [1].
Abstract translation: 要解决的问题：提供一种有效地生产用于喷墨记录的分散体的方法，其中细颗粒颜料稳定地分散。 [1]方法：[1]该方法包括：步骤（A），用于通过颜料与可以将亲水基团引入颜料的处理剂的反应来制备含有处理颜料的水性颜料分散体，同时混合 其含有颜料，水介质用介质研磨机研磨;和步骤（B），用于将含有150-250mg-KOH / g酸值的聚合物加入到含有处理颜料的水性颜料分散体中 并通过使用高压均化器分散所得材料。 [2]喷墨记录用水性油墨含有通过[1]所述的方法制造的水性颜料分散体。 版权所有（C）2013，JPO＆INPIT
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