Abstract:
A read head with reduced height sensitivity for use in a reflectance photometer that measures reflectance of diffuse light from a sample disposed outside the readhead includes a housing with an upper spherical portion and a lower conical portion. The inner peripheral surface of the upper portion is hemispherically configured and the inner peripheral surface of the lower portion is conically configured to permit illumination of a sample disposed outside the readhead. The angle of the cone defined in the conical portion of the housing is in the range of 45°-60°. The inner peripheral surfaces of the upper and lower portions are coated with a highly reflective material, such as barium sulfate. The apex of the conically configured housing portion is truncated to provide a light transmitting aperture for sample illumination. A sample is positioned adjacent the light-transmitting aperture below and outside the conically shaped readhead housing portion. The housing includes a second aperture for receiving a high intensity light from a flash lamp or incandescent light to illuminate the interior of the housing and diffusely illuminate the sample. A baffle is located adjacent the second aperture to avoid direct illumination of the sample. Fiberoptic bundles and photodetectors as well as lenses and reflecting surfaces are provided to detect the amount of diffuse light reflected from the sample.
Abstract:
Reflectance apparatus is disclosed for obtaining measurement of nonspecular reflected light in which one or more light sources and one or more detectors are mounted together on the same plane surface in close proximity to each other at an angle (φ) from the normal to the surface of the specimen holder. Angle (φ) is selected such that the specular reflection at the surface of the specimen is insignificant compared to the minimum diffused reflection expected from the specimen.
Abstract:
A method of calibrating reflectance measuring devices, such as spectrophotometers, that incorporate automatic gain or sensitivity setting capability. According to the method, offset reflectance and reflectance of a secondary reflectance standard for several wavelengths are calculated and stored in a memory of a reflectance measuring device. A secondary standard is mounted in the reflectance measuring device and reflectances at a selected wavelengths from the secondary standard are read prior to measurement of the reflectance of the test sample. The stored offset reflectance and secondary reflectance for the operational wavelength are used to calculate true reflectance of the test sample.
Abstract:
A method of calibrating reflectance measuring devices, such as spectrophotometers, that incorporate automatic gain or sensitivity setting capability. According to the method, offset reflectance and reflectance of a secondary reflectance standard for several wavelengths are calculated and stored in a memory of a reflectance measuring device. A secondary standard is mounted in the reflectance measuring device and reflectances at a selected wavelengths from the secondary standard are read prior to measurement of the reflectance of the test sample. The stored offset reflectance and secondary reflectance for the operational wavelength are used to calculate true reflectance of the test sample.