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    NEW QUINONE COMPOUND
    1.
    发明专利
    NEW QUINONE COMPOUND 失效

    公开(公告)号：JPH06312951A

    公开(公告)日：1994-11-08

    申请号：JP10332093

    申请日：1993-04-28

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： FUJITA TERUNORI ,  NITAHARA MASATOSHI ,  KAWAI KOJI ,  KISO YOSHIHISA

    IPC: C07C46/00 ,  C07C50/32 ,  C07C69/017 ,  C07C69/16 ,  C07C69/28 ,  C07C69/614 ,  C07C69/773 ,  C07C69/96 ,  C07C271/44 ,  C07C271/58 ,  C07C309/65 ,  C07C309/66 ,  C07C309/73 ,  C07F7/18 ,  G03G5/06

    Abstract: PURPOSE:To provide a new quinone compound stable against heat, not having sublimating property and an irritating smell, and useful as a functional chemical. CONSTITUTION:A quinone compound of formula I [A, B are hydrocarbon group, R -CO, R -O-CO, R R N-CO, R -SO2, R R R Si (R to R are H, hydrocarbon group). The compound of formula I is produced by thermally dimerizing 1,2- naphthoquinone into dinaphthyldiquinhydrone in the presence of an acid, and subsequently reacting the produced compound with a reagent containing a suitable nucleating agent such as a compound of formula II [X is C, SO; Y is hydrocarbon group, OR, NRR (R is hydrocarbon group)] (e.g. tosyl chloride), a compound of formula III (e.g. acetic anhydride), a compound of formula IV (e.g. diphenyl carbonate), etc. The compound of formula I is useful as a color- developing agent, an intermediate for dyestuffs, pigments, medicines, agricultural chemicals, rubber chemicals, etc., an oxidizing agent, etc.

    COLOR FORMING RECORDING MATERIAL
    2.
    发明专利
    COLOR FORMING RECORDING MATERIAL 失效

    公开(公告)号：JPH06179287A

    公开(公告)日：1994-06-28

    申请号：JP33274992

    申请日：1992-12-14

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： NITAHARA MASATOSHI ,  FUJITA TERUNORI ,  KAWAI KOJI ,  KISO YOSHIHISA

    IPC: B41M5/132 ,  B41M5/155 ,  B41M5/26 ,  B41M5/30 ,  B41M5/323 ,  B41M5/333

    Abstract: PURPOSE:To provide a color forming recording material having high absorption within the range from a visible region to a near infrared region and having a high light resistance by providing a recording layer containing a azo compd. represented by a specific general formula and an acidic substance on a support. CONSTITUTION:A predetermined amt. of an azo compd. represented by formula I (wherein X is H, an amino group, an alkyl group or an acyl group, Y is H, halogen, an alkyl group or an aryl group, m is a natural number of 4 or less and A and B are H, an alkyl group or an aralkyl group) and a predetermined amt. of an acidic substance are mixed. The obtained mixture is compounded with an aqueous soln. of a binder such as polyvinyl alcohol and ground to prepare a coating soln. This coating soln. is applied to a support such as fine paper and dried to form a recording layer, thus obtaining a color forming recording material. As a concrete example of the azo compd., there is 4-aminoazobenzene or 4-(N-methylamino)azobenzene and, as examples of the acidic substance, there are phenol, naphthol, acid clay, kaolin and the like.

    PRODUCTION OF P-PHENYLENEDIAMINE DERIVATIVE
    3.
    发明专利
    PRODUCTION OF P-PHENYLENEDIAMINE DERIVATIVE 失效

    公开(公告)号：JPH0625112A

    公开(公告)日：1994-02-01

    申请号：JP25806991

    申请日：1991-10-04

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： NITAHARA MASATOSHI ,  FUJITA TERUNORI ,  KAWAI KOJI ,  KISHIKAWA KEIKI ,  MIKI HISAYA

    IPC: C07C209/60 ,  C07C211/54 ,  C07C213/02 ,  C07C217/92 ,  C07C309/73 ,  C07C311/21

    Abstract: PURPOSE:To obtain a p-phenylenediamine at one stage in high yield by reacting a phenylenediamine derivative with a 4-hydroxydiphenylamine derivative in the presence of specific titanium compound or a zirconium compound. CONSTITUTION:A compound of formula I (X to X are H, alkyl, acyl or arylsulfonyl; X is alkyl, alkoxy, halogen, dialkylamino, acylamine, etc.; 1 is 0-4)(e.g. p-phenylenediamine) is reacted with a compound of formula II (X is H or alkyl); X and X are alkyl, alkoxy, halogen, dialkylamino, etc.; (m) is 0-4; (n) is 0-5)(e.g. 4-hydroxydiphenylamine) in the presence of an alkoxy, aryloxy or halogen-containing titanium compound or zirconium compound (e.g. tetraisopropoxytitanium) to give a pphenylenediamine derivative of formula III [e.g. N-(4-aminophenyl)-N'-phenyl-p-phenylenediamine].

    COLOR FORMING RECORDING MATERIAL
    4.
    发明专利
    COLOR FORMING RECORDING MATERIAL 失效

    公开(公告)号：JPH04320882A

    公开(公告)日：1992-11-11

    申请号：JP11667991

    申请日：1991-04-22

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： KISHIKAWA KEIKI ,  KAWAI KOJI ,  KAWAMURA MASATO ,  NITAHARA MASATOSHI ,  MIKI HISAYA

    IPC: B41M5/323 ,  B41M5/26 ,  B41M5/30

    Abstract: PURPOSE:To provide a color forming recording material imparting a developed color of practically sufficient intensity immediately after color forming operation and having absorption in a long wavelength region from a visible light region to a near infrared region. CONSTITUTION:A color forming recording material contains an acyldiamine derivative (a) represented by general formula (I) A-NR -B-NR -CO-X (wherein A is an aryl group, B is an arylene group, X is an alkyl group, an aryl group or an aralkyl group and R and R are respectively independently hydrogen, a lower alkyl group, an aryl group or an aralkyl group), an oxidizing agent (b) and an acidic substance (c).

    RECORDING MATERIAL CAPABLE OF DEVELOPING COLOR
    5.
    发明专利
    RECORDING MATERIAL CAPABLE OF DEVELOPING COLOR 失效

    公开(公告)号：JPH0561149A

    公开(公告)日：1993-03-12

    申请号：JP25656991

    申请日：1991-10-03

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： KAWAI KOJI ,  TANAKA MICHIO ,  FUJITA TERUNORI ,  KISHIKAWA YOSHIKI ,  NITAHARA MASATOSHI ,  TARUMOTO HIROMASA ,  KAWAMURA MASATO ,  MIKI HISAYA

    IPC: B41M5/323 ,  B41M5/30 ,  G03C1/675

    Abstract: PURPOSE:To obtain the color developing recording material capable of developing practicable sufficiently intense color immediately after making color developing operation and enabling readout of information through instruments using lights of all the wavelengths by incorporating a specified diamine derivative and an oxidant, and an organic acid material solid at normal temperature. CONSTITUTION:The recording material contains the oxidant, the organic acidic material solid at normal temperature, and the diamine derivative represented by formula I in which each of A and B is, independently, aryl; X is arylene, and each of R and R is, independently, H, lower alkyl, aryl, or aralkyl. It is preferred that the oxidant is a quinoid type electron receptor, thus permitting practicable sufficiently intense color to be developed and the color developing part to have strong absorption in the wide region from visible to near infra wavelengths, and therefore, readout of information to be made by instruments using all the wavelengths.

    PRODUCTION OF HYDROXY AROMATIC HYDROCARBON
    6.
    发明专利
    PRODUCTION OF HYDROXY AROMATIC HYDROCARBON 失效

    公开(公告)号：JPS63258826A

    公开(公告)日：1988-10-26

    申请号：JP9299087

    申请日：1987-04-17

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： MIKI HISAYA ,  ARAKI SHINTARO ,  YASUDA MASAAKI ,  NITAHARA MASATOSHI

    IPC: C07C37/08 ,  B01J27/02 ,  C07B61/00 ,  C07C27/00 ,  C07C29/132 ,  C07C39/08 ,  C07C39/10 ,  C07C39/14 ,  C07C67/00

    Abstract: PURPOSE:To obtain the titled compound by one-stage reaction advantageously, by reacting carbinol and/or carbinol hydroperoxide in a nitro compound, a phenol and/or a halogenated hydrocarbon in the presence of an acid and hydrogen peroxide. CONSTITUTION:A compound shown by the formula (Ar is aryl; R and R are H or hydrocarbon group; m is 0, 1 or 2; n is 1, 2 or 3) in one or more solvents selected from a nitro compound, a phenol and a halogenated hydrocarbon) in the presence of an acid and hydrogen peroxide preferably at 20-80 deg.C to give the titled compound such as resorcin or 2,6-dihydroxynaphthalene from the raw material by one stage reaction selectively and in high yield. A reaction mixture obtained by oxidizing an alkyl aromatic hydrocarbon such as diisopropylbenzene or 2,6-diisopropylnaphthalene with molecular oxygen may be also used as the raw material.

    CATALYST FOR POLYMERIZING OLEFIN AND POLYMERIZATION OF OLEFIN
    7.
    发明专利
    CATALYST FOR POLYMERIZING OLEFIN AND POLYMERIZATION OF OLEFIN 失效

    公开(公告)号：JPH1087716A

    公开(公告)日：1998-04-07

    申请号：JP25035396

    申请日：1996-09-20

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： FUKUOKA ONORI ,  KAWAI KOJI ,  NITAHARA MASATOSHI

    IPC: C08F4/642 ,  C08F4/645 ,  C08F4/6592 ,  C08F10/00

    Abstract: PROBLEM TO BE SOLVED: To obtain a catalyst, comprising a specific transition metallic compound and a specified compound, having excellent polymerizing activities agent an olefin and capable of providing a polyolefin having a high molecular weight. SOLUTION: This catalyst for polymerizing an olefin comprises (A) a transition metallic compound represented by the formula [M is a group IV to VI transition metallic atom of the periodic table; R and R are each a 1-4C alkyl; R and R are each a C1-16 aryl; R is H or a C4 alkyl; X and X are each H, a halogen a C1-20 (halogenated)hydrocarbon, etc.; Y is a C1-20 bivalent (halogenated)hydrocarbon, a bivalent silicon-containing group, a bivalent germanium-containing group, etc.] [e.g. dimethylsilanediyl(2-ethyl-4-(9-phenanthryl) indenyl) (2-methyl-4-(9-phenanthryl)z indenyl)zirconium dichloride], (B) an organoaluminum compound and/or (C) a compound reactive with the component A and capable of forming ion pairs.

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