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公开(公告)号：WO2004087631A3
公开(公告)日：2004-12-02
申请号：PCT/IL2004000203
申请日：2004-03-03
Applicant: STALEY MFG CO A E , BANIEL AVRAHAM , VITNER ASHER , GONEN DAVID , HEIDEL DAVID
Inventor： BANIEL AVRAHAM , VITNER ASHER , GONEN DAVID , HEIDEL DAVID
IPC: C07C51/43 , C07C51/48 , C07C59/265
CPC classification number: C07C51/43 , C07C51/48 , C07C59/265
Abstract: The invention provides a process for the recovery of citric acid from an aqueous solution feed stream originating in fermentation of carbohydrates and utilizing an amine solvent extraction step for separation of impurities comprising: subjecting said aqueous solution feed stream A to a treatment for partial recovery of citric acid, wherein said treatment is other than amine solvent extraction, to form a first portion of purified citric acid B and a secondary feed stream F; subjecting at least a portion G of said secondary feed stream F to a treatment consisting of amine solvent extraction to form a second portion of purified citric acid solution and to reject substantial of impurities initially present in said portion of said secondary feed stream; subjecting said second portion of purified citric acid solution to crystallization; and recycling mother liquor from said crystallization.
Abstract translation: 本发明提供从源自碳水化合物发酵的水溶液进料流中回收柠檬酸的方法，并利用胺溶剂提取步骤分离杂质，所述方法包括：使所述水溶液进料流A经受部分回收柠檬酸 酸，其中所述处理不是胺溶剂萃取，以形成纯化柠檬酸B的第一部分和第二进料流F; 使至少部分G的所述二级原料流F经受由胺溶剂萃取组成的处理以形成第二部分纯化的柠檬酸溶液并且除去最初存在于所述二级原料流的所述部分中的大量杂质; 使所述第二部分纯化的柠檬酸溶液结晶; 并从所述结晶回收母液。
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公开(公告)号：WO2004101437A2
公开(公告)日：2004-11-25
申请号：PCT/US2004013905
申请日：2004-05-06
Applicant: STALEY MFG CO A E
Inventor： BANIEL AVRAHAM M , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
CPC classification number: C07C29/86 , B01D11/0446 , B01D11/0488 , B01D11/0492 , C02F1/26 , C07C31/205
Abstract: Disclosed herein are processes for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The weight ratio in the first phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant. The first phase can be removed from the separated second phase in order to recover the 1,3-propanediol.
Abstract translation: 本文公开了从含水原料流中回收1,3-丙二醇的方法。 本发明涉及将包含水，1,3-丙二醇和至少一种污染物的含水进料流与至少一种溶剂萃取剂接触以形成混合物。 将混合物分离成第一相和第二相。 第二相包含来自含水进料流的大部分水。 第一阶段包括溶剂萃取剂和存在于含水进料流中的至少一些1,3-丙二醇。 在水性进料流与溶剂接触之前，1,3-丙二醇与任何一种污染物的第一相中的重量比大于1,3-丙二醇与含水进料流中相同污染物的重量比 萃取剂。 为了回收1,3-丙二醇，可以将第一相从分离的第二相中除去。
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公开(公告)号：EP1620362A4
公开(公告)日：2007-12-19
申请号：EP04751324
申请日：2004-05-06
Applicant: STALEY MFG CO A E
Inventor： BANIEL AVRAHAM M , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
IPC: B01D11/00 , B01D11/04 , C02F1/00 , C02F1/26 , C02F1/44 , C07C29/86 , C07C31/18 , C12P7/04 , C12P7/14
CPC classification number: C07C29/86 , B01D11/0446 , B01D11/0488 , B01D11/0492 , C02F1/26 , C07C31/205
Abstract: Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.
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公开(公告)号：AU2004238804A1
公开(公告)日：2004-11-25
申请号：AU2004238804
申请日：2004-05-06
Applicant: STALEY MFG CO A E
Inventor： BAIADA ANTHONY , BANIEL AVRAHAM M , JANSEN ROBERT P , VITNER ASHER
Abstract: Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.
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公开(公告)号：NO20055383D0
公开(公告)日：2005-11-14
申请号：NO20055383
申请日：2005-11-14
Applicant: STALEY MFG CO A E
Inventor： BANIEL AVRAHAM , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
Abstract: Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.
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Patent Agency Ranking
公开(公告)号：ES2408344T3
公开(公告)日：2013-06-20
申请号：ES04751324
申请日：2004-05-06
Applicant: STALEY MFG CO A E , TATE & LYLE INGREDIENTS
Inventor： BANIEL AVRAHAM , JANSEN ROBERT , VITNER ASHER , BAIADA ANTHONY
IPC: B01D11/00 , B01D11/04 , C02F1/00 , C02F1/26 , C02F1/44 , C07C29/86 , C07C31/18 , C12P7/04 , C12P7/14
Abstract: Un procedimiento para recuperar 1,3-propanodiol de un caldo de fermentación que comprende 1,3-propanodiol, que comprende las etapas de: poner en contacto un caldo de fermentación que contiene agua, 1,3-propanodiol y al menos un contaminante escogido entre glicerol, glucosa y butanotriol, con al menos un disolvente de extracción escogido entre alcanoles, cetonas, ésteres, ácidos, éteres o aceites vegetales, para formar una primera mezcla y separar la primera mezcla en una primera fase y una segunda fase, donde la primera fase comprende la mayor parte del disolvente de extracción y al menos parte del 1,3-propanodiol que estaba presente en el caldo de fermentación y la relación de pesos de 1,3-propanodiol a al menos uno de los compuestos glicerol, glucosa o butanotriol en la primera fase es mayor que la relación de pesos de 1,3-propanodiol al mismo contaminante en el caldo de fermentación antes de que el caldo de fermentación se haya puesto en contacto con el disolvente de extracción y en el que la segunda fase comprende la mayor parte del agua y al menos alguno de los contaminantes de la corriente de alimentación acuosa; recuperar 1,3-propanodiol eliminando la primera fase de la segunda fase, poner en contacto la primera fase eliminada con una primera cantidad de disolución acuosa para formar una segunda mezcla y separar la segunda mezcla en una tercera fase y una cuarta fase, donde la tercera fase comprende la mayor parte del disolvente de extracción de la primera fase y donde la cuarta fase comprende 1,3-propanodiol y la mayor parte de la primera cantidad de disolución acuosa y la relación de peso en la cuarta fase de 1,3-propanodiol a cualquier contaminante presente es mayor que la relación en peso de 1,3-propanodiol al mismo contaminante en el caldo de fermentación antes de que el caldo de fermentación se haya puesto en contacto con el disolvente de extracción
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公开(公告)号：BRPI0409540A
公开(公告)日：2006-04-18
申请号：BRPI0409540
申请日：2004-03-03
Applicant: STALEY MFG CO A E
Inventor： BANIEL AVRAHAM , VITNER ASHER , GONEN DAVID , HEIDEL DAVID
Abstract: The invention provides a process for the recovery of citric acid from an aqueous solution feed stream originating in fermentation of carbohydrates and utilizing an amine solvent extraction step for separation of impurities comprising: subjecting said aqueous solution feed stream A to a treatment for partial recovery of citric acid, wherein said treatment is other than amine solvent extraction, to form a first portion of purified citric acid B and a secondary feed stream F; subjecting at least a portion G of said secondary feed stream F to a treatment consisting of amine solvent extraction to form a second portion of purified citric acid solution and to reject substantial of impurities initially present in said portion of said secondary feed stream; subjecting said second portion of purified citric acid solution to crystallization; and recycling mother liquor from said crystallization.
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公开(公告)号：IL119986A
公开(公告)日：2000-10-31
申请号：IL11998697
申请日：1997-01-09
Applicant: AMYLUM NV , STALEY MFG CO A E
Inventor： EYAL AHARON M , VITNER ASHER , CAMI PIERRE , JANSEN ROBERT , JARRY BRUNO , LECOMTE D , SCOTT JEAN , CHATTAWAY THOMAS , LANCKER F VAN
IPC: C07C227/42 , C07C229/24 , C08G69/10 , C08G73/10 , C12P7/46 , C12P13/20 , C07C227/00
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公开(公告)号：CA2524452C
公开(公告)日：2012-02-07
申请号：CA2524452
申请日：2004-05-06
Applicant: STALEY MFG CO A E
Inventor： BANIEL AVRAHAM M , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
IPC: B01D11/00 , B01D11/04 , C02F1/00 , C02F1/26 , C02F1/44 , C07C29/86 , C07C31/18 , C12P7/04 , C12P7/14
Abstract: Disclosed herein are processes for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The weight ratio in the first phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant. The first phase can be removed from the separated second phase in order to recover the 1,3-propanediol.
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公开(公告)号：CA2524452A1
公开(公告)日：2004-11-25
申请号：CA2524452
申请日：2004-05-06
Applicant: STALEY MFG CO A E
Inventor： JANSEN ROBERT P , BAIADA ANTHONY , VITNER ASHER , BANIEL AVRAHAM M
IPC: B01D11/00 , B01D11/04 , C02F1/00 , C02F1/26 , C02F1/44 , C07C29/86 , C07C31/18 , C12P7/04 , C12P7/14
Abstract: Disclosed herein are processes for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous fe ed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprise s solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The weight ratio in the first phase of 1,3- propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant. The fir st phase can be removed from the separated second phase in order to recover the 1,3-propanediol.
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