PROCESS FOR PRODUCING 1, 3-PROPANEDIOL
    1.
    发明申请
    PROCESS FOR PRODUCING 1, 3-PROPANEDIOL 审中-公开
    生产1,3-丙二醇的方法

    公开(公告)号:WO2004101437A2

    公开(公告)日:2004-11-25

    申请号:PCT/US2004013905

    申请日:2004-05-06

    Abstract: Disclosed herein are processes for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The weight ratio in the first phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant. The first phase can be removed from the separated second phase in order to recover the 1,3-propanediol.

    Abstract translation: 本文公开了从含水原料流中回收1,3-丙二醇的方法。 本发明涉及将包含水,1,3-丙二醇和至少一种污染物的含水进料流与至少一种溶剂萃取剂接触以形成混合物。 将混合物分离成第一相和第二相。 第二相包含来自含水进料流的大部分水。 第一阶段包括溶剂萃取剂和存在于含水进料流中的至少一些1,3-丙二醇。 在水性进料流与溶剂接触之前,1,3-丙二醇与任何一种污染物的第一相中的重量比大于1,3-丙二醇与含水进料流中相同污染物的重量比 萃取剂。 为了回收1,3-丙二醇,可以将第一相从分离的第二相中除去。

    PROCESS FOR PRODUCING 1, 3-PROPANEDIOL
    2.
    发明公开
    PROCESS FOR PRODUCING 1, 3-PROPANEDIOL 有权
    用于生产1,3-丙二醇

    公开(公告)号:EP1620362A4

    公开(公告)日:2007-12-19

    申请号:EP04751324

    申请日:2004-05-06

    Abstract: Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.

    PROCESS FOR PURIYING AN ORGANIC ACID
    3.
    发明公开
    PROCESS FOR PURIYING AN ORGANIC ACID 审中-公开
    法提纯有机酸

    公开(公告)号:EP1470099A4

    公开(公告)日:2006-04-12

    申请号:EP02797276

    申请日:2002-12-11

    CPC classification number: C07C51/48 C07C59/08

    Abstract: A process is disclosed for purifying an aqueous feed stream (10) comtaining a product organic acid and a strong contaminant such as another organic acid. The molar concentration of the organic acid in the feed stream (10) is at least 20 times greater than that of the contaminant. The feed stream (10) is contacted with an immiscible basic extractant (18) that has a greater affinity for the contaminant and which complexes with the contaminant and some of the organic acid. The complexed extractant is separated from the aqueous stream (10), so as to produce a first effluent stream (20) comprising product organic acid. The complexed extractant is contacted with a displacing acid, for which the extractant has a greater affinity than contaminant or extractant. As a result, a second effluent stream (28) comprising organic acid and a third effluent stream (30) are produced.

    Process for producing 1,3-propanediol

    公开(公告)号:ZA200509090B

    公开(公告)日:2007-03-28

    申请号:ZA200509090

    申请日:2005-11-10

    Abstract: Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.

    Process for producing 1, 3-propanediol

    公开(公告)号:AU2004238804A1

    公开(公告)日:2004-11-25

    申请号:AU2004238804

    申请日:2004-05-06

    Abstract: Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.

    PROCESS FOR PURIFYING AN ORGANIC ACID

    公开(公告)号:CA2470978A1

    公开(公告)日:2003-07-24

    申请号:CA2470978

    申请日:2002-12-11

    Abstract: A process is disclosed for purifying an aqueous feed stream (10) comtaining a product organic acid and a strong contaminant such as another organic acid. The molar concentration of the organic acid in the feed stream (10) is at least 20 times greater than that of the contaminant. The feed stream (10) is contacted with an immiscible basic extractant (18) that has a greater affini ty for the contaminant and which complexes with the contaminant and some of the organic acid. The complexed extractant is separated from the aqueous stream (10), so as to produce a first effluent stream (20) comprising product organ ic acid. The complexed extractant is contacted with a displacing acid, for whic h the extractant has a greater affinity than contaminant or extractant. As a result, a second effluent stream (28) comprising organic acid and a third effluent stream (30) are produced.

    PROCESS FOR PRODUCING 1, 3-PROPANEDIOL

    公开(公告)号:CA2524452C

    公开(公告)日:2012-02-07

    申请号:CA2524452

    申请日:2004-05-06

    Abstract: Disclosed herein are processes for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The weight ratio in the first phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant. The first phase can be removed from the separated second phase in order to recover the 1,3-propanediol.

    PROCESS FOR PRODUCING 1, 3-PROPANEDIOL

    公开(公告)号:CA2524452A1

    公开(公告)日:2004-11-25

    申请号:CA2524452

    申请日:2004-05-06

    Abstract: Disclosed herein are processes for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous fe ed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprise s solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The weight ratio in the first phase of 1,3- propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant. The fir st phase can be removed from the separated second phase in order to recover the 1,3-propanediol.

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