Abstract:
Compounds, synthesis of, and methods for synthesizing metal alkoxide derivatives; and metal alkoxide derivatives for use as flame retardants are described. Group 13 metal alkoxides having flame retardant properties may be prepared by reacting the group 13 metal trihydroxide with an alcohol.
Abstract:
A reaction system and method for preparing compounds or intermediates from solid reactant materials is provided. In a specific aspect, a reaction system and methods are provided for preparation of boron-containing precursor compounds useful as precursors for ion implantation of boron in substrates. In another specific aspect, a reactor system and methods are provided for manufacture of boron precursors such as B2F4.
Abstract:
The present invention relates to a thermowell blocking apparatus for a high-pressure reactor used in a desulfurization process, which can rapidly prevent noxious high-temperature and high-pressure gases from leaking out of a high-pressure reactor when the noxious high-temperature and high-pressure gases leak from the high-pressure reactor due to unexpected damage occurring to a thermowell used for measuring a reaction temperature of a catalyst. The thermowell blocking apparatus can prevent the economic losses caused by the stoppage of the desulfurization process, and can reduce consequential damages to human life, the environment, and the like.
Abstract:
The invention relates to a process and apparatus for preparing an ethylene polymer by free radical polymerization under ultra-high pressure. The polymerization is carried out in an autoclave reactor in the presence of a free radical initiator. The autoclave reactor is characterized by having one or more elongated baffles affixed to the interior reactor wall.
Abstract:
An adapter for releasably securing a probe to a reaction vessel. Embodiments of the adapter include a cover plate for mating with a reaction vessel, a body portion extending from the cover plate, and a probe gripping portion secured to the body portion. A collet and at least one anvil resides within the body portion/probe gripping portion assembly. The collet has at least one split conical end that may be divided into a plurality of flexible gripping fingers, the conical end of the collet adapted to mate with the at least one anvil. An o-ring is preferably located in the body portion and surrounds a probe when the probe is passed through the adapter. Pressure from the reaction vessel exerts an axial force on the o-ring which, in turn, exerts a like force on the anvil, thereby causing the gripping fingers of the collet to exert a gripping force on the probe.
Abstract:
A closure 10 is provided for retaining fluid pressure within a vessel, and comprises a hub 12 having an access opening to the vessel, with the hub having a circumferential stop 17 and one or more recesses 50 each extending radially outward from an adjacent inner surface 26 of the hub. A door 22 is positioned between the stop surface and the vessel, and a latch member 30 brings the door into sealing engagement with the stop member. One or more lugs 24 each extend radially outward from an exterior surface of the door, which may be tilted from a closed position to an open position then back to the closed position by a pair of cables extending from the door to outside the hub.
Abstract:
An instrument for carrying out controlled microwave assisted chemical processes is particularly useful for handling relatively small samples. The instrument includes a needle, and a needle seal adjacent the needle and having a shaft coaxial with the needle and in communication with the needle. A pressure transducer is opposite the needle seal from the needle and in communication with the shaft. A housing holds the needle to the needle seal and the needle seal to the transducer. A chamber is formed between the housing and the needle seal. A lateral shaft goes through the needle seal from the coaxial shaft to the chamber in the housing, and a valve is in communication with the chamber.
Abstract:
A vacuum roll-to-roll device includes: a first chamber; a second chamber neighboring the first chamber; a shutter disposed between the first chamber and the second chamber; a sealing member attached to the shutter; and a roll-type substrate which moves from the first chamber to the second chamber through the sealing member. A thickness of a lateral side of the roll-type substrate decreases in a direction toward an edge thereof.
Abstract:
Provided is a stirred tank polymerization reactor system having a reactor tank, a stirring assembly including a rotatable shaft that extends through a wall of the tank, and a triple barrier mechanical seal. The mechanical seal includes an outer cylinder mounted in the wall of the tank, an inner cylinder that is rotatable relative to the outer cylinder and connected to the shaft, and first, second, and third fluid barrier seals mounted between the outer and inner cylinders at different positions along the axis of rotation of the inner cylinder. First and second sources of pressurized barrier fluid are connected between the first and second pressure fluid barrier seals and the second and third barrier seals, respectively. The three barrier seals advantageously “step down” the differential pressure experienced by the uppermost barrier seals, substantially reducing mechanical stresses experienced by the annular sealing rings and seats. The mechanical seal can further include a closed loop cooling channel in its outer cylinder that is connected to a circulating source of cooling fluid.
Abstract:
A closure 10 is provided for retaining fluid pressure within a vessel, and comprises a hub 12 having an access opening to the vessel, with the hub having a circumferential stop 17 and one or more recesses 50 each extending radially outward from an adjacent inner surface 26 of the hub. A door 22 is positioned between the stop surface and the vessel, and a latch member 30 brings the door into sealing engagement with the stop member. One or more lugs 24 each extend radially outward from an exterior surface of the door, such that a respective lug engages the hub about a respective recess to seal the door to the hub, while the door may be moved to pass through the one or more recesses and out of the hub.