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公开(公告)号:US10790096B2
公开(公告)日:2020-09-29
申请号:US15752947
申请日:2016-09-07
Inventor: Yabing Qi , Min-cherl Jung , Sonia Ruiz Raga
Abstract: A method of forming a Pb-free perovskite film is provided, the method based on vacuum evaporation and comprising: first depositing a first material comprising Sn halide on a substrate to form a first layer; second depositing a second material comprising organic halide to form a second layer on the first layer to obtain a sequentially-deposited two-layer film on the substrate; and annealing the sequentially-deposited two-layer film on the substrate. During the annealing, the first and second materials inter-diffuse and react to form the Pb-free perovskite film. The second layer is formed to cover the first layer so as to prevent the first layer from air exposure. The solar cell device including the Pb-free perovskite film formed by using the present method exhibits good stability.
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公开(公告)号:US20190339219A1
公开(公告)日:2019-11-07
申请号:US16312579
申请日:2017-06-26
Inventor: Jerome Vernieres , Stephan Steinhauer , Mukhles Ibrahim Sowwan
Abstract: A gas sensor includes a substrate; a pair of electrodes facing each other on the substrate; and a plurality of metallic nanocubes each containing Fe, aggregated between the pair of electrodes and forming percolating paths between the pair of electrodes.
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公开(公告)号:US20190218657A1
公开(公告)日:2019-07-18
申请号:US16230095
申请日:2018-12-21
Inventor: Yabing QI , Luis Katsuya ONO , Shenghao WANG
CPC classification number: C23C14/24 , C23C14/06 , C23C14/545 , C23C14/548 , H01L51/001 , H01L51/0012 , H01L51/42 , H01L51/44 , Y02E10/549
Abstract: A system and method for fabricating perovskite films for solar cell applications are provided, the system including a housing for use as a vacuum chamber, a substrate stage coupled to the top section of the housing; a first evaporator unit coupled to the bottom section of the housing and configured to generate BX2 (metal halide material) vapor; a second evaporator unit coupled to the housing and configured to generate AX (organic material) vapor; and a flow control unit coupled to the housing for controlling circulation of the AX vapor. The dimensions of the horizontal cross-sectional shape of the first evaporator unit, the dimensions of the horizontal cross-sectional shape of the substrate stage, and the relative position in the horizontal direction between the two horizontal cross-sectional shapes are configured to maximize the overlap between the two horizontal cross-sectional shapes.
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公开(公告)号:US20190211453A1
公开(公告)日:2019-07-11
申请号:US16357837
申请日:2019-03-19
Inventor: Yabing Qi , Luis Ono , Shenghao Wang
IPC: C23C16/52 , C23C14/54 , C23C16/46 , C23C14/06 , C23C14/12 , C23C14/24 , C23C14/50 , C23C16/455 , C23C16/40 , H01L31/0256
Abstract: A system and method for fabricating a perovskite film is provided, the system including a substrate stage configured to rotate around its central axis at a rotation speed, a first set of evaporation units, each coupled to the side section or the bottom section of the chamber, a second set of evaporation units coupled to the bottom section, and a shield defining two or more zones having respective horizontal cross-sectional areas, which are open and facing the substrate, designated for the two or more evaporation units in the second set. The resultant perovskite film includes multiple unit layers, wherein each unit layer is formed by one rotation of the substrate stage, and the composition and thickness of the unit layer are controlled by adjusting at least the evaporation rates, the rotation speed and the horizontal cross-sectional areas.
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15.
公开(公告)号:US20190187034A1
公开(公告)日:2019-06-20
申请号:US16311342
申请日:2017-06-20
Inventor: Doojin Lee , Amy Shen Fried
CPC classification number: G01N13/02 , B01L3/502707 , B01L7/00 , B01L7/54 , B01L2300/0627 , B01L2300/0663 , B01L2300/0816 , B01L2300/1827 , G01N2013/0216
Abstract: A temperature-controllable microfluidic device includes: a microfluidic channel generally extending in a first direction for passing a specimen fluid; a microheater disposed along the microfluidic channel, the microheater being made of a resistive wire having a pair of serpentine-shaped portions generally extending in the first direction along respective sides of the microfluidic channel; and a temperature sensor disposed along the microfluidic channel, the temperature sensor being made of a resistive wire having a pair of serpentine-shaped portions generally extending in the first direction along the respective sides of the microfluidic channel.
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16.
公开(公告)号:US20190087751A1
公开(公告)日:2019-03-21
申请号:US16130482
申请日:2018-09-13
Inventor: Tomotake Sasaki , Eiji Uchibe , Kenji Doya , Hirokazu Anai , Hitoshi Yanami , Hidenao Iwane
Abstract: A non-transitory, computer-readable recording medium stores therein a reinforcement learning program that uses a value function and causes a computer to execute a process comprising: estimating first coefficients of the value function represented in a quadratic form of inputs at times in the past than a present time and outputs at the present time and the times in the past, the first coefficients being estimated based on inputs at the times in the past, the outputs at the present time and the times in the past, and costs or rewards that corresponds to the inputs at the times in the past; and determining second coefficients that defines a control law, based on the value function that uses the estimated first coefficients and determining input values at times after estimation of the first coefficients.
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公开(公告)号:US10084145B2
公开(公告)日:2018-09-25
申请号:US15523500
申请日:2015-11-05
Inventor: Yabing Qi , Min-Cherl Jung , Sonia Ruiz Raga
Abstract: An optoelectronic device is provided, the device comprising an active layer comprising organometal halide perovskite and a hole transport layer (HTL) formed by vacuum evaporation and configured to transport hole carriers. The HTL includes a first sublayer comprising a hole transport material (HTM) doped with an n-dopant and disposed adjacent to the active layer, a second sublayer comprising the HTM that is undoped and disposed adjacent to the first sublayer, and a third sublayer comprising the HTM doped with a p-dopant and disposed adjacent to the second sublayer. The doping concentration of the n-dopant for the n-doped sublayer is determined to match the highest occupied molecular orbital energy level of the n-doped sublayer with the valence band maximum energy level of the perovskite active layer.
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公开(公告)号:US20180247769A1
公开(公告)日:2018-08-30
申请号:US15752947
申请日:2016-09-07
Inventor: Yabing Qi , Min-cherl Jung , Sonia Ruiz Raga
Abstract: A method of forming a Pb-free perovskite film is provided, the method based on vacuum evaporation and comprising: first depositing a first material comprising Sn halide on a substrate to form a first layer; second depositing a second material comprising organic halide to form a second layer on the first layer to obtain a sequentially-deposited two-layer film on the substrate; and annealing the sequentially-deposited two-layer film on the substrate. During the annealing, the first and second materials inter-diffuse and react to form the Pb-free perovskite film. The second layer is formed to cover the first layer so as to prevent the first layer from air exposure. The solar cell device including the Pb-free perovskite film formed by using the present method exhibits good stability.
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公开(公告)号:US09630940B2
公开(公告)日:2017-04-25
申请号:US15148716
申请日:2016-05-06
Inventor: Pandurang V. Chouthaiwale , Fujie Tanaka
IPC: C07D309/28 , C07D309/16 , C07C201/14 , C07D309/30 , C07D317/30 , C07D407/04 , C07D241/44 , C07D243/02 , C07D307/54 , C07C205/55
CPC classification number: C07D309/28 , C07C201/14 , C07C205/55 , C07C2601/14 , C07D241/44 , C07D243/02 , C07D307/54 , C07D309/30 , C07D317/30 , C07D407/04
Abstract: Disclosed is a process for preparing dihydro-2H-pyran derivatives of formula I: wherein R1 and R2 are defined herein. The process of the invention provides the compound of formula I in concise cascade reactions and in one pot. The compound of formulae I prepared by the process of the invention and its further transformed derivatives are useful for making pharmaceutical composition for the treatment of proliferative diseases.
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公开(公告)号:US20160071690A1
公开(公告)日:2016-03-10
申请号:US14888414
申请日:2014-05-14
Inventor: Tsumoru SHINTAKE
IPC: H01J37/244 , H01J37/295
CPC classification number: H01J37/244 , G01N23/20 , H01J37/2955 , H01J2237/2449 , H01J2237/24578 , H01J2237/2544 , H01J2237/2803
Abstract: A low energy electron diffraction (LEED) detection module (100) includes: a first vacuum chamber for receiving diffracted electrons from a specimen (109); a larger second vacuum chamber connected to the first vacuum chamber to receive the diffracted electrons that have been transported through the first vacuum chamber; a two-dimensional electron detector disposed in the second vacuum chamber to detect the diffracted electrons; a potential shield (106) disposed generally along an inner surface of the first vacuum chamber and an inner surface of the second vacuum chamber; a magnetic lens (105) to expand a beam of the diffracted electrons that have been transported through the first vacuum chamber towards the two-dimensional electron detector; and a generally plane-shaped energy filter (103) to repel electrons having an energy lower than the probe beam (203) of electrons that impinges on the specimen (109).
Abstract translation: 低能电子衍射(LEED)检测模块(100)包括:用于从样品(109)接收衍射电子的第一真空室; 连接到第一真空室的较大的第二真空室,以接收已经传送通过第一真空室的衍射电子; 设置在第二真空室中以检测衍射电子的二维电子检测器; 大致沿第一真空室的内表面设置的电位屏蔽件(106)和第二真空室的内表面; 用于将已经通过第一真空室传送的衍射电子束朝向二维电子检测器扩大的磁性透镜(105); 和大致平面状的能量过滤器(103),以排斥能量低于碰撞在样本(109)上的电子的探针光束(203)的能量的电子。
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