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    THIN-LAYER CHROMATOGRAPHY PLATE
    42.
    发明申请
    THIN-LAYER CHROMATOGRAPHY PLATE 有权
    薄层色谱板

    公开(公告)号：US20140248196A1

    公开(公告)日：2014-09-04

    申请号：US14348989

    申请日：2012-10-04

    Applicant: DAICEL CORPORATION

    Inventor： Toshiharu Minoda ,  Isamu Ikeda

    IPC: G01N30/92

    CPC classification number: G01N30/92 ,  B01D15/3833 ,  B01J20/285 ,  B01J20/286 ,  B01J20/29 ,  G01N2030/8877

    Abstract: An object of the present invention is to provide a TLC plate which allows separation and detection of target substances on one plate. Provided is a TLC plate comprising a substrate, a separating medium layer stacked on the substrate, and a permeation layer stacked on the separating medium layer and allowing permeation of a target substance separated in the separating medium layer, wherein the separating medium layer has separating property for the target substance and optical responsiveness for ultraviolet rays, and the permeation layer has optical responsiveness different from that of the separating medium layer.

    Abstract translation: 本发明的目的是提供一种TLC板，其允许在一个板上分离和检测目标物质。 提供了一种TLC板，其包括基板，层叠在基板上的分离介质层和层叠在分离介质层上的渗透层，并允许在分离介质层中分离的目标物质渗透，其中分离介质层具有分离性 对于目标物质和紫外线的光响应性，透过层具有与分离介质层不同的光响应性。

    Disposable monolithic column
    43.
    发明授权
    Disposable monolithic column 有权
    一次性整体柱

    公开(公告)号：US08795529B2

    公开(公告)日：2014-08-05

    申请号：US11932526

    申请日：2007-10-31

    Applicant: Shaofeng Xie

    Inventor： Shaofeng Xie

    IPC: B01J20/30 ,  B01J20/283 ,  B01J20/285 ,  B01D15/20 ,  G01N30/52

    CPC classification number: B01J20/3064 ,  B01D15/206 ,  B01J8/0005 ,  B01J19/0013 ,  B01J19/18 ,  B01J20/283 ,  B01J20/285 ,  B01J2219/00162 ,  B01J2220/54 ,  B01J2220/82 ,  G01N30/56 ,  G01N2030/522 ,  G01N2030/528 ,  G01N2030/567 ,  G01N30/30

    Abstract: Permeable polymeric monolithic materials are prepared in a plastic column casing. In one embodiment, the permeable polymeric monolithic materials are polymerized by the application of heat from an external source starting at a low temperature such as 40 degrees centigrade, depending on the mixture and size of the column, and continuing at a higher temperature, such as 60 degrees centigrade. The temperature at the start of the polymerization is low enough so as not to cause exothermal run-away conditions and to avoid high heat of reaction that would prevent a substantially constant temperature across the cross-section of the column. The higher temperature is used after sufficient monomer depletion has occurred and steric interference has increased so the polymerization reaction is sufficiently slow to avoid heat of reaction generation high enough to cause significant reduction in the homogeneousness of the pore sizes.

    Abstract translation: 在塑料柱套管中制备可渗透的聚合物整体材料。 在一个实施方案中，可透过的聚合物整体材料通过根据柱的混合物和尺寸从外部源起始于低温（例如40℃）进行聚合，并在较高温度下继续进行，例如 60摄氏度。 聚合开始时的温度足够低，从而不会引起放热的脱离条件，并避免高度的反应热，从而阻止整个塔的截面上的基本恒定的温度。 在发生足够的单体消耗并且空间干扰增加之后使用较高的温度，因此聚合反应足够慢，以避免足够高的反应产生热，导致孔径的均匀性显着降低。

    Porous cellulose gel, method for producing the same and use thereof
    46.
    发明授权
    Porous cellulose gel, method for producing the same and use thereof 有权
    多孔纤维素凝胶，其制造方法及其用途

    公开(公告)号：US08664152B2

    公开(公告)日：2014-03-04

    申请号：US12199715

    申请日：2008-08-27

    Applicant: Yasuto Umeda ,  Yasuo Matsumoto ,  Masami Shiina ,  Masami Todokoro ,  Yoshihiro Matsumoto

    Inventor： Yasuto Umeda ,  Yasuo Matsumoto ,  Masami Shiina ,  Masami Todokoro ,  Yoshihiro Matsumoto

    IPC: B01J20/291 ,  B05D5/00

    CPC classification number: B01J20/291 ,  B01J20/26 ,  B01J20/262 ,  B01J20/265 ,  B01J20/267 ,  B01J20/285 ,  C08B5/14 ,  C08L1/16

    Abstract: The present invention provides a porous cellulose gel having a high mechanical strength capable of being operated at a higher flow rate, and a method for producing the same. To a suspension liquid of cellulose particles, a crosslinking agent in an amount of from 4 to 12 times the amount of the cellulose monomer in terms of moles and an alkali in an amount of from 0.1 to 1.5 times the amount of the crosslinking agent in terms of moles are added continuously dropwise or added dividedly over a prescribed period of time, whereby flow rate characteristics of a resulting porous cellulose gel can be enhanced. According to the invention, the production efficiency of a polymer substance, such as a nucleic acid and a protein can be enhanced.

    Abstract translation: 本发明提供了能够以较高流量运转的机械强度高的多孔纤维素凝胶及其制造方法。 对于纤维素颗粒的悬浮液，交联剂的量为纤维素单体的摩尔数的4至12倍，碱的量为交联剂的量的0.1至1.5倍 连续滴加或分时加入规定的时间，由此可以提高所得多孔纤维素凝胶的流动速率特性。 根据本发明，可以提高聚合物物质如核酸和蛋白质的生产效率。

    Monolithic organic copolymer
    47.
    发明授权
    Monolithic organic copolymer 有权
    单片有机共聚物

    公开(公告)号：US08586641B2

    公开(公告)日：2013-11-19

    申请号：US11551181

    申请日：2006-10-19

    Applicant: Lukas Trojer ,  Günther Bonn

    Inventor： Lukas Trojer ,  Günther Bonn

    IPC: C08F220/06 ,  C08F220/14 ,  C08F236/20 ,  C08F212/08 ,  C08J9/28 ,  B01D15/08

    CPC classification number: C08J9/28 ,  B01J20/261 ,  B01J20/264 ,  B01J20/28042 ,  B01J20/285 ,  B01J2220/82 ,  C08J2201/0543 ,  C08J2201/0546 ,  C08J2325/08

    Abstract: The present invention relates to a monolithic organic copolymer prepared by copolymerization of at least one monomer of the group consisting of styrene, (C1-C3)alkylstyrene, (meth)acrylic acid and esters thereof with a crosslinker in the presence of a macroporogen and a microporogen, wherein a) the sum of said at least one monomer of the group and the crosslinker is 10-20%, preferably 10-15%, by volume of the reaction mixture, with the rest being essentially macroporogen and microporogen, and the degree of said copolymerization is at least 70%, preferably at least 90%, more preferably at least 99%, or b) the sum of said at least one monomer of the group and the crosslinker is 30-50%, preferably 35-45%, by volume of the reaction mixture, with the rest being essentially macroporogen and microporogen, and the degree of said copolymerization is in the range of 25-60%, preferably 35-50%. These copolymers can be used in high-performance liquid chromatography for the separation of biopolymers as well as small molecules.

    Abstract translation: 本发明涉及一种整体式有机共聚物，其通过在大孔原子存在下将苯乙烯，（C1-C3）烷基苯乙烯，（甲基）丙烯酸及其酯与至少一种单体与交联剂共聚而成， 微生物，其中a）所述基团和交联剂的所述至少一种单体的总和为反应混合物的体积的10-20％，优选10-15％，其余基本上为大孔隙和微孔，以及程度 的所述共聚物为至少70％，优选至少90％，更优选至少99％，或b）所述基团和交联剂的所述至少一种单体之和为30-50％，优选35-45％ ，反应混合物的体积，其余基本上是大孔原子和微孔，并且所述共聚的程度在25-60％，优选35-50％的范围内。 这些共聚物可用于高效液相色谱分离生物聚合物以及小分子。

    Methods for making polymer beads
    50.
    发明授权
    Methods for making polymer beads 有权
    聚合物珠粒的制备方法

    公开(公告)号：US08481603B2

    公开(公告)日：2013-07-09

    申请号：US12085260

    申请日：2006-12-06

    Applicant: Ecevit Yilmaz ,  Johan Billing

    Inventor： Ecevit Yilmaz ,  Johan Billing

    IPC: C08J9/26 ,  C08J9/00

    CPC classification number: C08F2/18 ,  B01J20/26 ,  B01J20/268 ,  B01J20/285 ,  B01J20/305 ,  B01J20/3057 ,  C08F2/44 ,  C08F212/08 ,  C08F212/36

    Abstract: The present invention relates to a polymer bead material that are characterised by having pore sizes that can be pre-determined and that can be obtained with a narrow distribution of such pore sizes created by use of sacrificial filler materials within the polymer material. The invention also discloses processes for production of the material as spherical or approximately spherical beads or resins with predefined sizes. Also, the invention relates to the preparation of molecularly imprinted polymer materials that are created by the said method. Further the invention relates to the use of said polymer materials for separation, detection, catalysis or entrapment of chemicals, metal ions, inorganic compounds, drags, peptides, proteins, DNA, natural and artificial polymers, natural or artificial compounds, food or pharma products, viruses, bacteria, cells and other entities.

    Abstract translation: 本发明涉及一种聚合物珠粒材料，其特征在于具有可以预先确定的孔径，并且可以通过在聚合物材料中使用牺牲填料材料产生的这种孔径的窄分布来获得。 本发明还公开了用于制备具有预定尺寸的球形或近似球形的珠粒或树脂的材料的方法。 此外，本发明涉及通过所述方法制备的分子印迹聚合物材料的制备。 此外，本发明涉及所述聚合物材料用于分离，检测，催化或捕获化学品，金属离子，无机化合物，拖动剂，肽，蛋白质，DNA，天然和人造聚合物，天然或人造化合物，食品或制药产品 ，病毒，细菌，细胞等实体。

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