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    N-3-oxohydrocarbon-substituted acrylamides and polymers thereof
    71.
    发明授权
    N-3-oxohydrocarbon-substituted acrylamides and polymers thereof 失效
    N-3-氧代烃取代的丙烯酰胺及其聚合物

    公开(公告)号：US3277056A

    公开(公告)日：1966-10-04

    申请号：US32639463

    申请日：1963-11-27

    Applicant: LUBRIZOL CORP

    Inventor： COLEMAN LESTER E

    IPC: C08F20/58 ,  C08F20/62 ,  C08L33/26 ,  C10L1/236 ,  C10M149/06

    CPC classification number: C10M149/06 ,  C08F20/58 ,  C08F20/62 ,  C08L33/26 ,  C10L1/2364 ,  C10M143/00 ,  C10M145/12 ,  C10M149/10 ,  C10M2205/00 ,  C10M2205/02 ,  C10M2207/026 ,  C10M2207/16 ,  C10M2207/40 ,  C10M2207/404 ,  C10M2209/082 ,  C10M2211/08 ,  C10M2215/065 ,  C10M2217/024 ,  C10M2217/028 ,  C10M2217/06 ,  C10M2219/044 ,  C10M2219/082 ,  C10M2223/04 ,  C10M2223/042 ,  C10M2223/045 ,  C10M2229/02 ,  C10M2229/05 ,  C10N2210/02 ,  C10N2210/08 ,  C08L2666/02

    Abstract: A lubricating composition comprises a mineral, vegetable, animal, silicone or synthetic polyester oil in admixture with a minor proportion of a homopolymer or copolymer of an N-3-oxohydrocarbon-substituted acrylamide of the formula R.CO.R1-NHCOC(R11)=CH2 wherein R and R11 represent hydrogen or C1- 10 alkyl or cycloalkyl radicals and R1 represents an ethylene radical or an ethylene radical substituted by a C1- 10 alkyl or cycloalkyl group, with the proviso that at least one such group is on the carbon atom attached to the nitrogen atom of the acrylamide group. The composition may contain as additional ingredients sulphonates, thiophosphates, phosphites,amines, phenols, disulphides and chlorinated wax.ALSO:Novel N-3-oxohydrocarbon-substituted acrylamides of the formula R.CO.R1-NHCOC(R11) = CH2 wherein R and R11 represent hydrogen or C1- 10 alkyl or cycloalkyl radicals and R1 represents an ethylene radical or an ethylene radical substituted by a C1- 10 alkyl or cycloalkyl group, with the proviso that at least one such group is on the carbon atom attached to the nitrogen atom of the acrylamide group, are prepared by reacting at a temperature below 100 DEG C. one mol. of an acrylonitrile of the formula CH2 = C(R11)-CN with either one mole of a beta-hydroxy oxohydrocarbon of the formula R.COC(R111)2.C(R111)2-OH or two moles of an aliphatic oxohydrocarbon of the formula R1.COCH(R2)2 in the presence of at least one mole of sulphuric acid, and subse hydrolysing the product, R111 representing hydrogen or a C1- 10 alkyl or cycloalkyl group, with the proviso that if any R111 represents a C1- 10 alkyl or cycloalkyl group at least one of the R111 radicals on the carbon atom adjacent the OH group represents a C1- 10 alkyl or cycloalkyl group, and each of R1 and R2 representing hydrogen or a C1- 10 alkyl or cycloalkyl radical, with the proviso that the sum of the carbon atoms in the two R2 groups does not exceed 9.ALSO:N - 3 - Oxohydrocarbon - substituted acrylamides of the formula R.CO.R1-NHCOC(R11)=CH2 wherein R and R11 represent hydrogen or C1- 10 alkyl or cycloalkyl radicals and R1 represents an ethylene radical or an ethylene radical substituted by a C1- 10 alkyl or cycloalkyl group, with the proviso that at least one such group is on the carbon atom attached to the nitrogen atom of the acrylamide group, are polymerized alone or in admixture with other ethylenically unsaturated compounds in the presence of azo, peroxide, sodium in ammonia, Ziegler, metal aryl or metal alkyl catalysts, or using heat or gamma ray irradiation. Suitable comonomers include esters of unsaturated alcohols, polyols or unsaturated acids, vinyl cyclic compounds, vinyl halides and unsaturated ethers, ketones, amides, aliphatic hydrocarbons, acids, acid anhydrides, acid chlorides and nitriles. Examples describe the preparation of homopolymers, copolymers and terpolymers using as comonomers decyl acrylate, vinyl acetate, mixtures of dialkyl fumarates, N-vinyl pyrrolidone, N-vinyloxazolidone, isoprene and acrylonitrile, and employing benzene/azobisisobutyronitrile or benzoyl peroxide, tetrahydrofuran/sodium naphthalene or sodium/liquid ammonia solvent/catalysts systems.

    Methods and systems for predicting a need for introducing anti-fouling additives to a hydrocarbon stream to reduce fouling of crude hydrocarbon refinery components
    78.
    发明授权
    Methods and systems for predicting a need for introducing anti-fouling additives to a hydrocarbon stream to reduce fouling of crude hydrocarbon refinery components 有权
    用于预测将污垢添加剂引入烃流的需要的方法和系统，以减少粗炼油部件的结垢

    公开(公告)号：US09416325B2

    公开(公告)日：2016-08-16

    申请号：US14132103

    申请日：2013-12-18

    Applicant: Glen B. Brons

    Inventor： Glen B. Brons

    IPC: C10G75/04 ,  G01F3/00 ,  C08F8/32 ,  C10L1/236 ,  C10L1/2383 ,  C10L10/04

    CPC classification number: C10G75/04 ,  C08F8/32 ,  C10L1/2364 ,  C10L1/2383 ,  C10L10/04 ,  C10L2290/141 ,  C10L2290/58 ,  C10L2290/60 ,  G01F3/00

    Abstract: Method and system for predicting a need for introducing anti-fouling additives to a hydrocarbon stream in a hydrocarbon refinery. The method comprises characterizing whether the hydrocarbon stream is a non-high solvency dispersive power (“HSDP”) crude and performing at least one of determining whether the hydrocarbon stream is subject to filterable solids levels greater than about 100 wppm or classifying whether the hydrocarbon stream has an expected low flow velocity during normal operating conditions within the refinery. The method further comprises indicating, using a processor, that anti-fouling additives are recommended if the hydrocarbon stream is characterized to be a non-HSDP crude and either the hydrocarbon stream is determined to be subject to filterable solids levels greater than about 100 wppm or the hydrocarbon stream is classified as having expected low flow within a heat exchanger of the refinery.

    Abstract translation: 用于预测在烃精炼厂中向烃流引入防污添加剂的需求的方法和系统。 该方法包括表征烃流是否是非高溶解力分散能力（“HSDP”）粗品，并且执行至少一种以确定烃流是否经受大于约100wppm的可过滤固体水平或分级烃流 在炼油厂的正常运行条件下具有预期的低流速。 该方法还包括使用处理器指示如果烃流被表征为非HSDP原油并且烃流被确定为经受大于约100wppm的可过滤固体水平，则建议使用防污添加剂，或 烃流被分类为在炼油厂的热交换器内具有预期的低流量。

    Additives for improving the cold properties of fuel oils
    80.
    发明授权
    Additives for improving the cold properties of fuel oils 有权
    用于改善燃油的冷特性的添加剂

    公开(公告)号：US08968428B2

    公开(公告)日：2015-03-03

    申请号：US11879431

    申请日：2007-07-17

    Applicant: Bettina Siggelkow ,  Werner Reimann ,  Matthias Krull ,  Ulrike Neuhaus ,  Markus Kupetz ,  Andre Graf

    Inventor： Bettina Siggelkow ,  Werner Reimann ,  Matthias Krull ,  Ulrike Neuhaus ,  Markus Kupetz ,  Andre Graf

    IPC: C10L1/196 ,  C10M145/10 ,  C10L1/14 ,  C10L10/14 ,  C10L1/16 ,  C10L1/197 ,  C10L1/198 ,  C10L1/224 ,  C10L1/236

    CPC classification number: C10L1/146 ,  C10L1/1641 ,  C10L1/165 ,  C10L1/1658 ,  C10L1/1966 ,  C10L1/1973 ,  C10L1/1981 ,  C10L1/1985 ,  C10L1/224 ,  C10L1/2364 ,  C10L10/14

    Abstract: The invention provides additive mixtures comprising A) at least one terpolymer of ethylene, propene and at least one ethylenically unsaturated ester, which i) contains from 6.0 to 12.0 mol % of structural units derived from at least one ethylenically unsaturated ester having a C1- to C3-alkyl radical, ii) contains from 0.5 to 4.0 methyl groups derived from propene per 100 aliphatic carbon atoms, iii) has fewer than 8.0 methyl groups stemming from chain ends per 100 CH2 groups, and B) from 0.5 to 20 parts by weight, based on A), of at least one further component which is effective as a cold additive for mineral oils and is selected from B1) copolymers of ethylene and ethylenically unsaturated compounds whose content of ethylenically unsaturated compounds is at least 2 mol % higher than the content of ethylenically unsaturated esters in the terpolymer defined under A), B2) comb polymers, and B3) mixtures of B1) and B2), and also their use as a cold additive for middle distillates.

    Abstract translation: 本发明提供添加剂混合物，其包括A）至少一种乙烯，丙烯和至少一种烯键式不饱和酯的三元共聚物，其i）含有6.0至12.0mol％的至少一种烯属不饱和酯的结构单元，其具有C1-至 C3-烷基，ii）含有每100个脂族碳原子衍生自丙烯的0.5至4.0个甲基，iii）由每100个CH 2基团的链端衍生的少于8.0个甲基，和B）0.5至20重量份 基于A）的至少一种作为矿物油的冷添加剂有效的其它组分，并且选自B1）乙烯和烯属不饱和化合物的共聚物，其烯键式不饱和化合物的含量比所述烯属不饱和化合物的含量高至少2摩尔％ 在A），B2）梳状聚合物和B3）B1）和B2的混合物中定义的三元共聚物中的烯键式不饱和酯的含量，以及它们作为中间馏分的冷添加剂的用途。

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