Apparatus and process for purification of aromatic carboxylic acid
    6.
    发明授权
    Apparatus and process for purification of aromatic carboxylic acid 有权
    用于芳族羧酸纯化的装置和方法

    公开(公告)号:US09302973B2

    公开(公告)日:2016-04-05

    申请号:US14433831

    申请日:2013-10-31

    Abstract: In a reaction vessel for the purification of crude aromatic carboxylic acid, a bed of hydrogenation catalyst having a vapor space is located above the hydrogenation catalyst bed. A packed bed and a holdup section are located within the vapor space and spaced above the catalyst bed. The reaction vessel has means for introducing crude aromatic carboxylic acid and means for introducing hydrogen to the reaction vessel at respective locations such that in use the crude carboxylic acid contacts the hydrogen in the packed bed. The reaction vessel also has means for removing purified aromatic carboxylic acid.

    Abstract translation: 在用于净化粗芳香族羧酸的反应容器中,具有蒸气空间的氢化催化剂床位于氢化催化剂床的上方。 填充床和保持部分位于蒸气空间内并在催化剂床之上间隔开。 反应容器具有引入粗芳族羧酸的装置和在相应位置将氢引入反应容器的装置,使得在使用中,粗羧酸与填充床中的氢接触。 反应容器还具有除去纯化的芳族羧酸的方法。

    C-11 cyanide production system
    8.
    发明授权
    C-11 cyanide production system 有权
    C-11氰化物生产系统

    公开(公告)号:US08932551B2

    公开(公告)日:2015-01-13

    申请号:US13584033

    申请日:2012-08-13

    Abstract: A method for providing 11C-labeled cyanides from 11C labeled oxides in a target gas stream retrieved from an irradiated high pressure gaseous target containing O2 is provided, wherein 11C labeled oxides are reduced with H2 in the presence of a nickel catalyst under a pressure and a temperature sufficient to form a product stream comprising at least about 95% 11CH4 , the 11CH4 is then combined with an excess of NH3 in a carrier/reaction stream flowing at an accelerated velocity and the combined 11CH4 carrier/reaction stream is then contacted with a platinum (Pt) catalyst particulate supported on a substantially-chemically-nonreactive heat-stable support at a temperature of at least about 900 ° C., whereby a product stream comprising at least about 60%H11CN is provided in less than 10 minutes from retrieval of the 11C labeled oxide.

    Abstract translation: 提供了一种从含有O 2的被照射的高压气态靶中提取的目标气体流中的11C标记的氧化物提供11C标记的氰化物的方法,其中在镍催化剂存在下,在压力下,用H 2还原11℃标记的氧化物, 温度足以形成包含至少约95%11CH4的产物流,然后将11CH4与以加速速度流动的载体/反应物流中的过量NH 3合并,然后将组合的11CH 4载体/反应物流与铂 (Pt)催化剂颗粒,其在至少约900℃的温度下负载在基本上化学反应性的热稳定性载体上,由此在不到10分钟内提供包含至少约60%H11CN的产物流, 11C标记的氧化物。

Patent Agency Ranking