公开(公告)号：US20190233607A1

公开(公告)日：2019-08-01

申请号：US16375904

申请日：2019-04-05

Applicant: Virginia Commonwealth University

Inventor： Massimo Bertino

IPC: C08J9/28 ,  C01B33/158 ,  B01J13/00

CPC classification number: C08J9/28 ,  B01J13/0091 ,  C01B33/1585 ,  C08J9/286 ,  C08J2201/022 ,  C08J2201/026 ,  C08J2201/0522 ,  C08J2201/0524 ,  C08J2205/026 ,  C08J2205/042 ,  C08J2333/08 ,  C08J2383/06 ,  C08L33/08 ,  Y02P20/544

Abstract: A method of synthesizing aerogels and cross-linked aerogels in a single step and in a single pot without requiring any solvent exchange is described. Porous matrices are synthesized through a modification of hydrolysis condensation of alkoxides in which addition of water is minimized. The reaction occurs in an ethanol-water azeotrope mixture; the water in the azeotrope slowly hydrolyzes the alkoxide. Additionally, after gelation, the porous matrix is dried in supercritical ethanol rather than liquid CO2, which allows for elimination of solvent exchange steps. These modifications allow for the preparation of aerogel monoliths in any size in one step and in one pot and much faster than conventional procedures. In addition, the method provides for custom aerogel parts with large dimensions, as well as high volume fabrication of aerogels. The custom aerogel parts may be used in a variety of thermal insulation applications.

公开(公告)号：US20160096941A1

公开(公告)日：2016-04-07

申请号：US14507523

申请日：2014-10-06

Applicant: The Regents of the University of Michigan

Inventor： Peter X. Ma ,  Zhanpeng Zhang

IPC: C08J9/28

CPC classification number: C08J9/28 ,  C08J9/16 ,  C08J2201/0484 ,  C08J2201/0522 ,  C08J2205/044 ,  C08J2207/10 ,  C08J2300/206 ,  C08J2367/04

Abstract: A nanofibrous spongy microsphere includes porous walls that define an exterior of the microsphere and that extend through an interior of the microsphere. The porous walls consist of interconnected nanofibers and spaces formed between the interconnected nanofibers. A plurality of micro-scale pores are formed throughout the interior of the microsphere. Each of the micro-scale pores i) is partially defined by the porous walls, ii) has an interpore opening that opens to an adjacent micro-scale pores, and iii) has a diameter ranging from about 1 μm to about 100 μm. A total diameter of the microsphere ranges from about 5 μm to about 1000 μm.

Abstract translation: 纳米纤维海绵状微球包括限定微球的外部并延伸穿过微球内部的多孔壁。 多孔壁由互连的纳米纤维和互连的纳米纤维之间形成的空间组成。 在微球的整个内部形成多个微尺度孔。 每个微尺度孔隙i）部分地由多孔壁限定，ii）具有通向相邻的微尺度孔隙的插层孔，以及iii）具有约1μm至约100μm的直径。 微球的总直径为约5μm至约1000μm。

公开(公告)号：US20150057367A1

公开(公告)日：2015-02-26

申请号：US14474217

申请日：2014-09-01

Applicant: Bridgestone Corporation

Inventor： Xiaorong Wang ,  Mindaugas Rackaitis ,  Naruhiko Mashita ,  Victor Foltz

IPC: C08J9/28 ,  C08J9/36

CPC classification number: C08J9/28 ,  C08J9/36 ,  C08J2201/0522 ,  C08J2201/0542 ,  C08J2353/00 ,  C09K19/544 ,  C11D17/0039 ,  H01F1/44

Abstract: Micro-sized particles having a polymeric structure of cells are provided. Also provided is a method of producing micro-sized particles having a polymeric structure comprising: (1) forming a homogenous solution by heating a mixture of a high molecular weight polymer and a low molecular weight material, wherein said low molecular weight material makes up at least about 50% by weight of the homogenous solution, (2) forming a dispersed solution by dispersing the homogenous solution formed in step (1) into an inert material, (3) cooling the dispersed solution to cause the high molecular weight polymer to phase separate from the low molecular weight material, (4) forming solid particles comprised of said low molecular weight material trapped inside a structure of cells of said high molecular weight polymer, and (5) removing the solid particles from the dispersed solution.

公开(公告)号：US20150018442A1

公开(公告)日：2015-01-15

申请号：US14444530

申请日：2014-07-28

Applicant: LG CHEM, LTD

Inventor： Bong-Tae KIM ,  Heon-Sik SONG ,  Seung-Yup LEE ,  Kyoung-Min KIM

IPC: C08J5/18 ,  B29C47/00

CPC classification number: C08J5/18 ,  B29C47/0071 ,  B29D7/01 ,  B29L2007/008 ,  C08J2201/03 ,  C08J2201/0522 ,  C08J2323/02 ,  C08J2323/06 ,  C08L23/02

Abstract: The present invention discloses a method for preparing a microporous polyolefin film comprising: a step of injecting a composition comprising polyolefin 30 to 60 wt % and a diluent mixture comprising a diluent, which can make liquid-liquid phase separation with the polyolefin thermodynamically 40 to 70 wt %, into an extruding machine, and melting and kneading thereof to prepare a single phase melt; and a step of extruding the melt while conducting liquid-liquid phase separation by passing through a section having the temperature below the liquid-liquid phase separation temperature and forming thereof in the form of a sheet, and a microporous polyolefin film prepared according to the method.

Abstract translation: 本发明公开了一种微孔性聚烯烃膜的制造方法，其特征在于，包括以下步骤：将含有聚烯烃30〜60重量％的组合物和包含稀释剂的稀释剂混合物进行热力学动力学分析， wt％进入挤出机，并将其熔融和捏合以制备单相熔体; 以及通过使液体 - 液相分离温度低于液 - 液相分离温度的部分进行液 - 液相分离而挤出熔融物的步骤，并将其形成为片状，以及根据该方法制备的微孔聚烯烃膜 。

公开(公告)号：US20120219799A1

公开(公告)日：2012-08-30

申请号：US13505880

申请日：2010-11-19

Applicant: Akihiro Omori

Inventor： Akihiro Omori

IPC: B01J20/26 ,  B05B17/04

CPC classification number: C02F1/288 ,  B01J20/06 ,  B01J20/08 ,  B01J20/16 ,  B01J20/262 ,  B01J20/28004 ,  B01J20/28042 ,  B01J20/28057 ,  B01J20/28088 ,  B01J20/3021 ,  B01J20/3085 ,  B01J20/3204 ,  B01J20/3236 ,  C08J3/16 ,  C08J9/28 ,  C08J2201/0522 ,  C08J2381/06 ,  C08J2481/06 ,  Y10T428/2982

Abstract: There is provided a porous formed article which can remove hazardous substances at a high speed, has a high adsorption capacity and has high durability to cleaning chemicals and further which is scarcely broken even if being repeatedly used, and which contains an organic polymeric resin and an inorganic ion-adsorbing material, wherein the organic polymeric resin is a polyether sulfone resin and/or a polysulfone resin, and is an organic polymeric resin having a hydroxyl group.

Abstract translation: 提供一种能够高速除去有害物质，具有高吸附能力，对清洗化学品具有高耐久性的多孔成形制品，而且即使重复使用也几乎不破裂，并且其含有有机聚合物树脂和 无机离子吸附材料，其中有机聚合物树脂是聚醚砜树脂和/或聚砜树脂，并且是具有羟基的有机聚合物树脂。

公开(公告)号：US11807732B2

公开(公告)日：2023-11-07

申请号：US16760468

申请日：2018-11-15

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Derek J. Dehn ,  Clinton P. Waller, Jr. ,  Jeanne M. Bruss ,  Bharat R. Acharya ,  Brandon A. Bartling ,  Michael S. Graff ,  Noah O. Shanti ,  Fabian Stolzenburg ,  Satinder K. Nayar

IPC: C08J9/28 ,  C08K3/22 ,  C08J9/00

CPC classification number: C08J9/28 ,  C08J9/0004 ,  C08J9/0066 ,  C08K3/22 ,  C08J2201/0522 ,  C08J2201/0542 ,  C08J2205/05 ,  C08J2323/06 ,  C08K2003/2237 ,  C08K2201/001 ,  C08K2201/01

Abstract: Method of making a polymer matrix composite comprising a porous polymeric network structure; and a plurality of particles distributed within the polymeric network structure, the method comprising: combining a thermoplastic polymer, a solvent that the thermoplastic polymer is soluble in, and a plurality of particles to provide a slurry; forming the slurry in to an article; heating the article in an environment to retain at least 90 percent by weight of the solvent, based on the weight of the solvent in the slurry, and inducing phase separation of the thermoplastic polymer from the solvent to provide the polymer matrix composite.

公开(公告)号：US11643517B2

公开(公告)日：2023-05-09

申请号：US16616157

申请日：2018-06-11

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Bharat R. Acharya ,  Derek J. Dehn ,  Fabian Stolzenburg ,  Noah O. Shanti

IPC: G10K11/165 ,  C08J9/00 ,  C08J9/28 ,  C08K3/22 ,  C08K5/01 ,  G10K11/162

CPC classification number: C08J9/0066 ,  C08J9/28 ,  C08K3/22 ,  C08K5/01 ,  G10K11/162 ,  G10K11/165 ,  C08J2201/0502 ,  C08J2201/0522 ,  C08J2325/04 ,  C08J2367/00 ,  C08J2369/00 ,  C08J2371/00 ,  C08J2375/04 ,  C08J2377/00 ,  C08K2201/005 ,  C08K2201/006

Abstract: A polymer matrix composite includes a porous polymeric network structure; and a plurality of acoustically active particles distributed within the polymeric network structure. The weight fraction of acoustically active particles is between 0.80 and 0.99, based on the total weight of the polymer matrix composite. The polymer matrix composite has an air flow resistance of less than 100 seconds/50 mL/500 μm.

公开(公告)号：US09889409B2

公开(公告)日：2018-02-13

申请号：US14585778

申请日：2014-12-30

Applicant: GWANGJU INSTITUTE OF SCIENCE AND TECHNOLOGY

Inventor： Ji-Woong Park ,  Eun-Kyung Jeon

IPC: B01D67/00 ,  C08J9/00 ,  C08J9/28 ,  B01D71/58 ,  B01D69/06 ,  B01D69/02 ,  B01D69/14 ,  B01D71/02

CPC classification number: B01D67/0079 ,  B01D69/02 ,  B01D69/06 ,  B01D69/148 ,  B01D71/024 ,  B01D71/027 ,  B01D2325/20 ,  C08J9/0066 ,  C08J9/286 ,  C08J2201/0502 ,  C08J2201/0522 ,  C08J2205/02 ,  C08J2205/042 ,  C08J2375/02

Abstract: Disclosed herein is a method of preparing a nanoporous organic-inorganic hybrid film. The method includes preparing an organic sol including a compound having amino groups, a compound having isocyanate groups, and a solvent; adding an inorganic oxide precursor to the organic sol to form a mixed solution; and subjecting the mixed solution to heat treatment to form an organic molecule network structure in which the organic sol is gelled, and an inorganic molecule network structure located along a surface of the organic molecule network structure.

公开(公告)号：US09862807B2

公开(公告)日：2018-01-09

申请号：US14507523

申请日：2014-10-06

Applicant: The Regents of the University of Michigan

Inventor： Peter X. Ma ,  Zhanpeng Zhang

IPC: C08J9/28 ,  C08J9/16

CPC classification number: C08J9/28 ,  C08J9/16 ,  C08J2201/0484 ,  C08J2201/0522 ,  C08J2205/044 ,  C08J2207/10 ,  C08J2300/206 ,  C08J2367/04

Abstract: A nanofibrous spongy microsphere includes porous walls that define an exterior of the microsphere and that extend through an interior of the microsphere. The porous walls consist of interconnected nanofibers and spaces formed between the interconnected nanofibers. A plurality of micro-scale pores are formed throughout the interior of the microsphere. Each of the micro-scale pores i) is partially defined by the porous walls, ii) has an interpore opening that opens to an adjacent micro-scale pores, and iii) has a diameter ranging from about 1 μm to about 100 μm. A total diameter of the microsphere ranges from about 5 μm to about 1000 μm.

公开(公告)号：US09567446B2

公开(公告)日：2017-02-14

申请号：US14474217

申请日：2014-09-01

Applicant: Bridgestone Corporation

Inventor： Xiaorong Wang ,  Mindaugas Rackaitis ,  Naruhiko Mashita ,  Victor Foltz

IPC: A61K9/16 ,  A61K9/50 ,  C09K9/00 ,  C09K19/00 ,  C08J9/28 ,  C09K19/54 ,  C11D17/00 ,  C08J9/36 ,  H01F1/44

CPC classification number: C08J9/28 ,  C08J9/36 ,  C08J2201/0522 ,  C08J2201/0542 ,  C08J2353/00 ,  C09K19/544 ,  C11D17/0039 ,  H01F1/44

Abstract: Micro-sized particles having a polymeric structure of cells are provided. Also provided is a method of producing micro-sized particles having a polymeric structure comprising: (1) forming a homogenous solution by heating a mixture of a high molecular weight polymer and a low molecular weight material, wherein said low molecular weight material makes up at least about 50% by weight of the homogenous solution, (2) forming a dispersed solution by dispersing the homogenous solution formed in step (1) into an inert material, (3) cooling the dispersed solution to cause the high molecular weight polymer to phase separate from the low molecular weight material, (4) forming solid particles comprised of said low molecular weight material trapped inside a structure of cells of said high molecular weight polymer, and (5) removing the solid particles from the dispersed solution.

Abstract translation: 提供具有电池聚合结构的微尺寸颗粒。 还提供了一种生产具有聚合物结构的微尺寸颗粒的方法，包括：（1）通过加热高分子量聚合物和低分子量材料的混合物形成均匀溶液，其中所述低分子量材料组成 至少约50重量％的均匀溶液，（2）通过将步骤（1）中形成的均匀溶液分散在惰性物质中形成分散溶液，（3）冷却分散溶液使高分子量聚合物相 与低分子量材料分离，（4）形成由所述低分子量材料构成的固体颗粒，所述低分子量材料被捕获在所述高分子量聚合物的细胞结构内，和（5）从分散溶液中除去固体颗粒。