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    DEHYDROGENATION PROCESS
    1.
    发明申请
    DEHYDROGENATION PROCESS 审中-公开
    脱水过程

    公开(公告)号：WO2007093533A2

    公开(公告)日：2007-08-23

    申请号：PCT/EP2007051149

    申请日：2007-02-07

    Applicant: BASF AG ,  KOTREL STEFAN ,  ERNST MARTIN

    Inventor： KOTREL STEFAN ,  ERNST MARTIN

    CPC classification number: C07B35/04 ,  C07D213/06 ,  C07D213/133

    Abstract: The present invention relates to a process for dehydrogenating compounds which can be dehydrogenated, at a temperature of 150 to 400°C, in the presence of oxygen.

    Abstract translation: 本发明涉及在氧气存在下在150-400℃的温度下使可脱氢化合物脱氢的方法。

    METHOD FOR THE HYDROGENATION OF NITRILES TO FORM PRIMARY AMINES OR AMINO NITRILES AND SUITABLE CATALYSTS FOR SAID PROCESS
    3.
    发明申请
    METHOD FOR THE HYDROGENATION OF NITRILES TO FORM PRIMARY AMINES OR AMINO NITRILES AND SUITABLE CATALYSTS FOR SAID PROCESS 审中-公开
    亚硝酸盐成伯胺或氨基腈和合适的催化剂的加氢方法

    公开(公告)号：WO2007031488A3

    公开(公告)日：2007-05-18

    申请号：PCT/EP2006066228

    申请日：2006-09-11

    Applicant: BASF AG ,  HAHN THILO ,  ERNST MARTIN ,  MELDER JOHANN-PETER

    Inventor： HAHN THILO ,  ERNST MARTIN ,  MELDER JOHANN-PETER

    IPC: C07C209/48 ,  B01J25/02 ,  C07C253/30

    CPC classification number: C07C209/48 ,  B01J25/02 ,  C07C211/12 ,  C07C253/30 ,  C07C255/24

    Abstract: The invention relates to a method for the hydrogenation of oligonitriles comprising at least two nitrile groups, in the presence of a catalyst, which is pre-treated by being brought into contact with a compound A prior to the hydrogenation process, said compound being selected from the following: alkaline metal carbonates, alkaline-earth metal carbonates, ammonium carbonate, alkaline metal hydrogencarbonates, alkaline-earth metal hydrogencarbonates, ammonium hydrogencarbonate, alkaline-earth metal oxocarbonates, alkaline metal carboxylates, alkaline-earth metal carboxylates, ammonium carboxylates, alkaline metal dihydrogen phosphates, alkaline-earth metal dihydrogen phosphates, alkaline metal hydrogen phosphates, alkaline-earth metal hydrogen phosphates, alkaline metal phosphates, alkaline-earth metal phosphates and ammonium phosphate, alkaline metal acetates, alkaline-earth metal acetates, ammonium acetate, alkaline metal formiates, alkaline-earth metal formiates, ammonium formiate, alkaline metal oxalates, alkaline-earth metal oxalates and ammonium oxalate.

    Abstract translation: 本发明涉及用于寡腈的氢化过程中，具有至少两个腈基，在催化剂的存在下通过氢化开始，它是从碱金属碳酸盐，碱土金属碳酸盐，碳酸铵，碱金属碳酸氢盐，Erdalkalimetallhydrogencarbonaten选择前，用化合物A接触预处理 ，碳酸氢铵，Erdalkalimetalloxocarbonaten，碱金属羧酸盐，碱土金属羧酸盐，羧酸铵，Alkalimetalldihydrogenphosphaten，Erdalkalimetalldihydrogenphosphaten，碱金属磷酸氢盐，Erdalkalimetallhydrogenphosphaten，lkalimetallphosphaten，碱土磷酸盐和磷酸铵，碱金属乙酸盐，碱土金属乙酸盐，乙酸铵，碱金属甲酸盐，Erdalkalimetallformiaten，甲酸铵，Alkalimetalloxalaten，Erdalkalimetalloxalaten和草酸铵。

    METHOD FOR THE HYDROGENATION OF NITRILES TO PRIMARY AMINES OR AMINONITRILES, AND CATALYSTS SUITED THEREFOR
    4.
    发明专利
    METHOD FOR THE HYDROGENATION OF NITRILES TO PRIMARY AMINES OR AMINONITRILES, AND CATALYSTS SUITED THEREFOR 未知

    公开(公告)号：CA2631124A1

    公开(公告)日：2007-06-21

    申请号：CA2631124

    申请日：2006-12-05

    Applicant: BASF AG

    Inventor： MELDER JOHANN-PETER ,  ERNST MARTIN ,  HAHN THILO

    IPC: C07C209/48 ,  B01J25/02 ,  C07C211/12

    Abstract: The invention relates to a method for hydrogenating oligonitriles containing at least two nitrile groups in the presence of a catalyst which is pre-treat ed by being contacted with a compound A prior to the hydrogenation process, sai d compound A being selected among alkali metal carbonates, alkaline earth meta l carbonates, ammonium carbonate, alkali metal hydrogen carbonates, alkaline earth metal hydrogen carbonates, ammonium hydrogen carbonate, alkaline earth metal oxocarbonates, alkali metal carboxylates, alkaline earth metal carboxylates, ammonium carboxylates, alkali metal dihydrogen phosphates, alkaline earth metal dihydrogen phosphates, alkali metal hydrogen phosphates , alkaline earth metal hydrogen phosphates, alkali metal phosphates, alkaline earth metal phosphates and ammonium phosphate, alkali metal acetates, alkali ne earth metal acetates, ammonium acetate, alkali metal formates, alkaline eart h metal formates, ammonium formate, alkali metal oxalates, alkaline earth meta l oxalates, and ammonium oxalate.

    METHOD FOR THE HYDROGENATION OF NITRILES TO FORM PRIMARY AMINES OR AMINO NITRILES AND SUITABLE CATALYSTS FOR SAID PROCESS
    5.
    发明专利
    METHOD FOR THE HYDROGENATION OF NITRILES TO FORM PRIMARY AMINES OR AMINO NITRILES AND SUITABLE CATALYSTS FOR SAID PROCESS 未知

    公开(公告)号：CA2624999A1

    公开(公告)日：2007-03-22

    申请号：CA2624999

    申请日：2006-09-11

    Applicant: BASF AG

    Inventor： ERNST MARTIN ,  MELDER JOHANN-PETER ,  HAHN THILO

    IPC: C07C209/48 ,  B01J25/02 ,  C07C253/30

    Abstract: The invention relates to a process for hydrogenating oligonitriles which have at least two nitrile groups in the presence of a catalyst which, before commencement of the hydrogenation, is pretreated by contacting with a compound A which is selected from alkali metal carbonates, alkaline earth metal carbonates, ammonium carbonate, alkali metal hydrogencarbonates, alkaline earth metal hydrogencarbonates, ammonium hydrogencarbonate, alkaline earth metal oxocarbonates, alkali metal carboxylates, alkaline earth metal carboxylates, ammonium carboxylates, alkali metal dihydrogenphosphates, alkaline earth metal dihydrogenphosphates, alkali metal hydrogenphosphates, alkaline earth metal hydrogenphosphates, alkali metal phosphates, alkaline earth metal phosphates and ammonium phosphate, alkali metal acetates, alkaline earth metal acetates, ammonium acetate, alkali metal formiates, alkaline earth metal formiates, ammonium formiate, alkali metal oxalates, alkaline earth metal oxalates and ammonium oxalate.

    7.
    发明专利
    未知

    公开(公告)号：DE102005052457A1

    公开(公告)日：2007-05-10

    申请号：DE102005052457

    申请日：2005-11-03

    Applicant: BASF AG

    Inventor： ERNST MARTIN ,  OEHLENSCHLAEGER STEFFEN ,  KUHNKE FRANK ,  ROS KARL-HEINZ ,  DEEG ROLAND ,  MELDER JOHANN-PETER

    IPC: C07C211/11 ,  C07C209/48

    Abstract: The present invention relates to a process for the industrial preparation of a diamine starting from a corresponding alkenyl nitrile comprising at least one C—C double bond, which comprises the steps (a) reaction of the alkenyl nitrile with a corresponding monoamine in a first reactor so that the monoamine adds exothermically onto the at least one double bond to form an aminoalkyl nitrile, with the monoamine and water being charged initially and the alkenyl nitrile being fed in; (b) evaporation of unreacted alkenyl nitrile and monoamine to increase the concentration of the aminoalkyl nitrile product in the bottoms of the first reactor; (c) transfer of the aminoalkyl nitrile bottom product from step (b) to a second reactor; (d) batchwise catalytic hydrogenation of the aminoalkyl nitrile transferred in step (c) to the diamine in the second reactor, with each batch being obtained by initially charging a catalyst suitable for the hydrogenation of nitriles to amines and also water, the desired diamine and a base, introducing hydrogen into the second reactor and feeding in the aminoalkyl nitrile transferred in step (c); and (e) isolation of the diamine and, if appropriate, repetition of the steps (a) to (e). The invention further relates to an apparatus for preparing these diamines and the use of the apparatuses. A preferred diamine is 3-dimethylaminopropylamine (DMAPA).

    Hydrogenation of oligonitrile with at least two nitrile groups, in the presence of a catalyst, which is pre-treated by contacting with a compound e.g. alkali metal carbonates and ammonium carbonate
    10.
    发明专利
    Hydrogenation of oligonitrile with at least two nitrile groups, in the presence of a catalyst, which is pre-treated by contacting with a compound e.g. alkali metal carbonates and ammonium carbonate 未知

    公开(公告)号：DE102005057198A1

    公开(公告)日：2007-06-06

    申请号：DE102005057198

    申请日：2005-11-29

    Applicant: BASF AG

    Inventor： ERNST MARTIN ,  HAHN THILO ,  MELDER JOHANN-PETER

    IPC: C07C209/48 ,  B01J23/00 ,  C07B43/04

    Abstract: Hydrogenation of oligonitrile with at least two nitrile groups in the presence of a catalyst, which is pre-treated by contacting with a compound A, before the hydrogenation process; where the compound A is e.g. alkaline metal carbonates, alkaline-earth metal carbonates, ammonium carbonate, alkaline metal hydrogencarbonate, alkaline-earth metal hydrogencarbonate, ammonium hydrogencarbonate and alkaline-earth metal oxycarbonate. Hydrogenation of oligonitrile with at least two nitrile groups in the presence of a catalyst, which is pre-treated by contacting with a compound A, before the hydrogenation process; where the compound A is alkaline metal carbonates, alkaline-earth metal carbonates, ammonium carbonate, alkaline metal hydrogencarbonate, alkaline-earth metal hydrogencarbonate, ammonium hydrogencarbonate, alkaline-earth metal oxycarbonate, alkaline metal carboxylate, alkaline-earth metal carboxylate, ammonium carboxylate, alkaline metal dihydrogen phosphate, alkaline-earth metal dihydrogen phosphates, alkaline metal hydrogen phosphates, alkaline-earth metal hydrogen phosphates, alkaline metal phosphates, alkaline-earth metal phosphates, ammonium phosphate, alkaline metal acetates, alkaline-earth metal acetates, ammonium acetate, alkaline metal formate, alkaline-earth metal formate, ammonium formate, alkaline metal oxalates, alkaline-earth metal oxalates or ammonium oxalate. Independent claims are also included for: (1) an oligo amine or amino nitrile, obtained from an oligo nitrile; (2) a catalyst comprising a metal from group VIII to X, which are pretreated with the compound A, where the cobalt or nickel catalyst is pre-treated with compound A excluding alkali metal carbonate or alkali metal hydrogen carbonate; and (3) a method for preparing the catalyst comprising treating a metal form group VIII to X with the compound.

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