公开(公告)号：WO2007071626A2

公开(公告)日：2007-06-28

申请号：PCT/EP2006069777

申请日：2006-12-15

Applicant: BASF AG ,  ERNST MARTIN ,  KUSCHE ANDREAS ,  HEYDRICH GUNNAR ,  GRAFMANS HORST ,  EVERS HOLGER ,  MELDER JOHANN-PETER ,  MEISSNER HARALD ,  FREUND TORSTEN

Inventor： ERNST MARTIN ,  KUSCHE ANDREAS ,  HEYDRICH GUNNAR ,  GRAFMANS HORST ,  EVERS HOLGER ,  MELDER JOHANN-PETER ,  MEISSNER HARALD ,  FREUND TORSTEN

IPC: C07C231/12 ,  C07C237/06

CPC classification number: C07C231/14 ,  Y02P20/582 ,  C07C237/06

Abstract: The invention relates to a method for producing aminoalkane acid amines by reacting cyanoalkane acid esters with a) ammonia or an amine and b) hydrogen in the presence of a catalyst, the reaction with component b) being started simultaneously or a maximum of 100 minutes after starting to react the cyanoalkane acid ester with component a).

Abstract translation: 本发明涉及一种用于Aminoalkansäureamiden的制备方法通过用）氨或胺Cyanalkansäureestern反应，和b）在催化剂的存在下，氢气其中Cyanalkansäureesters的执行开始后在同一时间与组分b）的反应或不晚于最大100分钟 从组件a）开始。

公开(公告)号：DE102004058887A1

公开(公告)日：2006-06-08

申请号：DE102004058887

申请日：2004-12-06

Applicant: BASF AG

Inventor： GRAFMANS HORST ,  MAAS STEFFEN ,  WECK ALEXANDER ,  RUETTER HEINZ ,  SCHULZ MICHAEL ,  ROS KARL-HEINZ

IPC: C07C231/02 ,  C07C233/05

Abstract: A process for preparing N,N-dimethylacetamide (DMAC) by continuously reacting methyl acetate (MeOAc) with dimethylamine (DMA) in the presence of a basic catalyst, wherein MeOAc is used in the form of a methanolic solution and in the range from 0.0002 to 0.09 mol of catalyst per mole of MeOAc, and performing the reaction at a temperature in the range from 90 to 140° C. and at an absolute pressure in the range from 10 to 30 bar.

公开(公告)号：DE102004058886A1

公开(公告)日：2006-06-08

申请号：DE102004058886

申请日：2004-12-06

Applicant: BASF AG

Inventor： GRAFMANS HORST ,  MAAS STEFFEN ,  WECK ALEXANDER ,  RUETTER HEINZ ,  SCHULZ MICHAEL ,  ROS KARL-HEINZ

IPC: C07C231/02 ,  C07C233/05

Abstract: A process for preparing N,N-dimethylacetamide (DMAC) by continuously reacting methyl acetate (MeOAc) with dimethylamine (DMA) in the presence of a basic catalyst, wherein MeOAc is used in the form of a methanolic solution which is obtained as a by-product in the preparation of polyTHF by transesterifying polyTHF diacetate with methanol.

公开(公告)号：DE102005060803A1

公开(公告)日：2007-06-28

申请号：DE102005060803

申请日：2005-12-20

Applicant: BASF AG

Inventor： ERNST MARTIN ,  KUSCHE ANDREAS ,  HEYDRICH GUNNAR ,  GRAFMANS HORST ,  EVERS HOLGER ,  MELDER JOHANN-PETER ,  MEISNER HARALD ,  FREUND TORSTEN

IPC: C07C231/06

Abstract: Preparation of aminoalkanoic acid amide comprises reaction of cyanoalkanoic acid ester with (a) at least a mol-equivalent of ammonia or amine, and (b) hydrogen in the presence of catalyst, at increased pressure, where optionally the formed intermediate stages are not isolated and the reaction with (b) takes place simultaneously or less than 100 minutes, after the beginning of the reaction of cyanoalkanoic acid ester with (a).

公开(公告)号：DE102004058888A1

公开(公告)日：2006-06-08

申请号：DE102004058888

申请日：2004-12-06

Applicant: BASF AG

Inventor： GRAFMANS HORST ,  MAAS STEFFEN ,  WECK ALEXANDER ,  RUETTER HEINZ ,  SCHULZ MICHAEL ,  ROS KARL-HEINZ

IPC: C07C231/02 ,  C07C233/05