METHOD FOR SEPARATING TRIETHANOLAMIN FROM A MIXTURE OBTAINABLE BY AMMONIA AND ETHYLENE OXIDE REACTION
    2.
    发明申请
    METHOD FOR SEPARATING TRIETHANOLAMIN FROM A MIXTURE OBTAINABLE BY AMMONIA AND ETHYLENE OXIDE REACTION 审中-公开
    方法用于分离三乙醇胺从THROUGH氨氧化乙烯燃混合物的实现

    公开(公告)号:WO2005035481A3

    公开(公告)日:2005-06-02

    申请号:PCT/EP2004011022

    申请日:2004-10-02

    CPC classification number: C07C213/10 C07C215/12

    Abstract: The invention relates to a method for distillative separation of triethanolamin from a substance mixture consisting of mono- di-, and triethanolamin, ethanolamin-ether and water obtainable by an ammonia and ethylene oxide reaction in a liquid phase at a high pressure and temperature consisting in distilling the substance mixture in two stages. In the first stage, a low-boiling fraction and a high-boiling fraction are withdrawn and discharged, and in the second stage, a medium-boiling fractions is distilled at a triethanolamin content >99.4 % by weight and a diethanolamin content

    Abstract translation: 一种用于三乙醇胺的从图像在压力下,并在一,二和三乙醇胺的升高的温度下混合,以及乙醇胺醚和水,通过氨与环氧乙烷在液相中反应而获得的连续蒸馏分离工艺,其中在两个阶段中蒸馏该混合物 是。 在第一阶段中的低沸点馏分和高沸点馏分被取出和排出并在第二阶段中,中间沸点馏分蒸馏具有<0.2重量%的> 99.4重量%三乙醇胺的含量和二乙醇胺。 该混合物的蒸馏在第一列中优选进行和相互连接该第二塔或间壁塔。

    6.
    发明专利
    未知

    公开(公告)号:DE50003718D1

    公开(公告)日:2003-10-23

    申请号:DE50003718

    申请日:2000-01-20

    Applicant: BASF AG

    Abstract: A process for working up at least partially deactivated polymerization catalysts for the polymerization or copolymerization of THF which are contaminated with the products of the polymerization or copolymerization of THF comprises(a) in a first step, cleaning the polymerization catalyst by treatment with steam at from 80 to 250° C. and a pressure of from 0.5 to 40 bar and, preferably,(b) in a second step, regenerating the clean polymerization catalyst.

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