(n-(2-aminoethyl)) piperazine prepn - from ethanolamine and ammonia

    公开(公告)号:DE2230735A1

    公开(公告)日:1974-01-03

    申请号:DE2230735

    申请日:1972-06-23

    Applicant: BASF AG

    Abstract: Ethanolamine and NH3 are reacted in a known manner, in presence of H2 and a hydrogenation catalyst at elevated temp. and press. and the ethylene diamine main prod., unreacted starting materials and opt other prods are distilled off; the distn. residue is then reacted with NH3 and H2 in presence of a hydrogenation catalyst and opt. water to give piperazine and/or N-(2-aminoethyl) piperazine (I). Valuable prods. are thus obtd. from the previously useless distn. residue.

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