MASS SPECTROMETER
    131.
    发明申请
    MASS SPECTROMETER 有权
    质谱仪

    公开(公告)号:US20100176293A1

    公开(公告)日:2010-07-15

    申请号:US12376542

    申请日:2007-07-27

    CPC classification number: H01J49/08 H01J49/147 H01J49/16

    Abstract: A cathode configuration for emission of electrons has a reaction zone connected to an entrance opening for the supply of neutral particles. The opening communicates with the cathode configuration for the ionization of the neutral particles and an ion extraction system communicates with the reaction zone. Ions from the extraction system are sent to a detection system and a mechanism for the evacuation of the mass spectrometer arrangement. The cathode configuration includes a field emission cathode with an emitter surface, wherein at a short distance from this emitter surface, an extraction grid is disposed for the extraction of electrons, which grid substantially covers the emitter surface. The emitter surface encompasses herein at least partially a hollow volume such that a tubular structure is formed.

    Abstract translation: 用于发射电子的阴极配置具有连接到用于供应中性粒子的入口的反应区。 开口与阴极结构连通,用于中性粒子的电离,离子提取系统与反应区连通。 来自提取系统的离子被发送到检测系统和用于疏散质谱仪装置的机构。 阴极配置包括具有发射极表面的场致发射阴极,其中在离该发射体表面短的距离处,设置用于提取电子的提取栅格,栅格基本上覆盖发射器表面。 发射器表面在此包括至少部分为中空体积,从而形成管状结构。

    MINIATURIZED NON-RADIOACTIVE ELECTRON EMITTER
    132.
    发明申请
    MINIATURIZED NON-RADIOACTIVE ELECTRON EMITTER 审中-公开
    微型非放射性电子发射器

    公开(公告)号:US20100006751A1

    公开(公告)日:2010-01-14

    申请号:US12423182

    申请日:2009-04-14

    Abstract: A novel, compact non-radioactive electron emitter is provided with a cylindrical shape and with an interior space (6), which forms a vacuum chamber. A substrate (7) forms the bottom of the arrangement with a plurality of field emitter tips (5) formed of carbon nanotubes in the interior space (6). The tips are fastened to the substrate. A layer structure forms the cover of the arrangement, having, from the outside towards the interior space (6), an electrode layer (13), which acts as a counterelectrode and is applied to a gas-impermeable and electron-permeable membrane (10). A substrate (11), which is left open in the form of a window (12) in the area above the field emitter tips (6), acts as a carrier substrate for the membrane (10) and the electrode layer (13). A circumferential wall (14) of the arrangement is formed by an electrically insulating material. The field emitter tips (5) and the electrode layer (13) are connected to a d.c. power source, so that the electrons exiting from the field emitter tips (5) are accelerated through the vacuum chamber, window (12) and the membrane (10) towards the electrode layer (13), pass through the electrode layer (13) and enter the ionization area (3) outside the electron emitter (1, 1′).

    Abstract translation: 一种新颖紧凑的非放射性电子发射器设置有圆柱形形状并具有形成真空室的内部空间(6)。 衬底(7)在所述内部空间(6)中形成由碳纳米管形成的多个场发射器尖端(5)构成所述装置的底部。 尖端固定在基底上。 层结构形成了从外部到内部空间(6)的布置的盖,电极层(13),其用作反电极并被施加到气体不可渗透和电渗透膜(10 )。 在场发射器尖端(6)上方的区域中以窗口(12)的形式打开的衬底(11)用作膜(10)和电极层(13)的载体衬底。 该装置的圆周壁(14)由电绝缘材料形成。 场发射器尖端(5)和电极层(13)连接到直流 电源,使得从场发射器尖端(5)出射的电子通过真空室,窗口(12)和膜(10)朝向电极层(13)加速,穿过电极层(13)和 进入电子发射器(1,1')外的电离区域(3)。

    Electron gun assembly
    133.
    发明申请
    Electron gun assembly 有权
    电子枪组装

    公开(公告)号:US20080023642A1

    公开(公告)日:2008-01-31

    申请号:US11495628

    申请日:2006-07-31

    Abstract: A device which employs an electron beam, for performing a desired function, includes an electron gun for generating the electron beam. The electron gun includes a barrel shaped rotatable structure having a plurality of annularly disposed electron sources. A curvature of a surface portion of the rotatable structure is shaped to optimize electric field concentrations. The rotatable structure further includes end portion protrusions.

    Abstract translation: 使用电子束来执行所需功能的装置包括用于产生电子束的电子枪。 电子枪包括具有多个环形设置的电子源的桶形可旋转结构。 可旋转结构的表面部分的曲率被成形为优化电场浓度。 可旋转结构还包括端部突起。

    Electron source for ionization with leakage current suppression
    134.
    发明申请
    Electron source for ionization with leakage current suppression 失效
    具有泄漏电流抑制的电离源

    公开(公告)号:US20070132357A1

    公开(公告)日:2007-06-14

    申请号:US11301588

    申请日:2005-12-13

    CPC classification number: H01J49/14 H01J3/024 H01J49/08

    Abstract: An electron source includes a first electrode, a second electrode, a thermionic element interposed between and electrically isolated from the first electrode and the second electrode, and a guard electrode interposed between and electrically isolated from the first electrode and the second electrode. The thermionic element and the guard electrode may be at substantially the same voltage. Another electron source includes a first electrode, a second electrode, a thermionic element interposed between and electrically isolated from the first electrode and the second electrode, and a thermal expansion component interposed between and electrically isolated from the first electrode and the second electrode. The thermal expansion component may be heated to cause expansion. The heating may be cycled to cause alternating expansion and contraction.

    Abstract translation: 电子源包括插入在第一电极和第二电极之间并且与第一电极和第二电极电绝缘的第一电极,第二电极和热电离元件,以及插入在第一电极和第二电极之间并与之电隔离的保护电极。 热电离元件和保护电极可以处于基本上相同的电压。 另一电子源包括介于第一电极和第二电极之间并与之电隔离的第一电极,第二电极和热电离元件,以及介于第一电极和第二电极之间并与之电隔离的热膨胀组件。 热膨胀部件可能被加热以引起膨胀。 可以循环加热以引起交替的膨胀和收缩。

    Apparatus and method for elemental mass spectrometry
    135.
    发明申请
    Apparatus and method for elemental mass spectrometry 有权
    元素质谱仪的装置及方法

    公开(公告)号:US20050199795A1

    公开(公告)日:2005-09-15

    申请号:US10489215

    申请日:2004-03-09

    CPC classification number: H01J49/08

    Abstract: A mass spectrometer and method of mass spectrometry in which polyatomic and doubly charged ion interferences are attenuated by establishing an electron population through which a beam of particles containing elemental sample ions and the interfering ions is passed such that the interfering ions preferentially undergo ion-electron recombination and thus dissociation to remove a significant number of the interfering ions. Means (30 or 32) for providing a population of electrons (34 or 36) in an ICP-MS (22) may comprise a magnetic field means such as an electric coil, or an electron generating device. The population of electrons has an electron number density (>1011 cm−3 to 1014 cm−3), a free electron energy (>0.01 eV to

    Abstract translation: 通过建立电子群减少多原子和双电荷离子干扰的质谱仪和质谱法,通过该质谱仪将含有元素样品离子和干扰离子的粒子束通过,使得干扰离子优先进行离子电子重组 并因此解离以除去大量的干扰离子。 用于在ICP-MS(22)中提供电子群体(34或36)的装置(30或32)可以包括诸如电线圈或电子产生装置的磁场装置。 电子群体具有电子数密度(> 10×10 -3 cm -3至10 14 cm -3 -3 / ),在低压(<10Torr)的区域中的自由电子能量(> 0.01eV至<5eV),使得通过电子群体的离子的预定路径长度(1-4cm), 干扰离子将优先通过解离复合过程减弱。 离子束(40)然后通过质量分析器(42),并且通过离子检测器(44)检测已经根据其质荷比分离的离子。

    Miniature quadrupole mass spectrometer having a cold cathode ionization source
    136.
    发明授权
    Miniature quadrupole mass spectrometer having a cold cathode ionization source 有权
    具有冷阴极电离源的微型四极杆质谱仪

    公开(公告)号:US06452167B1

    公开(公告)日:2002-09-17

    申请号:US09315001

    申请日:1999-05-19

    Inventor: Thomas E. Felter

    Abstract: An improved quadrupole mass spectrometer is described. The improvement lies in the substitution of the conventional hot filament electron source with a cold cathode field emitter array which in turn allows operating a small QMS at much high internal pressures then are currently achievable. By eliminating of the hot filament such problems as thermally “cracking” delicate analyte molecules, outgassing a “hot” filament, high power requirements, filament contamination by outgas species, and spurious em fields are avoid all together. In addition, the ability of produce FEAs using well-known and well developed photolithographic techniques, permits building a QMS having multiple redundancies of the ionization source at very low additional cost.

    Abstract translation: 描述了改进的四极质谱仪。 改进之处在于用冷阴极场发射体阵列代替传统的热丝电子源,该冷阴极场发射器阵列又允许在很高的内部压力下操作小的QMS,然后目前是可实现的。 通过消除热丝,诸如热“裂解”精细的分析物分子,排除“热”丝,高功率需求,排气物质的细丝污染和杂散电场等问题都避免在一起。 此外,使用已知和发展良好的光刻技术制造FEA的能力允许以非常低的附加成本构建具有多个电离源冗余的QMS。

    Secondary electron spectrometer for measuring voltages on a sample
utilizing an electron probe
    137.
    发明授权
    Secondary electron spectrometer for measuring voltages on a sample utilizing an electron probe 失效
    二次电子光谱仪,用于使用电子探针测量样品上的电压

    公开(公告)号:US4514682A

    公开(公告)日:1985-04-30

    申请号:US398542

    申请日:1982-07-15

    CPC classification number: H01J49/08 H01J49/44

    Abstract: An improved secondary electron spectrometer for measuring voltages occurring on a specimen, such as an integrated circuit chip, utilizing an electron probe has a grating structure for measuring the energy distribution of the secondary electrons independently of the angular distribution of the secondary electrons at the measuring point on the specimen. If the secondary electron spectrometer has an extraction electrode and a deceleration electrode, the grating structure is spherically symmetric.

    Abstract translation: 用于测量在诸如集成电路芯片的样本上发生的电压的改进的二次电子光谱仪利用电子探针具有用于独立于测量点处的二次电子的角分布来测量二次电子的能量分布的光栅结构 在标本上。 如果二次电子光谱仪具有提取电极和减速电极,则光栅结构是球形对称的。

    Axial beam time of flight mass spectrometer
    138.
    发明授权
    Axial beam time of flight mass spectrometer 失效
    飞行质谱仪的轴向时间

    公开(公告)号:US3586853A

    公开(公告)日:1971-06-22

    申请号:US3586853D

    申请日:1968-11-14

    Inventor: VESTAL MARVIN L

    CPC classification number: H01J49/147 H01J49/08 H01J49/40

    Abstract: A time of flight mass spectrometer wherein the ionizing electron beam is in axial alignment with the path of the ions produced thereby and wherein an electron multiplier is utilized to generate a high intensity electron beam for ionization. An open mesh control grid is utilized to control the axial dimension of the ionization region so that it can be maintained very small in order that the distance traveled by each of the ions to an ion detector at the opposite end of a drift tube is very nearly the same. This will result in a more accurate measurement of the mass of the ions since the difference in travel time to reception by the ion detector will be primarily because of difference in mass alone and not because of a difference in the distance traveled.

    절대연대측정법을 이용한 고대 토기 및 도자기의 진위감정 방법 및 시스템
    139.
    发明授权
    절대연대측정법을 이용한 고대 토기 및 도자기의 진위감정 방법 및 시스템 有权
    古陶陶器真伪鉴定方法与体系的绝对年代测定方法

    公开(公告)号:KR101722692B1

    公开(公告)日:2017-04-03

    申请号:KR1020160145068

    申请日:2016-11-02

    Applicant: 김명진

    Inventor: 김명진

    CPC classification number: G01N23/225 H01J49/08

    Abstract: 본발명은절대연대측정법을이용한고대토기및 도자기의진위감정방법및 시스템에관한것이다. 본발명의제 1 측면은, 절대연대측정법을이용한고대토기및 도자기의진위감정방법은, 일체형 TL/OSL 측정장비(1)의 TL/OSL 신호측정부(400)이고대토기및 도자기로부터추출된코아시료로만든시료디스크(2) 중하나를대상으로 TL/OSL 연대측정을수행하는제 1 단계; 일체형 TL/OSL 측정장비(1)의알파되튐흔적측정부(500)가고대토기및 도자기로부터추출된코아시료의알파되튐흔적연대측정을수행하는제 2 단계; 및일체형 TL/OSL 측정장비(1)의제어부(600)는제어프로그램모듈(600a)을통해측정된 TL/OSL 연대(Age)와측정된알파되튐흔적연대(Age)의비교를통한진품여부를분석하는제 3 단계; 를포함하는절대연대측정법을이용한고대토기및 도자기의진위감정방법을제공함에있다. 본발명의제 2 측면은, 일체형 TL(thermoluminescence)/OSL(optically stimulated luminescence) 측정장비(1)와하나의시료디스크(2)를포함하는절대연대측정법을이용한고대토기및 도자기의진위감정시스템에있어서, 일체형 TL/OSL 측정장비(1)는, 고대토기및 도자기로부터추출된코아시료로만든시료디스크(2) 중하나를대상으로 TL/OSL 연대측정을수행하는 TL/OSL 신호측정부(400); 고대토기및 도자기로부터추출된코아시료의알파되튐흔적연대측정을수행하는알파되튐흔적측정부(500); 및제어프로그램모듈(600a)을통해측정된 TL/OSL 연대(Age)와측정된알파되튐흔적연대(Age)의비교를통한위조품여부를분석하는제어부(600); 를포함하는절대연대측정법을이용한고대토기및 도자기의진위감정시스템을제공함에있다. 이에의해, 고대토기및 도자기의보존환경에대한자세한정보를확인할수 없는경우에도연대측정의신뢰도를향상시킬수 있는효과를제공한다. 또한, 모조품을제작한후 진품과동일한고고선량이나오도록인위적인방사선조사가수행된경우에도진품인지모조품인지를구별할수 있는효과를제공한다. 뿐만아니라, 종래의 TL/OSL 연대측정법을적용할경우연대측정에사용되는시료의양이많이요구되는한계점을극복하여적은시료만으로도토기및 도자기에대한정확한제작연대산출및 진위감정이가능한효과를제공한다.

    Abstract translation: 本发明涉及一种使用绝对年代测定古陶器和陶瓷真伪性的方法和系统。 本发明的第一个方面,所述真实性感觉古陶器和绝对约会瓷的方法是集成测量装置的TL / OSL TL / OSL信号测量单元400(1)从大陶器和瓷器提取 对由芯样品制成的样品盘2之一进行TL / OSL老化测量的第一步骤; 去阿尔法弹跳跟踪测量集成TL的部分500 / OSL测量设备(1)执行阿尔法弹跳的第二步骤迹线从陶瓷中提取的核心样本的约会; 并通过比较积分TL / OSL测量设备的真实性(1)议程渔夫600具有控制程序模块(600A),则TL / OSL年龄(年龄),和α弹跳线索年龄(年龄)测定通过将测量 分析的第三步; 本发明还提供了一种使用绝对年龄测量方法鉴定古陶器和陶器的方法。 本发明的第二方面是一单件TL(热释)/ OSL(光释光)测量设备(1)古陶瓷真实性情绪系统具有绝对的约会到瓦哈包括我的试样盘2 集成TL / OSL测量设备(1)中,用从古代陶瓷样品盘(2)TL / OSL信号测量单元400中提取用于执行TL / OSL约会靶向我重载用芯样品进行; 一种阿尔法钟轨迹测量单元500,用于对从古代陶器和陶瓷中提取的岩心样品进行α贝尔痕迹老化; 和控制程序模块,所述TL / OSL年龄控制器600分析是否伪造通过比较通过(600A)测定的(年龄)α和弹跳线索年龄(年龄)测量; 并运用绝对年龄测年法提供古陶器和陶器的真实情感体系。 因此,即使关于古陶器和陶瓷的保存环境的详细信息不能得到确认,也可以提高测年的可靠性。 此外,使得模仿后提供了可以假冒区分的效果是否,即使相同的剂量或考古文物,使得辐射与真正真实性进行。 此外,在施加常规TL时/ OSL约会提供陶器和瓷器,只有小样本精确制造年龄计算和真实性情感可能产生的影响,以克服需要大量样品的用于约会的量的限制 的。

    자외선 다이오드와 CEM을 이용한 질량분석기의 이온화원 획득장치
    140.
    发明公开
    자외선 다이오드와 CEM을 이용한 질량분석기의 이온화원 획득장치 有权
    使用UV LED和CEM获取大量光谱的离子源的装置

    公开(公告)号:KR1020130031181A

    公开(公告)日:2013-03-28

    申请号:KR1020110136092

    申请日:2011-12-16

    CPC classification number: H01J49/10 H01J49/0022 H01J49/08 H01J49/424

    Abstract: PURPOSE: An ionization source securing device of a mass spectrometer using a UV diode and a CEM is provided to secure the bulk of amplified electron beams by inducing the discharging of initial electrons through irradiating UV photons to the entrance of a CEM module. CONSTITUTION: An UV diode(110) emits an ultraviolet ray. A CEM(Channeltron Electron Multiplier) module(120) induces and amplifies the discharging of initial electrons and secures the bulk of electron beams at an exit(122). An electron integrating lens integrates an amplified electronic beam. An ion trap mass separator ionizes gas sample molecules with an injected electron beam. An ion detector detects an ion separated from an ion trap mass separator with a mass spectrum. The CEM module respectively applies negative voltage to a CEM module entrance(121) and a CEM module exit. The CEM module insulates using first and second insulators(123,124).

    Abstract translation: 目的:提供使用UV二极管和CEM的质谱仪的电离源固定装置,以通过将UV光子照射到CEM模块的入口来引起初始电子的放电来固定大部分放大的电子束。 构成:UV二极管(110)发射紫外线。 CEM(通道电子倍增器)模块(120)引发和放大初始电子的放电并且在出口处固定大部分电子束(122)。 电子积分透镜集成放大电子束。 离子阱质量分离器用注入的电子束离子化气体样品分子。 离子检测器利用质谱检测离子阱质量分离器分离的离子。 CEM模块分别向CEM模块入口(121)和CEM模块出口施加负电压。 CEM模块使用第一和第二绝缘体(123,124)进行绝缘。

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