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公开(公告)号：KR101225448B1
公开(公告)日：2013-01-24
申请号：KR1020120099051
申请日：2012-09-07
Applicant: 재단법인나주시천연염색문화재단
CPC classification number: C09B7/00 , C09B61/00 , C09B67/0002 , C09B67/0003
Abstract: PURPOSE: An indigo composition is provided to be harmful for human body, to have high fastness when dyeing, to be used in dyeing without indigo pre-treatment and to have excellent dyeing effect. CONSTITUTION: A manufacturing method of an indigo composition comprises: a step of extracting polygonum indigo by hot water, pulverizing the extract condensation, freeze-drying and crushing the extract to manufacture an indican powder; a step of polygonum leaf in the shade and pulverizing the polygonum leaf to manufacture polygonum powder; a step of drying and pulverizing a gall tannin and glucose powder; a step of storing the mixture of the indican powder, the polygonum powder and the mixture of the gall tannin and glucose powder at room temperature; and a step of adding water to the mixture and oxidizing the mixture. [Reference numerals] (AA) Process; (BB) Harvesting polygonum trinctorium leaves; (CC) Extracting; (DD) Evaporating and powder storing; (EE) Storing; (FF) Indican+dried polygonum trinctorium leaf powder+glucose; (GG) Adding water; (HH) Indoxyl; (II) Hairdye and paint; (JJ) Oxidization; (KK) Indigo; (LL) Contents; (MM) Fresh polygonum trinctorium leaves contain indican and indican hydrolase; (NN) Inactivating the indican hydrolase by hot water-extracting at 80-100°C; (OO) Freeze-drying using a decompression evaporator and pulverizing(1,800-2,000 mesh); (PP) Sealing and storing at room temperature(storing thickened products at 1-5°C); (QQ) Sealing and storing after the moisture content of the indican+the dried polygonum trinctorium leaf powder+the glucose powder+nutgall tannin becomes 3% or less; (RR) Adding water to decompose inactivated indican with the hydrolase such that the moisture content of a composition become in 70-80%; (SS) Generating indoxyl and glucose by hydrolyzing the indican with the hydrolase; (TT) Using the indoxyl as paint or hairdye; (UU) Oxidizing in the air; (VV) Oxidizing the indoxyl to become blue and insoluble
Abstract translation: 目的：提供对人体有害的靛蓝组合物，染色时具有高坚牢度，用于无靛蓝预处理的染色中，具有优异的染色效果。 构成：靛蓝组合物的制造方法包括：通过热水提取ind靛的步骤，粉碎提取物的冷凝，冷冻干燥并粉碎提取物以制造指甲粉; 在树荫下一步um叶，粉碎um叶以制造um粉; 干燥并粉碎胆汁单宁和葡萄糖粉末的步骤; 在室温下储存指示剂粉末，um粉和胆汁单宁和葡萄糖粉末的混合物的混合物的步骤; 以及向混合物中加入水并氧化混合物的步骤。 （附图标记）（AA）工艺; （BB）收获um ium叶; （CC）提取; （DD）蒸发和粉末储存; （EE）存储; （FF）Indican +干um叶粉+葡萄糖; （GG）加水; （HH）吲哚基; （二）头发和油漆; （JJ）氧化; （KK）靛蓝; （LL）内容; （MM）新鲜um叶含有an an和indic an水解酶; （NN）在80-100℃下通过热水提取来灭活印度水解酶; （OO）使用减压蒸发器冷冻干燥并粉碎（1,800-2,000目）; （PP）室温密封保存（1-5℃保存加厚产品）; （QQ）标记水分含量+干燥um叶粉+葡萄糖+甘草单宁后的密封保存量为3％以下; （RR）加水分解水解酶的灭活指示剂，使组合物的水分含量达到70-80％; （SS）通过用水解酶水解标记产生吲哚和葡萄糖; （TT）使用indoxyl作为油漆或发丝; （UU）在空气中氧化; （VV）氧化吲哚氧基成蓝色和不溶
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Patent Agency Ranking
公开(公告)号：KR101134910B1
公开(公告)日：2012-04-17
申请号：KR1020110090561
申请日：2011-09-07
Applicant: 재단법인나주시천연염색문화재단
IPC: C09B61/00
CPC classification number: C09B7/00 , C09B61/00 , C09B67/0002
Abstract: PURPOSE: A manufacturing method of indigo powder is provided to reduce the color separation time of indigo comparison with the existing method, and prevent the generation of strain because of high content of indigo colorant. CONSTITUTION: A manufacturing method of indigo powder comprises: a step of adding water into indigo, crushing the indigo to the size of 1-3 cm, and separating extract by squeezing the indigo to make the moisture content of 6-8%(v/w); a step of filtering the extract; a step of supplying oxygen to make the dissolved oxygen of 30-50 ppm, or oxidizing the indigo extract by adding 3-7% of hydrogen peroxide based on the volume of the indigo extract; a step of separating indigo colorant by centrifuging or precipitating the oxidized extract; and a step of drying the indigo colorant, and crushing the dried colorant.
Abstract translation: 目的：提供靛蓝粉末的制造方法，以减少靛蓝与现有方法的颜色分离时间，并防止由于靛蓝着色剂含量高而产生应变。 构成：靛蓝粉末的制造方法包括：向靛蓝中加入水，将靛蓝粉碎至1-3cm的步骤，通过挤压靛蓝分离提取物，使含水量为6-8％（v / W）; 过滤提取物的步骤; 提供氧气以使溶解氧为30-50ppm的步骤，或通过以靛蓝提取物的体积加入3-7％的过氧化氢来氧化靛蓝提取物; 通过离心或沉淀氧化提取物分离靛蓝着色剂的步骤; 以及干燥靛蓝着色剂并粉碎干燥着色剂的步骤。
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公开(公告)号：KR101912655B1
公开(公告)日：2018-10-30
申请号：KR1020170081422
申请日：2017-06-27
Applicant: 재단법인나주시천연염색문화재단
CPC classification number: D06P1/34 , D06P5/2077
Abstract: 본발명은천연염색방법에관한것으로, 더욱상세하게는염색성및 견뢰도가향상된 '저온감압농축방법을이용한무환자나무활용천연염색방법'에관한것이다.이러한본 발명은,무환자나무에서염료를추출하는무환자나무염료추출단계와; 피염물을무환자나무염료를녹인무환자나무염액에침적하고, 동시매염을수행하는피염물침적단계와; 침적한피염물을수세하는피염물수세단계와; 수세한피염물을열처리하는피염물열처리단계및; 열처리한피염물을건조하는피염물건조단계를포함하는것을특징으로한다.
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公开(公告)号：KR101799042B1
公开(公告)日：2017-11-20
申请号：KR1020160050539
申请日：2016-04-26
Applicant: 재단법인나주시천연염색문화재단
Abstract: 본발명은부레풀을이용하여천연염색, 특히황토염색과락 염색의견뢰도를향상시키는방법에관한것으로서, 본발명에따른방법에의하면, 견뢰도향상용으로만들어진화학물질을사용하지않고천연염색의견뢰도를향상시킬수 있어천연염색의의미를살릴수 있으며, 천연염색된직물의상품성을높일수 있다.
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公开(公告)号：KR1020120107754A
公开(公告)日：2012-10-04
申请号：KR1020110025466
申请日：2011-03-22
Applicant: 재단법인나주시천연염색문화재단
CPC classification number: C11D9/38 , A61K8/97 , A61K2800/74 , A61K2800/805 , A61Q19/02 , A61Q19/10 , C11D3/48 , C11D13/10
Abstract: PURPOSE: A manufacturing method of indigofera tinctoria extract is provided to maximize antibiotic, anti-inflammation and anti-whitening effects by controlling extraction solvent, extracting temperature, and extracting time. CONSTITUTION: A manufacturing method of indigofera tinctoria extract comprises a step of adding ethanol to indigofera tinctoria and extracting the added mixture at 25-30 °C for 11-15 hours. The added amount of the indigofera tintoria is 80-120 parts by weight. The ethanol is 90-100% ethanol and the added amount of the ethanol is 240-360 parts by weight. A soap contains the indigofera tinctoria manufactured through the same.
Abstract translation: 目的：提供靛蓝提取物的制备方法，通过控制提取溶剂，提取温度和提取时间，最大限度地提高抗生素，抗炎和抗美白效果。 构成：靛蓝提取物的制造方法包括向靛蓝染色剂中加入乙醇并在25-30℃下提取添加的混合物11-15小时的步骤。 靛蓝色素的添加量为80-120重量份。 乙醇为90-100％乙醇，乙醇的添加量为240-360重量份。 肥皂含有通过其制造的靛蓝染色剂。
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