METHOD FOR THE PRODUCTION OF CYCLOHEXANOL FROM BENZOLE

    公开(公告)号:AU2003210379A1

    公开(公告)日:2003-09-16

    申请号:AU2003210379

    申请日:2003-02-28

    Applicant: BASF AG

    Abstract: A process for preparing cyclohexanol from benzene by: a) preparing cyclohexene by hydrogenating benzene in the presence of a catalyst, and b) preparing cyclohexanol by hydrating the cyclohexene in the presence of a catalyst, comprises: carrying out steps a) and b) in a reaction facility which has a bottom region at the lower end, a top region at the upper end, and a reaction zone between the top region and the bottom region which contains the catalyst according to steps a) and b), evaporating a portion of the benzene using the heat of reaction in the reaction zone, condensing it in the top region and returning it to the reaction zone, and withdrawing a reaction mixture containing cyclohexanol in the bottom region.

    12.
    发明专利
    未知

    公开(公告)号:AT247083T

    公开(公告)日:2003-08-15

    申请号:AT00909259

    申请日:2000-02-28

    Applicant: BASF AG

    Abstract: The present invention relates to a process for the continuous preparation of methoxyamine hydrochloride by cleavage of acetone oxime methyl ether by means of hydrogen chloride and water, wherein the cleavage is carried out in a reaction column having less than 20 theoretical plates and the amount taken off at the top is set to at least 30% of the amount of feed.

    METODO PARA LA PURIFICACION DE DIMETILACETAMIDA (DMAC).

    公开(公告)号:ES2284003T3

    公开(公告)日:2007-11-01

    申请号:ES04725673

    申请日:2004-04-05

    Applicant: BASF AG

    Abstract: Dispositivo de corte de corriente eléctrico, tal como un interruptor seccionador, que incluye una caja (1), dos contactos fijos (21, 22) llevados por la caja, un contacto móvil (20) selectivamente aplicado sobre los contactos fijos (21, 22), un mecanismo de armado (3), que incluye un accionador (31), para desplazar selectivamente el contacto móvil (20) hacia los contactos fijos (21, 22), y medios de desencadenamiento (4) para liberar selectivamente el contacto móvil (20) de los contactos fijos (21, 22) en caso de desencadenamiento, el accionador (31) que incluyen una manecilla (311), una excéntrica (312) solidaria de la manecilla (311), y una biela (313) movida por la excéntrica, estando la manecilla (311) montada pivotante sobre la caja (1) entre su posición de reposo y una posición de enganche, estando elásticamente guiada hacia su posición de reposo, en la cual el contacto móvil (20) es liberado de los contactos fijos (21, 22), y estando dotada de un cubo (311a) que lleva un primer indicador luminoso de estado (61) visible desde el exterior de la caja (i) en la posición de reposo de la manecilla (311), el mecanismo de armado (3) que incluye, además el accionador (31), una corredera de arrastre (32) guiada siguiendo una primera dirección (D1) por una primera fuerza elástica (resorte 51) y que porta el contacto móvil (20), estando esta corredera 32 selectivamente desplazada en deslizamiento con relación a la caja (1), a lo largo de un primer eje (Z) que pasa entre los dos contactos fijos (21, 22), desde una posición inactiva que adopta en la posición de reposo de la manecilla (311) hasta una posición activa que adopta cuando la manecilla (311) alcanza su posición de enganchamiento y en la cual aplica el contacto móvil (20) sobre los contactos fijos (21, 22), y la biela (313) que adoptan selectivamente una configuración contratada que deja en caso de desencadenamiento, caracterizado por que la biela (313), en configuración contratada, vincula cinemáticamente la manecilla (311) a la corredera (32).

    15.
    发明专利
    未知

    公开(公告)号:BR0307813A

    公开(公告)日:2004-12-21

    申请号:BR0307813

    申请日:2003-02-28

    Applicant: BASF AG

    Abstract: A process for preparing cyclohexanol from benzene by: a) preparing cyclohexene by hydrogenating benzene in the presence of a catalyst, and b) preparing cyclohexanol by hydrating the cyclohexene in the presence of a catalyst, comprises: carrying out steps a) and b) in a reaction facility which has a bottom region at the lower end, a top region at the upper end, and a reaction zone between the top region and the bottom region which contains the catalyst according to steps a) and b), evaporating a portion of the benzene using the heat of reaction in the reaction zone, condensing it in the top region and returning it to the reaction zone, and withdrawing a reaction mixture containing cyclohexanol in the bottom region.

    16.
    发明专利
    未知

    公开(公告)号:DE10143424A1

    公开(公告)日:2003-03-20

    申请号:DE10143424

    申请日:2001-09-05

    Applicant: BASF AG

    Abstract: Production of ethanolamines comprises reacting ammonia with ethylene oxide in the presence of water in a pressurized reactive distillation column equipped with a reboiler. The energy supply to the reboiler and the ammonia:ethylene oxide ratio in the feed stream are controlled so that the bottoms stream can be separated into an ammonia and water stream and a mono-, di- and triethanolamine stream. Production of mono-, di- and triethanolamine comprises liquid-phase reaction of ammonia with ethylene oxide in the presence of water in a pressurized reactive distillation column (I) equipped with a reboiler, where the mono:di:triethanolamine ratio is controlled by the energy supply to the reboiler and the ammonia content of the bottoms stream is controlled by the ammonia:ethylene oxide ratio in the feed stream so that the bottoms stream can be separated into an ammonia and water stream and a mono-, di- and triethanolamine stream in a single distillation column (II).

    19.
    发明专利
    未知

    公开(公告)号:AT358666T

    公开(公告)日:2007-04-15

    申请号:AT04725673

    申请日:2004-04-05

    Applicant: BASF AG

    Abstract: The invention relates to a process for distillatively purifying crude dimethylacetamide (crude DMAc) comprising DMAc, low boilers and high boilers 5 by removing the low boilers and the high boilers to obtain pure DMAc in one of the column configurations listed hereinbelow: (I) a main column (MC) with sidestream column (SC) or (II) a dividing wall column (DWC), which operating at least the main column (MC) in column configuration (I) and the dividing wall column (DWC) in column configuration (II) at a top pressure in the range from 0.5 to 1.8 bar absolute.

    20.
    发明专利
    未知

    公开(公告)号:DE102004030616A1

    公开(公告)日:2006-01-26

    申请号:DE102004030616

    申请日:2004-06-24

    Applicant: BASF AG

    Abstract: Disclosed is a method for the distillative purification of aqueous raw dimethylacetamide (raw DMAc) containing DMAc as well as low-boiling and high-boiling components. According to the inventive method, the low-boiling and high-boiling components are eliminated in one column or several columns that are mounted in series so as to obtain pure DMAc. The disclosed method is characterized in that the pure DMAc is withdrawn from the single column or the last of several columns as a liquid side stream.

Patent Agency Ranking