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公开(公告)号:AU2003210379A1
公开(公告)日:2003-09-16
申请号:AU2003210379
申请日:2003-02-28
Applicant: BASF AG
Inventor: PESCHEL WERNER , ADRIAN TILL , RUST HARALD , BOTTCHER ARND , HILL THOMAS , MULLER ULRICH , PAPP RAINER
Abstract: A process for preparing cyclohexanol from benzene by: a) preparing cyclohexene by hydrogenating benzene in the presence of a catalyst, and b) preparing cyclohexanol by hydrating the cyclohexene in the presence of a catalyst, comprises: carrying out steps a) and b) in a reaction facility which has a bottom region at the lower end, a top region at the upper end, and a reaction zone between the top region and the bottom region which contains the catalyst according to steps a) and b), evaporating a portion of the benzene using the heat of reaction in the reaction zone, condensing it in the top region and returning it to the reaction zone, and withdrawing a reaction mixture containing cyclohexanol in the bottom region.
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公开(公告)号:AT247083T
公开(公告)日:2003-08-15
申请号:AT00909259
申请日:2000-02-28
Applicant: BASF AG
Inventor: HEIMANN FRANK , PESCHEL WERNER , BARTENBACH BERND , HARTMANN HORST , KEIL MICHAEL , WAHL JOSEF
IPC: B01D3/14 , B01D3/20 , C07C239/20
Abstract: The present invention relates to a process for the continuous preparation of methoxyamine hydrochloride by cleavage of acetone oxime methyl ether by means of hydrogen chloride and water, wherein the cleavage is carried out in a reaction column having less than 20 theoretical plates and the amount taken off at the top is set to at least 30% of the amount of feed.
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公开(公告)号:HU225876B1
公开(公告)日:2007-11-28
申请号:HU0200621
申请日:2000-02-28
Applicant: BASF AG
Inventor: HEIMANN FRANK DR , PESCHEL WERNER , BARTENBACH BERND , HARTMANN HORST , KEIL MICHAEL DR , WAHL JOSEF
IPC: B01D3/14 , C07C239/20 , B01D3/20
Abstract: The present invention relates to a process for the continuous preparation of methoxyamine hydrochloride by cleavage of acetone oxime methyl ether by means of hydrogen chloride and water, wherein the cleavage is carried out in a reaction column having less than 20 theoretical plates and the amount taken off at the top is set to at least 30% of the amount of feed.
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公开(公告)号:ES2284003T3
公开(公告)日:2007-11-01
申请号:ES04725673
申请日:2004-04-05
Applicant: BASF AG
Inventor: PESCHEL WERNER , SCHOENMAKERS HARTMUT , ALTHAUS KLAUS , KIRCHNER TANJA , STAATZ HARTMUT
IPC: C07C231/24 , C07C233/05
Abstract: Dispositivo de corte de corriente eléctrico, tal como un interruptor seccionador, que incluye una caja (1), dos contactos fijos (21, 22) llevados por la caja, un contacto móvil (20) selectivamente aplicado sobre los contactos fijos (21, 22), un mecanismo de armado (3), que incluye un accionador (31), para desplazar selectivamente el contacto móvil (20) hacia los contactos fijos (21, 22), y medios de desencadenamiento (4) para liberar selectivamente el contacto móvil (20) de los contactos fijos (21, 22) en caso de desencadenamiento, el accionador (31) que incluyen una manecilla (311), una excéntrica (312) solidaria de la manecilla (311), y una biela (313) movida por la excéntrica, estando la manecilla (311) montada pivotante sobre la caja (1) entre su posición de reposo y una posición de enganche, estando elásticamente guiada hacia su posición de reposo, en la cual el contacto móvil (20) es liberado de los contactos fijos (21, 22), y estando dotada de un cubo (311a) que lleva un primer indicador luminoso de estado (61) visible desde el exterior de la caja (i) en la posición de reposo de la manecilla (311), el mecanismo de armado (3) que incluye, además el accionador (31), una corredera de arrastre (32) guiada siguiendo una primera dirección (D1) por una primera fuerza elástica (resorte 51) y que porta el contacto móvil (20), estando esta corredera 32 selectivamente desplazada en deslizamiento con relación a la caja (1), a lo largo de un primer eje (Z) que pasa entre los dos contactos fijos (21, 22), desde una posición inactiva que adopta en la posición de reposo de la manecilla (311) hasta una posición activa que adopta cuando la manecilla (311) alcanza su posición de enganchamiento y en la cual aplica el contacto móvil (20) sobre los contactos fijos (21, 22), y la biela (313) que adoptan selectivamente una configuración contratada que deja en caso de desencadenamiento, caracterizado por que la biela (313), en configuración contratada, vincula cinemáticamente la manecilla (311) a la corredera (32).
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公开(公告)号:BR0307813A
公开(公告)日:2004-12-21
申请号:BR0307813
申请日:2003-02-28
Applicant: BASF AG
Inventor: PESCHEL WERNER , ADRIAN TILL , RUST HARALD , TTCHER ARND B , HILLMER THOMAS , LLER ULRICH M , PAPP RAINER
Abstract: A process for preparing cyclohexanol from benzene by: a) preparing cyclohexene by hydrogenating benzene in the presence of a catalyst, and b) preparing cyclohexanol by hydrating the cyclohexene in the presence of a catalyst, comprises: carrying out steps a) and b) in a reaction facility which has a bottom region at the lower end, a top region at the upper end, and a reaction zone between the top region and the bottom region which contains the catalyst according to steps a) and b), evaporating a portion of the benzene using the heat of reaction in the reaction zone, condensing it in the top region and returning it to the reaction zone, and withdrawing a reaction mixture containing cyclohexanol in the bottom region.
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公开(公告)号:DE10143424A1
公开(公告)日:2003-03-20
申请号:DE10143424
申请日:2001-09-05
Applicant: BASF AG
Inventor: PESCHEL WERNER , HILDEBRANDT AXEL , BESLING BERND
IPC: C07C213/04 , C07C215/08 , C07C215/12 , C07C215/10
Abstract: Production of ethanolamines comprises reacting ammonia with ethylene oxide in the presence of water in a pressurized reactive distillation column equipped with a reboiler. The energy supply to the reboiler and the ammonia:ethylene oxide ratio in the feed stream are controlled so that the bottoms stream can be separated into an ammonia and water stream and a mono-, di- and triethanolamine stream. Production of mono-, di- and triethanolamine comprises liquid-phase reaction of ammonia with ethylene oxide in the presence of water in a pressurized reactive distillation column (I) equipped with a reboiler, where the mono:di:triethanolamine ratio is controlled by the energy supply to the reboiler and the ammonia content of the bottoms stream is controlled by the ammonia:ethylene oxide ratio in the feed stream so that the bottoms stream can be separated into an ammonia and water stream and a mono-, di- and triethanolamine stream in a single distillation column (II).
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公开(公告)号:AU6994300A
公开(公告)日:2001-03-19
申请号:AU6994300
申请日:2000-08-10
Applicant: BASF AG
Inventor: PESCHEL WERNER , BESSLING BERND , REUTER PETER , LORZ PETER MICHAEL , ULRICH BERNHARD , KNAB JEAN WERNER , KUMMER MATTHIAS , RUHL THOMAS
IPC: B01D3/00 , B01D3/10 , B01D3/14 , C07C51/573 , C07C63/16 , C07D307/89
Abstract: On-spec phthalic anhydride is prepared by distillative purification of crude phthalic anhydride by a process in which crude phthalic anhydride is fed to a distillation column which is operated at reduced pressure, the low boilers are removed at the top or in the vicinity of the top of the distillation column and the on-spec phthalic anhydride is removed from the column via a side take-off.
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公开(公告)号:DE19939629A1
公开(公告)日:2001-02-22
申请号:DE19939629
申请日:1999-08-20
Applicant: BASF AG
Inventor: PESCHEL WERNER , BESLING BERND , REUTER PETER , LORZ PETER MICHAEL , ULRICH BERNHARD
IPC: B01D3/00 , B01D3/10 , B01D3/14 , C07C51/573 , C07C63/16 , C07D307/89
Abstract: Production of phthalic anhydride involves the distillation of crude PA under reduced pressure. Production of phthalic anhydride (PA) which complies with specifications involves the distillation of crude PA under reduced pressure in a column from which the volatiles are taken off at or near the top of the column and the pure PA is taken off at a side arm.
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公开(公告)号:AT358666T
公开(公告)日:2007-04-15
申请号:AT04725673
申请日:2004-04-05
Applicant: BASF AG
Inventor: PESCHEL WERNER , SCHOENMAKERS HARTMUT , ALTHAUS KLAUS , KIRCHNER TANJA , STAATZ HARTMUT
IPC: C07C231/24 , C07C233/05
Abstract: The invention relates to a process for distillatively purifying crude dimethylacetamide (crude DMAc) comprising DMAc, low boilers and high boilers 5 by removing the low boilers and the high boilers to obtain pure DMAc in one of the column configurations listed hereinbelow: (I) a main column (MC) with sidestream column (SC) or (II) a dividing wall column (DWC), which operating at least the main column (MC) in column configuration (I) and the dividing wall column (DWC) in column configuration (II) at a top pressure in the range from 0.5 to 1.8 bar absolute.
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公开(公告)号:DE102004030616A1
公开(公告)日:2006-01-26
申请号:DE102004030616
申请日:2004-06-24
Applicant: BASF AG
Inventor: PESCHEL WERNER , RUST HARALD , KIRCHNER TANJA
IPC: B01D3/14 , C07C231/24 , C07C233/05
Abstract: Disclosed is a method for the distillative purification of aqueous raw dimethylacetamide (raw DMAc) containing DMAc as well as low-boiling and high-boiling components. According to the inventive method, the low-boiling and high-boiling components are eliminated in one column or several columns that are mounted in series so as to obtain pure DMAc. The disclosed method is characterized in that the pure DMAc is withdrawn from the single column or the last of several columns as a liquid side stream.
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