Abstract:
The invention relates to a method for the production of phthalic anhydride to a specification, using a distillative purification of crude phthalic anhydride, by introduction of crude phthalic anhydride into a distillation column, operating at reduced pressure, withdrawal of the low-boiling fraction from the head, or near the head of the column and withdrawal of the phthalic anhydride, which meets the specification, from a side-tap on the column, whilst operating the column at a reflux ratio x, with 1:1.7
Abstract translation:一种用于通过粗邻苯二甲酸酐的纯化destillacive制备上规格邻苯二甲酸酐的过程中,邻苯二甲酸酐得到粗蒸馏。 列,其在降低的压力下操作,在顶部或附近经由从塔的侧取出口的蒸馏塔的顶部和上规格邻苯二甲酸酐供给低沸以N回流比x取出由列中1:1.7 < X <1:操作第三
Abstract:
The invention relates to an aqueous resin composition, comprising, in addition to water, a resin content in the range of from 65 to 80 % by weight, based on the aqueous resin composition. The resin is obtainable from melamine and formaldehyde and optionally at least one additive, and the aqueous resin composition has a viscosity ranging from 100 to 3000 mPas at 20 DEG C. The invention further relates to a method for producing the resin composition, to a composite containing said composition, to an impregnating resin dispersion, and to a method for producing the same. The invention also relates to the storage and use of said resin composition and impregnating resin dispersion.
Abstract:
The invention relates to a pump (1) comprising a pump feed tube (13) for transporting a heat exchange medium (6) for a reactor containing a bundle of catalyst tubes (2). The pump (1) has a housing (14) that surrounds the pump feed tube (13) and comprises an opening (15) in the lower part of the housing (14), which allows the heat exchange medium (6) that is drawn from the lower section of the reactor by the pump (1) to flow into the housing (14). The medium flows upwards in the section lying between the internal wall of the housing (14) and the external wall of the pump feed tube (13), optionally over a heat exchanger (18) and into the interior of the pump feed tube (13) via an opening (16) in the upper section of said pump feed tube (13). The medium then flows through the pump feed tube from top to bottom, into the reactor via an opening (17) in the lower section of said tube (13) and into the upper section of the intermediate chamber between the catalyst tubes (2).
Abstract:
Pump comprises a housing containing a guide pipe and having an opening in its lower part, via which heat transfer medium removed from the lower region of a reactor flows into the housing. Pump comprises a housing (14) containing a guide pipe (13) and having an opening (15) in its lower part, via which heat transfer medium (6) removed from the lower region of a reactor flows into the housing. The medium further flows up between the inner wall of the housing and the outer wall of the guide pipe via a heat exchanger (18), via an opening in the upper region of the pipe into the inner chamber of the pipe, then via an opening in the lower region of the pipe into a further intermediate chamber between the inner wall of the housing and the outer wall of the guide pipe, and finally into the upper region of the intermediate chamber between contact tubes. Preferred Features: The pump is a propeller pump having three or more blades. The housing is rectangular or circular. Baffle plates (19) are arranged in one or more deviating regions of the housing for the heat transfer medium.
Abstract:
On-spec phthalic anhydride is prepared by distillative purification of crude phthalic anhydride by a process in which crude phthalic anhydride is fed to a distillation column which is operated at reduced pressure, the low boilers are removed at the top or in the vicinity of the top of the distillation column and the on-spec phthalic anhydride is removed from the column via a side take-off.
Abstract:
PCT No. PCT/EP95/02747 Sec. 371 Date Jan. 23, 1997 Sec. 102(e) Date Jan. 23, 1997 PCT Filed Jul. 13, 1995 PCT Pub. No. WO96/03449 PCT Pub. Date Feb. 8, 1996Binders comprise A) an aminotriazine derivative in which the primary amino groups of the triazine are methylolated on average with at least one mole of formaldehyde per mole of primary amino groups, and these methylol groups are etherified on average with at least 0.5 mol of primary alcohol per mole of methylol group and the primary alcohols are a mixture containing a) 0.5-99.5 mol % of a C1-C4-alkanol and b) 99.5-0.5 mol % of an alcohol of the formulaR1-O-[R2-O]n-R3-OHI,in which R1 is C1-C24-alkyl or C6-C12-aryl which may be unsubstituted or substituted by from one to three C1-C8-alkyl groups, and R2 and R3 independently of one another are C2-C8-alkylene and n is an integer from 1 to 100, or of a mixture of higher-boiling alcohols having a boiling point of above 120 DEG C. at 1 bar which contains at least 10 mol %, based on the higher-boiling alcohols, of alcohols of the formula I, and B) a radical polymer, polycondensation product or polyadduct which is crosslinkable with the aminotriazine derivative.
Abstract:
The invention concerns binders containing: A) an aminotriazine derivative in which the triazine primary amino groups are methylolated on average with at least one mol of formaldehyde per mole of primary amino groups and these methylol groups are etherified on average with at least 0.5 mole primary alcohol per mole of methylol group, and the primary alcohols are a mixture containing: a) 0.5 to 99.5 mol % of a C1-C4 alkanol and b) 99.5 to 0.5 mol % of an alcohol of the formula (I) R1-O-¢R2-O!n-R3-OH, in which R1 stands for a C1-C24 alkyl group or a C6-C12 aryl group which may optionally be substituted by one to three C1-C8 alkyl groups, and R2 and R3, independently of each other, stand for a C2-C8 alkylene group, and n means an integer from 1 to 100, or a mixture of higher-boiling alcohols having a boiling point of more than 120 ~C at 1 bar, which contains at least 10 mol %, relative to the higherboiling alcohols, of alcohols of formula I; and B) a radical polymer, which can be crosslinked with the aminotriazine derivative, a polycondensate or polymer additive.
Abstract:
Process for the pretreatment of textile materials in aqueous media by alkaline scouring and/or bleaching using as auxiliary a compound of the formula I … … where R is C6-C10-alkyl, X is H, Na, K or NR R R R , and R , R , R and R are each H, C1-C4-alkyl or -CH2-CH2-OH.