VERFAHREN UND VORRICHTUNG ZUR HERSTELLUNG VON ISOCYANATEN

    公开(公告)号:EP2408738A2

    公开(公告)日:2012-01-25

    申请号:EP10709217.3

    申请日:2010-03-18

    Applicant: BASF SE

    Abstract: The invention relates to a method for producing isocyanates by converting the corresponding amine with phosgene in the gas phase, in the presence of an inert medium as applicable, wherein phosgene and amine are first vaporized and then overheated to reaction temperature, the overheated phosgene and amine are mixed and added to a reactor wherein the phosgene and the amine are converted to isocyanate, wherein the dwell time of the phosgene at temperatures greater than 300°C equals a maximum of 5 sec and/or the temperature of heat transfer surfaces in contact with the phosgene is 20 K above the phosgene temperature to be set at maximum. The invention further relates to a device for producing isocyanates by converting the corresponding amine with phosgene in the gas phase.

    Abstract translation: 本发明涉及一种生产异氰酸酯的方法,该方法通过在惰性介质存在下将气相中的相应胺转化为气相,其中光气和胺首先被蒸发,然后过热至反应温度,过热的光气和胺 混合并加入其中光气和胺转化为异氰酸酯的反应器中,其中光气在高于300℃的温度下的停留时间等于最多5秒和/或与其接触的传热表面的温度 光气比光气温度高20K以设定最大值。 本发明还涉及一种通过在气相中用光气转化相应的胺来生产异氰酸酯的装置。

    VERFAHREN ZUR HERSTELLUNG VON CAROTINOID-LÖSUNGEN V
    14.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON CAROTINOID-LÖSUNGEN V 有权
    VERFAHREN ZUR HERSTELLUNG VON CAROTINOID-LÖSUNGENV

    公开(公告)号:EP2403361A1

    公开(公告)日:2012-01-11

    申请号:EP10707006.2

    申请日:2010-03-03

    Applicant: BASF SE

    Abstract: The present invention relates to a method for producing carotenoid solutions in an oil suitable for food. In particular, the invention relates to a method for dissolving a carotenoid, in particular astaxanthin, in an oil suitable for food by heating a suspension of the carotenoid, especially astaxanthin, in the oil and then rapidly cooling (quenching) the obtained solution. The method comprises the following steps: i. providing a suspension of the carotenoid in an oil suitable for food; ii. continuously heating a flow of the carotenoid suspension, wherein a hot carotenoid solution is obtained; and iii. continuously rapidly cooling the hot carotenoid solution, wherein the carotenoid suspension is conducted over a heated heat exchanger surface as a thin liquid film in order to continuously heat the carotenoid suspension.

    Abstract translation: 本发明涉及在适用于食品的油中生产类胡萝卜素溶液的方法。 具体地说,本发明涉及一种通过在油中加热类胡萝卜素特别是虾青素的悬浮液然后快速冷却(骤冷)所得溶液来将类胡萝卜素,特别是虾青素溶解在适合食物的油中的方法。 该方法包括以下步骤:i。 提供类胡萝卜素在适合食物的油中的悬浮液; II。 连续加热类胡萝卜素悬浮液的流动,其中获得热的类胡萝卜素溶液; 和iii。 连续快速冷却热类胡萝卜素溶液,其中类胡萝卜素悬浮液作为薄液膜在加热的换热器表面上传导以连续加热类胡萝卜素悬浮液。

    VERFAHREN ZUR GEWINNUNG VON CYCLODODECATRIEN DURCH VERDAMPFUNG
    15.
    发明授权
    VERFAHREN ZUR GEWINNUNG VON CYCLODODECATRIEN DURCH VERDAMPFUNG 有权
    一种获得三烯由于膨胀

    公开(公告)号:EP1907342B1

    公开(公告)日:2011-12-21

    申请号:EP06763996.3

    申请日:2006-06-30

    Applicant: BASF SE

    CPC classification number: C07C7/04 C07C13/277

    Abstract: The invention relates to a method for obtaining cyclododecatriene (CDT) from a solution containing CDT and high-boiling components such as a deactivated catalyst and polymers. Said solution is supplied to a preheater and heated, and is then relaxed over a downstream pressure maintaining device, and the two-phase mixture obtained is supplied to a spiral tube evaporator where the CDT content of the liquid phase is reduced by partial evaporation and a gaseous product flow with an increased CDT concentration is derived.

    VERFAHREN ZUR HERSTELLUNG VON ISOCYANATEN

    公开(公告)号:EP2197836A1

    公开(公告)日:2010-06-23

    申请号:EP08803255.2

    申请日:2008-08-27

    Applicant: BASF SE

    CPC classification number: C07C263/10 C07C263/20 C07C265/14

    Abstract: The invention relates to a method for producing polyisocyanates, comprising the following steps: a) amines are reacted with phosgene; b) hydrogen chloride, excess phosgene, and, if necessary, the solvent are separated from the reaction mixture; c) the liquid mixture from step b) is separated into a liquid and a gaseous phase; d) the gaseous phase from step c) is processed into the polyisocyanate.

    Abstract translation: 本发明涉及一种生产多异氰酸酯的方法,包括以下步骤:a)胺与光气反应; b)将氯化氢,过量的光气和必要时的溶剂从反应混合物中分离出来; c)将来自步骤b)的液体混合物分离成液相和气相; d)将来自步骤c)的气相加工成多异氰酸酯。

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