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    Crystalline forms of 1-(1,2-dimethylpropyl)-N-ethyl-5-methyl-N-pyridazin-4-yl-pyrazole-4-carboxamide
    11.
    发明专利
    Crystalline forms of 1-(1,2-dimethylpropyl)-N-ethyl-5-methyl-N-pyridazin-4-yl-pyrazole-4-carboxamide 未知

    公开(公告)号：AU2020206519A1

    公开(公告)日：2021-07-15

    申请号：AU2020206519

    申请日：2020-01-10

    Applicant: BASF SE

    Inventor： GEBHARDT JOACHIM ,  VIERTELHAUS MARTIN ,  CHIODO TIZIANA ,  RACK MICHAEL ,  KLAUBER ERIC GEORGE ,  XU WEN ,  GOETZ ROLAND ,  VOGT FLORIAN ,  GOCKEL BIRGIT ,  SOERGEL SEBASTIAN

    IPC: C07D403/12

    Abstract: The present invention relates to a novel crystalline form of 1-(1,2-dimethylpropyl)- N-ethyl-5-methyl-N-pyridazin-4-yl-pyrazole-4-carboxamide recently assigned the common name dimpropyridaz. The invention also relates to the use of the crystalline form B for combating invertebrate pests and to formulations for plant protection which contain the crystalline form B of 1-(1,2-dimethylpropyl)-N-ethyl-5-methyl-N-pyridazin-4- yl-pyrazole-4-carboxamide. The crystalline form B according to the present invention can be identified by powder X-ray diffractometry on the basis of its powder X-ray diffraction diagram, hereinafter also termed powder X-ray diffraction pattern or PXRD pattern,of the polymorph form B recorded using Cu-Kα radiation (1.54178 Å) at 25°C displays the 3 following reflections, quoted as 2θ values: 20.69±0.10°, 24.15±0.10°and 30.52± 0.10°.In addition to these 3 reflections, the polymorph B of the present invention may display in such a PXRD pattern one or more, in particular at least 2, often at least 4, in particular at least 6 or at least 8 reflections and especially all of the reflections quoted hereinafter as 2θ values:7.99±0.10°, 10.07±0.10°, 12.38±0.10°,15.31±0.10°, 15.97±0.10°, 16.50±0.10°, 18.03±0.10°,19.29±0.10°, 20.22±.0.10°, 20.96± 0.10°, 23.40±0.10°, 23.70±0.10°,26.09±0.10°, 27.26±0.10°and 32.91±0.10°.

    Method for obtaining crystalline 2'-fucosyllactose
    12.
    发明专利
    Method for obtaining crystalline 2'-fucosyllactose 未知

    公开(公告)号：AU2019360630A1

    公开(公告)日：2021-04-29

    申请号：AU2019360630

    申请日：2019-10-17

    Applicant: BASF SE

    Inventor： PUHL MICHAEL ,  WLOCH SEBASTIAN ,  OEDMAN PETER ,  LETZEL ANNE-CATRIN ,  SCHROEDER HARTWIG ,  MALISZ JACEK ,  SEIBERT-LUDWIG DANIEL ,  KAPPERT EMIEL JAN ,  WONG CHUNG HUAN ,  BARROS GROSS MICHAEL ,  VIERTELHAUS MARTIN

    IPC: C07H1/06 ,  C07H1/08

    Abstract: The present invention relates to a method for obtaining crystalline 2'-fucosyllactose from a 2'-FL raw material, which contains 2'-FL as a main constituent and at least 0.5% by weight, frequently at least 1% by weight, in particular at least 2% by weight, more particularly at least 5% by weight, and especially at least 8% by weight,based on the total amount of mono-and oligosaccharides in the raw material, of one or more mono- or oligosaccharides different from 2'-FL, where the method comprises a)providing a solution of the 2'-FL raw material in water, which does not contain more than 10% by weight, preferably not more than 7% by weight, more preferably not more than 5% by weight of organic solvents, based on the total amount of water; b) effecting the crystallization of 2'-FL from the solution provided in step a) by inducing conditions of a controlled super saturation in the solution; and c) separating crystalline 2'-FL from the mother liquor, and where during controlled supersaturation in step b) not more than 10% by weight, preferably not more than 7% by weight, more preferably not more than 5% by weight of organic solvents are present, based on the total amount of water present during step b).

    CRYSTALLINE FORMS OF 1-(1,2-DIMETHYLPROPYL)-N-ETHYL-5-METHYL-N-PYRIDAZIN-4-YL-PYRAZOLE-4-CARBOXAMIDE
    13.
    发明专利
    CRYSTALLINE FORMS OF 1-(1,2-DIMETHYLPROPYL)-N-ETHYL-5-METHYL-N-PYRIDAZIN-4-YL-PYRAZOLE-4-CARBOXAMIDE 未知

    公开(公告)号：CA3122208A1

    公开(公告)日：2020-07-16

    申请号：CA3122208

    申请日：2020-01-10

    Applicant: BASF SE

    Inventor： GEBHARDT JOACHIM ,  VIERTELHAUS MARTIN ,  CHIODO TIZIANA ,  RACK MICHAEL ,  KLAUBER ERIC GEORGE ,  XU WEN ,  GOETZ ROLAND ,  VOGT FLORIAN ,  GOCKEL BIRGIT ,  SOERGEL SEBASTIAN

    IPC: C07D403/12

    Abstract: The present invention relates to a novel crystalline form of 1-(1,2-dimethylpropyl)- N-ethyl-5-methyl-N-pyridazin-4-yl-pyrazole-4-carboxamide recently assigned the common name dimpropyridaz. The invention also relates to the use of the crystalline form B for combating invertebrate pests and to formulations for plant protection which contain the crystalline form B of 1-(1,2-dimethylpropyl)-N-ethyl-5-methyl-N-pyridazin-4- yl-pyrazole-4-carboxamide. The crystalline form B according to the present invention can be identified by powder X-ray diffractometry on the basis of its powder X-ray diffraction diagram, hereinafter also termed powder X-ray diffraction pattern or PXRD pattern,of the polymorph form B recorded using Cu-Ka radiation (1.54178 Å) at 25°C displays the 3 following reflections, quoted as 2? values: 20.69±0.10°, 24.15±0.10°and 30.52± 0.10°.In addition to these 3 reflections, the polymorph B of the present invention may display in such a PXRD pattern one or more, in particular at least 2, often at least 4, in particular at least 6 or at least 8 reflections and especially all of the reflections quoted hereinafter as 2? values:7.99±0.10°, 10.07±0.10°, 12.38±0.10°,15.31±0.10°, 15.97±0.10°, 16.50±0.10°, 18.03±0.10°,19.29±0.10°, 20.22±Ø10°, 20.96± 0.10°, 23.40±0.10°, 23.70±0.10°,26.09±0.10°, 27.26±0.10°and 32.91±0.10°.

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