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公开(公告)号：KR101569664B1
公开(公告)日：2015-11-17
申请号：KR1020140035889
申请日：2014-03-27
Applicant: 한국화학연구원
IPC: C01B31/04
Abstract: 본발명에따르면, 쉬트상에하나이상의구멍이형성되어있는구멍뚫린그래핀옥사이드(GO) 쉬트및 층간삽입물질또는층간가교물질에의한층간가교연결을포함하는, 구멍뚫린(Holey) 그래핀옥사이드(GO)의다공성 3차원구조체및 이의제조방법이제공되는데, 전술한층간가교연결은 (A) 유기보론산화합물또는이의에스테르, (B) 아미노, 히드록시, 티올, 실란, 할라이드, 카르복실산및 시아노로구성된군에서선택되는치환기를하나이상갖는유기화합물및 (C) 아미노, 히드록시, 티올, 실란, 할라이드, 카르복실산및 시아노로구성된군에서선택되는치환기를하나이상가질수 있는유기금속화합물에서선택되거나이들로부터유래되는층간삽입물질일수 있다. 전술한구멍뚫린그래핀옥사이드(GO)의다공성 3차원구조체는층간물질에의해층간거리가확장될수 있고, 층간물질의선택에의해층간거리를조절할수 있고, 다층쉬트를가로질러물질이비교적용이하게출입할수 있기때문에수소, 질소, 산소와같은기체및 리튬과같은물질들의저장또는흡장성능이매우우수하다.
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公开(公告)号：KR1020150029460A
公开(公告)日：2015-03-18
申请号：KR1020130108693
申请日：2013-09-10
Applicant: 한국화학연구원
CPC classification number: A61L9/01 , A61L9/014 , A61L2209/21
Abstract: 본 발명은 담체로서, 불포화 금속 자리를 갖는 금속 유기 골격체(metal organic framework); 및 상기 금속 유기 골격체의 세공 내 포집되어, -30℃ 내지 60℃에서 0.001 wt% 이상 기화가능한 방향제 활성 성분을 포함하는 서방형 방향제 복합체로서, 금속 유기 골격체의 세공 내 포집된 상기 방향제 활성 성분이 공기 중으로 확산될 수 있는 것인 서방형 방향제 복합체; 및 이의 제조방법을 제공한다.
본 발명의 서방형 방향제 복합체는, 금속 유기 골격체 내에 방향제 활성성분이 담지되어 별도의 고착성분의 첨가나 캡슐화 없이도, 방향제 활성성분이 공기 중으로 서서히 방출된다. 용도에 따라, 금속 유기 골격체 내에 다양한 방향제 활성성분을 담지할 수 있으며, 조류 퇴치성분을 담지하는 경우 방충제로도 활용 가능하다.Abstract translation: 本发明涉及作为载体的持续释放的调味剂复合物，包括具有不饱和金属位置的金属有机骨架; 和0.001wt％的调味剂的活性成分，其被捕获在金属有机骨架的细胞中，因此能够改变为-30至60摄氏度之间的蒸气，其中提供了持续释放的调味剂复合物，其允许 将调味剂的捕获活性成分扩散到空气中金属有机框架工件的孔隙率及其制造方法中。 允许持续释放的调味剂复合物在空气中释放调味剂的活性成分而不添加额外的粘合剂组分或包封，因为调味剂的活性成分被携带在金属有机骨架中，从而使各种活性物质 调味剂的成分根据其用途携带在金属有机骨架中，并且如果携带用于排斥鸟类的组分被用作驱避剂。
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公开(公告)号：KR1020120021899A
公开(公告)日：2012-03-09
申请号：KR1020100080977
申请日：2010-08-20
Applicant: 한국화학연구원
CPC classification number: H01L51/5259 , H01L23/564 , H01L51/0077 , H01L51/5237
Abstract: PURPOSE: A porous organic-inorganic hybrid material, a method for manufacturing the same, an absorbent including the same, and the use of the same are provided to improve the initial absorbing speed of the hybrid material at high relative humidity and to improve the absorbing capability of the hybrid material at low relative humidity by carrying ionic compound or polar compound. CONSTITUTION: A method for manufacturing a porous organic-inorganic hybrid material includes the following: an ionic compound or a polar compound is carried in the hybrid material; a reaction mixture containing one or more inorganic metal precursor, one or more organic compounds functioning as ligand, and a solvent is prepared; porous organic-inorganic hybrid material is formed based on the reaction mixture. A moisture absorbent includes the hybrid material, a organic-inorganic hybrid material-inorganic complex, and the combination of the same.
Abstract translation: 目的：提供一种多孔有机 - 无机混合材料，其制造方法，包含该多孔有机 - 无机混合材料的吸收剂及其用途，以提高混合材料在高相对湿度下的初始吸收速度并改善吸收 通过携带离子化合物或极性化合物在低相对湿度下混合材料的能力。 构成：多孔有机 - 无机混合材料的制造方法包括：在混合材料中载带有离子性化合物或极性化合物; 制备含有一种或多种无机金属前体，一种或多种用作配体的有机化合物和溶剂的反应混合物; 基于反应混合物形成多孔有机 - 无机杂化材料。 吸湿剂包括混合材料，有机 - 无机杂化材料 - 无机复合物及其组合。
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公开(公告)号：KR100786613B1
公开(公告)日：2007-12-21
申请号：KR1020060086303
申请日：2006-09-07
Applicant: 한국화학연구원
Abstract: A method for preparing an olefin trimer and a method for preparing an alkylate having a high boiling point by using the olefin timer are provided to increase conversion rate and yield. An olefin trimer is prepared by using an acid catalyst comprising both Bronsted acid and Lewis acid or an acid catalyst obtained by sintering or washing the acid catalyst. Preferably the acid catalyst is prepared by introducing BF3, BCl3, BI3, SbF5, SbCl5, AlCl3, AlBr3, TiCl4, TiBr4, ZrCl4, PF5, FeCl3, FeBr3, SnBr4 or SnCl4 to a porous body such as hydrogen type zeolite or aluminophosphate, or an ion exchange resin having at least one acid group selected from a sulfonic acid group, a carboxyl group and a phosphoric acid group.
Abstract translation: 提供烯烃三聚体的制备方法和使用烯烃定时器制备具有高沸点的烷基化物的方法，以提高转化率和产率。 通过使用包含布朗斯台德酸和路易斯酸的酸催化剂或通过烧结或洗涤酸催化剂获得的酸催化剂制备烯烃三聚体。 优选地，通过将BF 3，BCl 3，BI 3，SbF 5，SbCl 5，AlCl 3，AlBr 3，TiCl 4，TiBr 4，ZrCl 4，PF 5，FeCl 3，FeBr 3，SnBr 4或SnCl 4引入多孔体如氢型沸石或磷酸铝，或 具有至少一个选自磺酸基，羧基和磷酸基的酸基的离子交换树脂。
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Patent Agency Ranking26.发明公开신규한 1-[1-(3,4-디알콕시페닐)-알킬]-1Ｈ-피라졸 화합물,이의 제조방법 및 이를 포함하는 약제학적 조성물 失效1- [1-（3,4-二甲氧基苯基） - 乙基] -1H-吡唑化合物，其制备方法和包含其的药物组合物
公开(公告)号：KR1020080065722A
公开(公告)日：2008-07-15
申请号：KR1020070002715
申请日：2007-01-10
Applicant: 한국화학연구원
Inventor： 전동주 , 노재성 , 송종환 , 이계형 , 김익연 , 박창민 , 소원영 , 이지선 , 김은주 , 강남숙 , 천혜경 , 조영식 , 송진숙 , 배명애 , 김지현 , 조중명 , 노성구 , 현영란 , 이철순 , 이재일 , 유성은
IPC: C07D231/12 , C07D401/04 , C07D403/10 , C07D413/04
Abstract: A novel compound is provided to show excellent activity on PDE-4 enzymes and high selectivity on other PDE enzymes, thereby being used as a therapeutic agent of inflammation related diseases, arthritis, atopic dermatitis, leukemia, various cancers and degenerative brain diseases with little side effects. A 1-[1-(3,4-dialkoxyphenyl)-alkyl]-1H-pyrazole compound is represented by a formula(1) and is prepared by reacting a halo-benzyl compound represented by a formula(2) with a pyrazole compound represented by a formula(3). In the formula(1), each R1 and R2 is independently H, linear or branched saturated or unsaturated C1-7 alkyl which may be substituted or unsubstituted by halogen, C3-7 cycloalkyl, (C3-7)cycloalkyl(C1-7)alkyl, aryl or heteroaryl, ar(C1-5)alkyl, or ar(C1-5)alkoxy, or the R1 and R2 may be linked to each other by C1-3 alkylene; each R3, R4 and R5 is independently H, phenyl, pyridinyl, N-oxypyridinyl, linear or branched saturated and unsaturated C1-7 alkyl, C3-7 cycloalkyl, (C3-10)cycloalkyl(C1-7)alkyl, halogen, cyano, nitro, amino, mono- or di(C1-7)alkylamino, mono or di(C1-7)alkylaminocarbonyl, C3-7 cycloalkylamino, 3 to 7-membered saturated or unsaturated hetero-ring including O, N or S, guanidinyl, ureido, benzyl, benzyloxy, formyl, C1-7 alkanoyl, C1-7 alkoxy, (C1-7)alkoxy(C1-7)alkyl, hydroxy(C1-7)alkyl, carboxyl, or (C1-7)alkoxycarbonyl; R6 is linear or branched saturated and unsaturated C1-7 alkyl, C3-7 cycloalkyl, (C3-10)cycloalkyl(C1-7)alkyl, phenyl, phenoxy, benzyl, benzyloxy, C1-7 alkoxy, or (C1-7)alkoxy(C1-7)alkyl. A pharmaceutical composition for treating or preventing diseases related to airway inflammation, arthritis, atopic dermatitis, leukemia, cancer or degenerative brain diseases comprises the 1-[1-(3,4-dialkoxyphenyl)-alkyl]-1H-pyrazole derivative as an effective ingredient.
Abstract translation: 提供了一种新型化合物，以显示对PDE-4酶的优异活性和对其他PDE酶的高选择性，从而被用作炎症相关疾病，关节炎，特应性皮炎，白血病，各种癌症和退行性脑病的治疗剂 效果。 1-（1-（3,4-二烷氧基苯基） - 烷基] -1H-吡唑化合物由式（1）表示，通过式（2）表示的卤代苄基化合物与吡唑化合物 由公式（3）表示。 在式（1）中，每个R 1和R 2独立地为H，可被卤素取代或未取代的直链或支链饱和或不饱和C 1-7烷基，C 3-7环烷基，（C 3-7）环烷基（C 1-7） 烷基，芳基或杂芳基，芳（C 1-5）烷基或芳（C 1-5）烷氧基，或者R 1和R 2可以被C 1-3亚烷基相互连接; 每个R 3，R 4和R 5独立地为H，苯基，吡啶基，N-氧代吡啶基，直链或支链饱和和不饱和C 1-7烷基，C 3-7环烷基，（C 3-10）环烷基（C 1-7）烷基，卤素，氰基 ，硝基，氨基，单或二（C1-7）烷基氨基，单或二（C1-7）烷基氨基羰基，C3-7环烷基氨基，3至7元饱和或不饱和杂环，包括O，N或S，胍基 （C 1-7）烷基，羟基（C 1-7）烷基，羧基或（C 1-7）烷氧基羰基;（C 1-7）烷氧基， R6是直链或支链饱和和不饱和的C1-7烷基，C3-7环烷基，（C3-10）环烷基（C1-7）烷基，苯基，苯氧基，苄基，苄氧基，C1-7烷氧基或（C1-7） 烷氧基（C 1-7）烷基。 用于治疗或预防与气道炎症，关节炎，特应性皮炎，白血病，癌症或退行性脑疾病相关的疾病的药物组合物包括1- [1-（3,4-二烷氧基苯基） - 烷基] -1H-吡唑衍生物作为有效的 成分。
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公开(公告)号：KR102211656B1
公开(公告)日：2021-02-04
申请号：KR1020180031678
申请日：2018-03-19
Applicant: 보드 오브 리전츠, 더 유니버시티 오브 텍사스 시스템 , 한국화학연구원
Abstract: 본발명은 2가금속이온과피리딘계카르복시산리간드로부터얻어진유무기하이브리드나노세공체를포함하는흡착제및 이의용도에관한것으로, 더욱상세하게는 2가금속이온과피리딘계카르복시산리간드로부터얻어짐으로인해저온에서탈착재생이가능하고, 낮은상대습도하에서도수분또는알코올에대해유무기하이브리드나노세공체 1 그램또는 1 밀리리터당 0.15 그램이상, 0.3 그램에가까운높은흡착량을보유하고, 특히저온에서탈착재생이가능하고, 낮은상대습도하에서도높은흡착량을갖는수분및/또는알코올흡착제를제공할수 있다.
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公开(公告)号：KR1020130015013A
公开(公告)日：2013-02-12
申请号：KR1020130004170
申请日：2013-01-14
Applicant: 한국화학연구원
CPC classification number: H01L51/5259 , B01J20/292 , F24F3/1411
Abstract: PURPOSE: A porous organic-inorganic hybrid, a manufacturing method thereof, an adsorbent comprising the same, and an application thereof are provided to have excellent adsorbing ability at the low relative humid condition by dipping an ionic compound or a polar compound to the porous organic-inorganic hybrid. CONSTITUTION: A manufacturing method of a porous organic-inorganic hybrid comprises the following step. A supplementary inorganic material is dipped to a moist adsorbent which is the porous organic inorganic hybrid in a crystallized form with constant rate or additionally mixed, and dipping inorganic salt with adsorption or hygroscopic ability to the porous organic inorganic hybrid. The supplementary inorganic material is selected from silica, alumina, mesopore, zeolite, boehmite, layer structured compounds, clay, carbon, graphite, graphene, and a combination thereof. The weight ratio of the supplementary inorganic material to the moist adsorbent is 0.1-200 parts by weight based on 100 parts by weight of organic-inorganic hybrid.
Abstract translation: 目的：提供一种多孔有机 - 无机杂化物，其制造方法，包含该吸附剂的吸附剂及其应用，其通过将离子化合物或极性化合物浸渍到多孔有机物中而在低相对湿度条件下具有优异的吸附能力 - 无机杂种。 构成：多孔有机 - 无机杂化物的制造方法包括以下步骤。 将补充的无机材料浸渍到具有恒定速率或另外混合的结晶形式的多孔有机无机杂化物的湿吸附剂中，并且对多孔有机无机混合物具有吸附或吸湿能力的浸渍无机盐。 辅助无机材料选自二氧化硅，氧化铝，中孔，沸石，勃姆石，层状结构化合物，粘土，碳，石墨，石墨烯及其组合。 辅助无机材料与湿吸附剂的重量比为0.1〜200重量份，基于100重量份的有机 - 无机杂化物。
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30.发明公开유무기 하이브리드 나노세공체의 제조방법, 상기 방법에 의하여 수득되는 유무기 하이브리드 나노세공체 및 이의 흡착제로서의 용도 有权用于制备有机 - 无机混合纳米材料的方法，通过公知方法获得的有机 - 无机混合纳米材料和用作吸收材料
公开(公告)号：KR1020100122300A
公开(公告)日：2010-11-22
申请号：KR1020090041276
申请日：2009-05-12
Applicant: 한국화학연구원
Abstract: PURPOSE: A manufacturing method of an organic-inorganic hybrid nanoporous material, the organic-inorganic hybrid nanoporous material manufactured therefrom, and the use thereof as an adsorber are provided to synthesize the nanoporous material using a microwave irradiation method. CONSTITUTION: A manufacturing method of an organic-inorganic hybrid nanoporous material comprises the following steps: stirring a divalent metal ion, dihydroxy-terephthalate organic ligand, and solvent, or ultrasonic wave processing the mixture to form a crystal nucleus with an organic ligand covalent-bonded with metals; and irradiating microwaves to a reaction solution including the crystal nucleus.
Abstract translation: 目的：提供一种有机 - 无机杂化纳米多孔材料的制造方法，由其制造的有机 - 无机杂化纳米多孔材料及其作为吸附剂的用途，以使用微波照射法合成纳米多孔材料。 构成：有机 - 无机杂化纳米多孔材料的制造方法包括以下步骤：搅拌二价金属离子，二羟基 - 对苯二甲酸酯有机配体和溶剂，或超声波处理该混合物以形成具有有机配体共价键的结晶核， 与金属结合; 并将微波照射到包含晶核的反应溶液中。
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