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    APPARATUS FOR FORMING COMPOSITE BUILT-UP FILM
    21.
    发明专利
    APPARATUS FOR FORMING COMPOSITE BUILT-UP FILM 失效

    公开(公告)号：JPS6393375A

    公开(公告)日：1988-04-23

    申请号：JP24025286

    申请日：1986-10-09

    Applicant: AGENCY IND SCIENCE TECHN ,  SANESU KEISOKU KK

    Inventor： NAKANISHI HACHIRO ,  OKADA SHUJI ,  MATSUDA HIROO ,  KATO MASAO ,  HARA KATSUHEI ,  ONO NOBUAKI

    IPC: H01B3/00 ,  B05C3/02 ,  B05D1/20 ,  H01L51/05 ,  H01L51/40

    Abstract: PURPOSE:To easily achieve the mass production of a precise composite built-up film, by partitioning the surface of the water in a water tank into a plurality of sections by providing a fixed plate to the water surface part of the water tank and using a lifter capable of independently supporting a film forming solid substrate in a gaseous phase and a liquid phase. CONSTITUTION:A lifter for preparing a composite built-up film is equipped with an upper arm 5 for supporting a solid substrate 10 in a gaseous phase to move left and right as well as up and down and a lower arm 6 for supporting the solid substrate 10 in a liquid phase to move left and right as well as up and down. At first, in such a state that the solid substrate 10 is mounted to the gripper 4 of the upper arm 5, A-molecules are developed on the left water surface 9-1 partitioned of a fixed plate barrier 2 of a water tank 1 and B-molecules are developed on the right water surface 9-2 and monomolecules are arranged by a movable plate barrier 3. Thereafter, the solid substrate 10 is transferred from the upper arm 5 to the lower arm 6 on the side of the left water surface 9-1 and both arms 5, 6 are rotated by 180 deg. around a support jig 7 and, now, the solid substrate 10 is transferred from the lower arm 6 to the upper arm 5 to successively build up monomolecular films A, B when passes the respective water surfaces.

    NOVEL DIACETYLENE COMPOUND POLYMERIZABLE IN SOLID PHASE
    22.
    发明专利
    NOVEL DIACETYLENE COMPOUND POLYMERIZABLE IN SOLID PHASE 失效

    公开(公告)号：JPS62255475A

    公开(公告)日：1987-11-07

    申请号：JP9595286

    申请日：1986-04-25

    Applicant: AGENCY IND SCIENCE TECHN

    Inventor： MATSUDA HIROO ,  OKADA SHUJI ,  NAKANISHI HACHIRO ,  KATO MASAO ,  HORAI SHIGERU

    IPC: C07D209/86 ,  C08F38/00 ,  G02F1/35 ,  G02F1/355 ,  G02F1/361 ,  G03F7/025

    Abstract: NEW MATERIAL:A diacetylene compound of formula I (R is hydroxymethyl, 4-hydroxybutyl or their toluenesulfonic acid ester or phenyl-carbamic acid ester). EXAMPLE:1-(N-carbazoline)-5-hydroxy-1,3-pentadiyne. USE:Useful as a monomer for forming a polymeric semiconductor crystal or a polymer crystal exhibiting singular optical characteristics. Polydiacetylene crystal has excellent electrical and optical properties. The solid-phase polymerization of the monomer can be carried out by the heating, gamma-ray irradiation, etc., of a crystal sealed in a glass tube in vacuum or in an inert gas atmosphere. PREPARATION:The compound of formula I can be produced e.g. by asymmetric coupling of N-ethynylcarbazole of formula II with a 1-bromopropyn-3-ol of formula III (n is 1 or 4).

    DIACETYLENE COMPOUND HAVING CROWN ETHER STRUCTURE AND ITS PRODUCTION
    24.
    发明专利
    DIACETYLENE COMPOUND HAVING CROWN ETHER STRUCTURE AND ITS PRODUCTION 失效

    公开(公告)号：JPH11255757A

    公开(公告)日：1999-09-21

    申请号：JP5536598

    申请日：1998-03-06

    Applicant: AGENCY IND SCIENCE TECHN ,  SHIMADA SATORU ,  MATSUDA HIROO

    Inventor： SHIMADA SATORU ,  MATSUDA HIROO ,  OKADA SHUJI ,  NAKANISHI HACHIRO

    IPC: C07D273/01 ,  G02F1/35 ,  G02F1/355 ,  G02F1/361

    Abstract: PROBLEM TO BE SOLVED: To obtain the subject new compound having crown ether structure, high in ion transfer ability, capable of solid phase polymerization, and useful as a raw material for functional materials such as electroconductive materials, electrode materials, nonlinear optical materials, photosensitive materials and semiconductor crystals. SOLUTION: This new compound is shown by the formula CH3 -(CH2 )k -C≡C- C≡C-(CH2 )m -CO- E [(k) and (m) are each 1-12; E is a structure of the formula ((n) is 1-4)], e.g. CH3 -(CH2 )11 -C≡C-C≡C-(CH2 )8 -COOH. This new compound of the above formula is obtained by reaction of a 1,3-alkadiynecarboxylic acid compound of the formula CH3 -(CH2 )k -C≡C-C≡C-(CH2 )m -COX (X is hydroxyl or a halogen) with an azacrown compound of the formula H-E pref. at 1.1-1.2 mol per mol of the 1,3-alkadiynecarboxylic acid compound in an aprotic solvent (e.g. methylene chloride, an ether compound) in an inert gas atmosphere such as argon or nitrogen under normal pressures pref. at 25-40 deg.C under agitation.

    PRODUCTION OF ORIENTED TWO-DIMENSIONAL POLYMER CRYSTAL
    28.
    发明专利
    PRODUCTION OF ORIENTED TWO-DIMENSIONAL POLYMER CRYSTAL 失效

    公开(公告)号：JPH01249830A

    公开(公告)日：1989-10-05

    申请号：JP7967388

    申请日：1988-03-31

    Applicant: AGENCY IND SCIENCE TECHN

    Inventor： MATSUDA HIROO ,  OKADA SHUJI ,  NAKANISHI HACHIRO ,  KATO MASAO ,  MICHIHASHI TAKAHISA ,  INOUE TAKAHITO ,  YATSUSE KIYOSHI ,  OKADA MASAKAZU

    IPC: C08G69/28 ,  C08F290/00 ,  C08F299/00 ,  C08G69/48

    Abstract: PURPOSE:To obtain the subject crystal having isotropically high strength, by orienting a specific alkyldiamine perpendicularly on a surface of a substrate, depositing a diamine and a diacetylenedicarboxylic acid by vacuum evaporation and irradiating with ultraviolet ray, etc., to effect the solid-phase polymerization. CONSTITUTION:(A) An alkyldimine of formula I (n is 8-18) (e.g., diaminodecane) is deposited on (B) a substrate such as polished glass plate by vacuum evaporation at a heating temperature of the component A of 30-110 deg.C, a substrate temperature of -30-10 deg.C and a vacuum degree of 10 -10 Torr. Thereafter, (C) a diamine of formula II (R is alkyl, aryl, etc.) and (D) a diacetylenedicarboxylic acid of formula III (R is alkyl, aralkyl, etc.) are deposited on the surface by vacuum evaporation, polymerized and then irradiated with ultraviolet ray or ionizing radiation (e.g., gamma-ray of cobalt 60) to effect the solid-phase polymerization and obtain the objective crystal.

    DIPHENYLDIACETYLENE DERIVATIVE
    30.
    发明专利
    DIPHENYLDIACETYLENE DERIVATIVE 失效

    公开(公告)号：JPS62255459A

    公开(公告)日：1987-11-07

    申请号：JP9595586

    申请日：1986-04-25

    Applicant: AGENCY IND SCIENCE TECHN ,  TODA KOGYO CORP

    Inventor： MATSUDA HIROO ,  OKADA SHUJI ,  NAKANISHI HACHIRO ,  KATO MASAO ,  HORAI SHIGERU ,  HORIISHI NANAO

    IPC: C08F38/00 ,  C07C67/00 ,  C07C231/00 ,  C07C233/15

    Abstract: NEW MATERIAL:A compound of formula I [either one of R1-R3 is -NHCO-(CH2)n-CH3 (n is 12-18) and the others are H]. EXAMPLE:1-(3-Nitrophenyl)-4-(2-heptadecylcarbamoylphenyl)-1,3-butadiyne. USE:Useful as a monomer of diacetylene compound for forming a nonlinear optical material, a photo-sensitive material or a polymeric semiconductor material. It is polymerizable in solid phase and is an aromatic compound having asymmetric structure and having substituent group conjugating with the triple bond of diacetylene. It has high electronic effect. PREPARATION:The compound of formula I can be produced by carrying out asymmetric coupling of 3-(bromoethynyl)nitrobenzene of formula II with an ethynylaniline of formula III (one of R1-R3 is amino and the others are H) and reacting the resultant compound of formula I (one of R1-R3 is amino and the others are H) with carboxylic acid chloride of formula IV in the presence of an amine.

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