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    23.
    发明专利
    未知

    公开(公告)号：DE19524619A1

    公开(公告)日：1997-01-09

    申请号：DE19524619

    申请日：1995-07-06

    Applicant: BASF AG

    Inventor： HENKELMANN JOCHEM DR ,  HEIDER MARC DR ,  RUEHL THOMAS DR

    IPC: C07D239/10 ,  B01J31/02 ,  C07B61/00 ,  C07C273/02 ,  C07C273/18 ,  C07C275/20

    Abstract: The prodn. of N-alkenyl ureas of formula (I) comprises reacting ureas of formula (II) with alkenyl carboxylate esters of formula (III), in which R , R = H, 1-40C alkyl, 2-40C alkenyl, 3-20C cycloalkyl, 4-20C alkyl-cycloalkyl or cycloalkyl- alkyl, or aryl, 7-20C alkaryl or 7-20C aralkyl (the last 3 opt. substd. with 1 to 5 halogen, 1-8C alkyl or 1-8C alkoxy gps.); or R + R = 2-10C alkylene (opt. substd. with 1 to 6 1-8C alkyl gps.); R , R = H or 1-8C alkyl; R = H, 1-40C alkyl, 3-20C cycloalkyl, 4-20C alkyl-cycloalkyl, aryl, 7-20C alkaryl or aralkyl, or substd. aryl or 7-20C aralkyl (with 1 to 3 1-8C alkyl gps.) The reaction is carried out at 0-180 degrees C and 0.01-10 bar in presence of a base.

    24.
    发明专利
    未知

    公开(公告)号：DE19524618A1

    公开(公告)日：1997-01-09

    申请号：DE19524618

    申请日：1995-07-06

    Applicant: BASF AG

    Inventor： HENKELMANN JOCHEM DR ,  HEIDER MARC DR ,  RUEHL THOMAS DR

    IPC: B01J31/02 ,  C07B61/00 ,  C07D233/56 ,  C07D233/58 ,  C07D235/06 ,  C07D249/08 ,  C07D521/00

    Abstract: Prepn. of N-alkenyl azoles of formula (I) is by reaction of azoles (II) with alkenyl carboxylic acid esters (III) at 0-180 degC/0.01-10 bar. The novel feature being that the reaction is in presence of a base and a quat. salt. X = CHR or N; R and R = H or 1-8C alkyl R -R = H; 1-40C alkyl; 2-40C alkenyl; 3-20C cycloalkyl; 4-20C alkylcycloalkyl or cycloalkyl-alkyl; or aryl or 7-20C alkaryl or aralkyl each opt substd up to 5 times by 1-8C alkyl or alkoxy or halogen; or R +R , R +R or R +R together form a 2-10C alkylene chain opt. substd. up to 6 times by 1-8C alkyl; and R = H; 1-40C alkyl; 3-20C cycloalkyl; 4-20C alkyl-cycloalkyl; aryl or 7-20C aralkyl, each opt. substd. up to 3 times by 1-8C alkyl; or 7-20C alkaryl.

    Silyl-alkyl, -cycloalkyl and -aryl vinyl ether(s) and thio:ether(s) prepn.
    27.
    发明专利
    Silyl-alkyl, -cycloalkyl and -aryl vinyl ether(s) and thio:ether(s) prepn. 未知

    公开(公告)号：DE19530565A1

    公开(公告)日：1996-02-29

    申请号：DE19530565

    申请日：1995-08-19

    Applicant: BASF AG

    Inventor： HEIDER MARC DR ,  HENKELMANN JOCHEM DR ,  KARCHER MICHAEL DR

    IPC: C07F7/08 ,  C07F7/18

    Abstract: In the prepn. of Si-contg. vinyl (thio)ethers (II) of formula (A; Y = -CH=CH2), by reacting Si-contg. alcohols or thiols (II) of formula (A; Y = H) with C2H2, reaction is carried out in phenyl methyl sulphoxide (PMSO), DMSO, sulpholan or hexamethylphosphoryl triamide (HMPA) in the presence of an alkali metal hydroxide: Si(R )(R )(R )-R -X-Y (A); X = O or S; R = 1-20C alkylene, 3-12C cycloalkylene or 6-10C arylene; R , R , R = H, 1-20C alkyl, 3-12C cycloalkyl, 1-12C alkoxy, phenoxy or heteroaryl or forms a 3-12C ring with R .

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