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    HYDROPHILIC-HYDROPHOBIC THERMALLY REVERSIBLE MATERIAL
    31.
    发明专利
    HYDROPHILIC-HYDROPHOBIC THERMALLY REVERSIBLE MATERIAL 失效

    公开(公告)号：JPS62277414A

    公开(公告)日：1987-12-02

    申请号：JP12049786

    申请日：1986-05-26

    Applicant: AGENCY IND SCIENCE TECHN

    Inventor： ITO SHOJI ,  MIZOGUCHI KENSAKU ,  SUDA MASAO

    IPC: B01J20/28 ,  B01D71/58 ,  B01J20/26 ,  C08F20/52 ,  C08F20/58 ,  C08L33/24

    Abstract: PURPOSE:To provide the titled material composed of an aqueous solution of a poly[N-(dimethoxyethyl)-N-methylacrylamide], reversibly taking a water-soluble state at low temperature and water-insoluble state at high temperature and useful as a light-shielding material, temperature sensor, heat-sensitive switch, toy, adsorptive separation material, etc. CONSTITUTION:The objective material is composed essentially of an aqueous solution of poly(N-(2,2-dimethoxyethyl)-N-methylacrylamide)(preferably having an intrinsic viscosity [eta] of 0.01-6.0 in methanol solution at 30 deg.C). The concentration of the aqueous solution is preferably >=0.01%.

    SELECTIVE SEPARATION PROCESS OF WATER
    33.
    发明专利
    SELECTIVE SEPARATION PROCESS OF WATER 失效

    公开(公告)号：JPS62129112A

    公开(公告)日：1987-06-11

    申请号：JP26995185

    申请日：1985-11-29

    Applicant: AGENCY IND SCIENCE TECHN

    Inventor： HIROTSU TOSHIHIRO ,  NAKAMURA EIICHIRO ,  MIZOGUCHI KENSAKU ,  SUDA MASAO

    IPC: B01D17/02

    Abstract: PURPOSE:To enhance durability and stability by preparing a hydrophilic separating membrane comprising graft polymerization of hydrophilic monomer over the surface of porous high-molecular membrane base, passing the mixed solution of water and alcohol through the said membrane and permeating water preferentially. CONSTITUTION:The graft polymerization is carried out by adding hydrophilic monomer such as acrylamide water solution, after plasma treatment, on the surface of porous high-molecular membrane such as porous polypropylene. The membrane thus prepared is washed with distilled water repeatedly to remove the unreacted monomer, homopolymer, etc., and a hydrophilic membrane is produced. The water-ethanol mixed solution is passed through the hydrophilic separating membrane thus produced, and water is permeated preferentially. Pervaporation is suitable for carrying out the said separation. Process of separation, durable and stabilized, is thus achieved.

    THERMOREVERSIBLY HYDROPHILIC AND HYDROPHOBIC POLYMER AND ITS PRODUCTION
    34.
    发明专利
    THERMOREVERSIBLY HYDROPHILIC AND HYDROPHOBIC POLYMER AND ITS PRODUCTION 失效

    公开(公告)号：JPS6291509A

    公开(公告)日：1987-04-27

    申请号：JP23077585

    申请日：1985-10-16

    Applicant: AGENCY IND SCIENCE TECHN

    Inventor： ITO SHOJI ,  MIZOGUCHI KENSAKU ,  SUDA MASAO

    IPC: C08F20/58 ,  C08F20/52 ,  C08F120/58

    Abstract: PURPOSE:To obtain the titled thermoreversible polymer which is soluble in water at low temperatures while insoluble in water at high temperatures and is suitable for temperature sensors, light-screening bodies, etc., by radical- polymerizing N-ethoxyethyl(meth)acrylamide. CONSTITUTION:The purpose thermoreversibly hydrophilic acid hydrophobic polymer of formula II (wherein n>=2) is obtained by radical-polymerizing N- ethoxyethyl(meth)acrylamide of formula I (wherein R1 is H or methyl). As a process for polymerizing this compound, a solution polymerization process is usually preferable, and one comprising dissolving the compound of formula I in a solvent (e.g., benzene) and irradiating the solution with a radiation or heating it in the presence of a radical polymerization initiator can be adopted, for example. The compound of formula I can be produced by, for example, reacting (meth)acryloyl chloride with 2-ethoxyethylamine and triethylamine in benzene.

    HIGH POLYMER CELL
    37.
    发明专利
    HIGH POLYMER CELL 失效

    公开(公告)号：JPS63168974A

    公开(公告)日：1988-07-12

    申请号：JP17787

    申请日：1987-01-06

    Applicant: AGENCY IND SCIENCE TECHN ,  NISSAN MOTOR

    Inventor： KAERIYAMA KYOJI ,  SUDA MASAO ,  SATO MASAAKI ,  OSAWA YASUHIKO ,  ISHIKAWA MASAZUMI ,  KAWAI MIKIO

    IPC: H01M4/60 ,  H01M10/05

    Abstract: PURPOSE:To restrict a side reaction with the solvent in order to stabilize a cell, and to make it possible to improve the output density, by using a conductive high polymer including triphenylamin structure units for a positive electrode, a conductive high polymer including quinoline structure units for a negative electrode, and a nitril solvent for a solvent. CONSTITUTION:A nitril-type solvent is used as a solvent, a conductive high polymer including triphenolamin structure unit, whose doped condition in the nitril-type solvent is stable, is used as a positive electrode, and a conductive high polymer including quinoline structure units, whose doped condition in the solvent is also stable, is used as a negative electrode. In such a composition, since a side reaction with the solvent is restricted, and the cell is stabilized without generating a gas and the like, the cell can be made maintenance-free. Furthermore, a high polymer cell whose output density is larger compared with a lithium negative electrode and the like can be produced.

    NOVEL THIOPHENE POLYMER, ITS PRODUCTION AND ORGANIC DISPLAY MATERIAL MADE THEREFROM
    38.
    发明专利
    NOVEL THIOPHENE POLYMER, ITS PRODUCTION AND ORGANIC DISPLAY MATERIAL MADE THEREFROM 失效

    公开(公告)号：JPS63161024A

    公开(公告)日：1988-07-04

    申请号：JP30798586

    申请日：1986-12-25

    Applicant: AGENCY IND SCIENCE TECHN ,  SHINTO PAINT CO LTD

    Inventor： TANAKA SUSUMU ,  KAERIYAMA KYOJI ,  SUDA MASAO ,  MITSUHARA TOSHIO

    IPC: C08G75/00 ,  C08G61/10 ,  C08G61/12 ,  C09K11/06

    Abstract: PURPOSE:To obtain the titled polymer useful as a display material developing green color and having excellent memory effect, by electrolytic polymerization of a thiophene compound having a specific structural formula. CONSTITUTION:The objective polymer consisting of the recurring unit of formula can be produced by the electrolytic polymerization of a compound of formula I [R is 1,3-phenylene, p,p'-diphenylene or (substituted)1,3-phenylene] [e.g. 1,3-di(2- thienyl)-benzene]. The polymerization is carried out generally in a polar solvent such as acetonitrile in an inert atmosphere in the presence of a supporting electrolyte (e.g. tetrafluoroboric acid tetramethyl ammonium salt). The polymer is obtained in a state doped with the anion of the supporting electrolyte.

    PALLADIUM-QUATERNARY AMMONIUM COMPOUND ADDUCT
    39.
    发明专利
    PALLADIUM-QUATERNARY AMMONIUM COMPOUND ADDUCT 失效

    公开(公告)号：JPS63101349A

    公开(公告)日：1988-05-06

    申请号：JP24856586

    申请日：1986-10-17

    Applicant: AGENCY IND SCIENCE TECHN

    Inventor： NAKAO YUKIMICHI ,  KAERIYAMA KYOJI ,  SUDA MASAO

    IPC: B01J23/44 ,  C07B61/00 ,  C07C211/63 ,  C07D213/20 ,  C07F15/00

    Abstract: NEW MATERIAL:A palladium-quaternary ammonium compound adduct expressed by formula I (RidenticalN is trilower alkylamino or pyridyl; R' is 6-22C alkyl; X is halogen). EXAMPLE:A compound expressed by formula II. USE:Useful for producing highly active palladium catalysts, the purpose of forming palladium coating layers on solids or adsorbing the palladium catalysts on porous carriers, etc., capable of forming solutions by dissolving in organic solvents and directly usable or depositing as metal by coating, drying the solutions and reducing the dried film with a reducing agent. PREPARATION:A water-soluble palladium complex compound is dissolved in water and an aqueous solution of a cationic surfactant expressed by formula II (Y is a group forming anion, e.g. halogen, methylsulfuric acid) is added and reacted therewith. The formed precipitates are separated by filtration, extraction, etc., to afford the aimed compound expressed by formula I.

    OPTICAL ELEMENT
    40.
    发明专利
    OPTICAL ELEMENT 失效

    公开(公告)号：JPS6344638A

    公开(公告)日：1988-02-25

    申请号：JP18983486

    申请日：1986-08-13

    Applicant: AGENCY IND SCIENCE TECHN

    Inventor： ITO SHOJI ,  MIZOGUCHI KENSAKU ,  SUDA MASAO

    IPC: G02F1/19

    Abstract: PURPOSE:To obtain a distinct image having high contrast and high resolution by sandwiching a soln. consisting of three components; a solvent, N-substd. acrylamide polymer are polyvinyl pyrolidone or PE glycol as a high-polymer dispersion stabilizer between a pair of substrates formed with heating elements on the surfaces. CONSTITUTION:This element has the substrate 1, a polymer liquid layer 2, a transparent protective plate 3 and an IR absorption layer 8 corresponding to the heating element. The polymer liquid layer 2 is the liquid layer consisting of the soln. contg. the N-substd. acrylamide polymer, for which; for example, the polymers obtainable from monomers such as N-isopropylacrylamide or N-isopropyl methacrylamide or the copolymers thereof or the copolymers essentially consisting thereof, etc., are adequate. Polyvinyl pyrolidone, PE glycol, etc., are adequate as the high-polymer dispersion stabilizer to be used.

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