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    3-AMINOMETHYL-1-CYCLOHEXYLAMIN UND EIN VERFAHREN ZU DESSEN HERSTELLUNG
    34.
    发明公开
    3-AMINOMETHYL-1-CYCLOHEXYLAMIN UND EIN VERFAHREN ZU DESSEN HERSTELLUNG 审中-公开

    公开(公告)号：EP2310354A2

    公开(公告)日：2011-04-20

    申请号：EP09780486.8

    申请日：2009-07-13

    Applicant: BASF SE

    Inventor： ERNST, Martin ,  DAHMEN, Kirsten ,  OFTRING, Alfred

    IPC: C07C211/36

    CPC classification number: C07C211/36 ,  C07B2200/09 ,  C07C2601/14

    Abstract: The invention relates to 3-aminomethyl-1-cyclohexylamine and a method for the production thereof by a) reacting cyclohexenone with hydrogen cyanide in the presence of a basic catalyst, b) reacting the cyclohexanone nitrile obtained in step a) with ammonia in the presence of an imine-forming catalyst, and c) reacting the reaction mixture that is obtained in step b) and contains 3-cyanocyclohexylimine with hydrogen and ammonia on hydrogenation catalysts. The invention further relates to the use of 3-aminomethyl-1-cyclohexylamine as a curing agent for epoxy resins, as an intermediate product when producing diisocyanates, as an initiator entity when producing polyetherols, and/or as a monomer for producing polyamides.

    Abstract translation: 本发明涉及3-氨基甲基-1-环己基胺及其制备方法，其通过以下步骤a）在碱性催化剂存在下使环己烯酮与氰化氢反应，b）在步骤a）中获得的环己腈与氨在存在下反应 的亚胺形成催化剂，和c）使步骤b）中获得的含3-氰基环己基亚胺的反应混合物与氢气和氨在氢化催化剂上反应。 本发明还涉及3-氨基甲基-1-环己胺作为环氧树脂的硬化剂的用途，作为制备二异氰酸酯的中间体，作为制备聚乙烯醇和/或聚酰胺制备单体的起始物。

    VERFAHREN ZUR HERSTELLUNG VON AMINODICARBONSÄURE-N,N-DIESSIGSÄUREN
    35.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON AMINODICARBONSÄURE-N,N-DIESSIGSÄUREN 有权
    VERFAHREN ZUR HERSTELLUNG VONAMINODICARBONSÄURE-N，N-DIESSIGSÄUREN

    公开(公告)号：EP2262760A1

    公开(公告)日：2010-12-22

    申请号：EP09716225.9

    申请日：2009-03-02

    Applicant: BASF SE

    Inventor： OFTRING, Alfred ,  STAMM, Armin ,  WIRSING, Friedrich ,  BRAUN, Gerold

    IPC: C07C227/26 ,  C07C229/24

    CPC classification number: C07C227/18 ,  C07C229/24

    Abstract: The present invention relates to a method for the production of aminodicarboxylic acid-N,N,diacetic acids of the general Formula I, wherein X independently of one another represents hydrogen or an alkali metal and n represents a number 1 or 2. Furthermore, the invention relates to aminodicarboxylic acid-N,N-diacetic acids of high purity. The inventive method comprises the following steps: A.) reacting an aminodicarboxylic acid of the general Formula II, wherein X and n have the aforementioned meanings, with 0.8 to 1.2 mole equivalents of formaldehyde and with 0.8 to 1.2 mole equivalents of hydrocyanic acid; b) reacting the reaction products of step a) with 0.8 to 1.2 mole equivalents of hydrocyanic acid and with 0.8 to 1.2 mole equivalents of formaldehyde; c) hydrolyzing in the reaction product obtained in step b).

    Abstract translation: 提供了制备式（I）的氨基二羧酸N，N-二乙酸的方法，其中X独立地为氢或碱金属，n为1或2.具有高纯度的氨基二羧酸-N，N-二乙酸 可以产生。 该方法包括：a）使氨基二羧酸与0.8至1.2摩尔当量的甲醛和0.8至1.2摩尔当量的氢氰酸反应; b）使a）的反应产物与0.8至1.2摩尔当量的氢氰酸和0.8至1.2摩尔当量的甲醛反应; c）在b）中得到的反应产物中水解。

    VERFAHREN ZUR HERSTELLUNG VON ETHYLENAMINEN AUS ROH-AAN
    37.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON ETHYLENAMINEN AUS ROH-AAN 审中-公开
    工艺生产乙烯胺的FROM ROH-AAN

    公开(公告)号：EP2132163A1

    公开(公告)日：2009-12-16

    申请号：EP08717206.0

    申请日：2008-02-28

    Applicant: BASF SE

    Inventor： DAHMEN, Kirsten ,  OFTRING, Alfred ,  HUGO, Randolf ,  HAHN, Thilo ,  BAUMANN, Katrin ,  MELDER, Johann-Peter

    IPC: C07C209/48 ,  C07C211/10

    CPC classification number: C07C209/48 ,  C07C211/10

    Abstract: The invention relates to a method for producing an ethyleneamine mixture, comprising the following steps: a) untreated AAN, which is substantially devoid of formaldehyde cyanohydrin (FACH), is heated to a temperature of between 50 and 150°C to obtain an aminonitrile mixture containing amino acetonitrile (AAN) and between 5 and 70 % by weight of iminodiacetonitrile (IDAN); b) the aminonitrile mixture obtained in step a) is hydrogenated in the presence of a catalyst. Ethylenediamine (EDA) and/or diethylenetriamine (DETA) and optionally other ethyleneamines can be isolated from the ethyleneamine mixtures thus obtained.

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