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公开(公告)号:DE59206479D1
公开(公告)日:1996-07-11
申请号:DE59206479
申请日:1992-09-17
Applicant: BASF AG
Inventor: DEGEN HELMUT , ZIMMERMANN NORBERT , BRUECKMANN RALF DR , LAMM GUNTHER DR , LANGE ARNO DR , REICHELT HELMUT DR
IPC: B01J27/125 , B01J27/128 , C07B61/00 , C07C201/12 , C07C205/45 , C09B29/01 , C09B29/36 , C09B29/42 , C09B67/00 , C09B67/48
Abstract: Process for the preparation of nitrobenzophenones by reaction of benzene or its derivatives with nitrobenzoyl chloride in the presence of a Lewis acid, a colour-fast modification of 1,4-dimethyl-5-cyano-3-[4-(2,4-dimethylbenzoyl)phenylazo]-2-hydroxy-py rid-6-one, and its use for dyeing or printing synthetic fibre material.
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公开(公告)号:DE59206360D1
公开(公告)日:1996-06-27
申请号:DE59206360
申请日:1992-11-12
Applicant: BASF AG
Inventor: HANSEN GUENTER DR , LAMM GUNTHER DR , LOEFFLER HERMANN , REICHELT HELMUT DR , DEGEN HELMUT , LANGE ARNO DR , GRUND CLEMENS DR
IPC: C09B29/00 , C09B29/033 , C09B29/42 , D06P1/18 , D06P3/54
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公开(公告)号:DE4142192C2
公开(公告)日:1996-02-29
申请号:DE4142192
申请日:1991-12-20
Applicant: BASF AG
Inventor: LAMM GUNTHER DR , LOEFFLER HERMANN , REICHELT HELMUT DR
IPC: C07D213/74 , C07D213/84 , C07D213/85 , C07D405/12
Abstract: PCT No. PCT/EP93/00538 Sec. 371 Date Jun. 17, 1994 Sec. 102(e) Date Jun. 17, 1994 PCT Filed Mar. 10, 1993 PCT Pub. No. WO94/20469 PCT Pub. Date Sep. 15, 1994.A process for preparing diaminopyridines of the formula where one of the two radicals X1 and X2 is hydrogen, C1-C4-alkyl, halogen or nitro and the other is cyano, R1 is hydrogen, C1-C4-alkyl or phenyl, R2 and R3 are each hydrogen, C1-C4-alkyl or C1-C4-alkoxy, R4 is hydrogen or C1-C4-alkyl, and R5 is optionally substituted C1-C10-alkyl, C3-C4-alkenyl or C5-C7-cycloalkyl, by reacting dichloropyridines of the formula (II) in a first step with an amine of the formula R5-NH2 at from 10 DEG to 80 DEG C. in the presence of a base and of an inert organic diluent and/or water, then removing the diluent and thereafter, with or without prior intermediate isolation of the reaction product, comprises carrying out the second step in a melt at from 90 DEG to 165 DEG C. and at a pH from 3.5 to 6.5 using from 1.3 to 3 mol of aniline IV are used per mole of dichloropyridine II.
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公开(公告)号:DE4416266A1
公开(公告)日:1995-11-09
申请号:DE4416266
申请日:1994-05-07
Applicant: BASF AG
Inventor: LAMM GUNTHER DR , REICHELT HELMUT DR , WIESENFELDT MATTHIAS DR
IPC: C07D213/71 , C09B33/12 , C09B33/28 , D06P1/39 , C07D213/85 , C07D413/10 , C07D417/08 , C07D521/00
Abstract: Bis(5-azo-6-hydroxy-4-methyl-3-hydroxysulphonyl-pyrid-2-on- 1-yl) dyes (I) of formula (A), in the form of free acids or their salts, are claimed. In A, A and Y are each -SO3H; Z is D-N=N-; D is the residue of a diazo component; and X is a 2-8 C alkylene opt. with an ether O atom in the chain. Also claimed are bis(6-hydroxy-4-methy-3-hydroxysulphonyl-pyrid-2-on-1-yl) cpds. (II) of formula (A), in which Y is -SO3H and Z is H, in the form of the free acids or salts, and the prepn. of (II).
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公开(公告)号:DE58908357D1
公开(公告)日:1994-10-20
申请号:DE58908357
申请日:1989-09-29
Applicant: BASF AG
Inventor: HANSEN GUENTER DR , LAMM GUNTHER DR , REICHELT HELMUT DR , SCHEFCZIK ERNST DR
IPC: C09B29/042 , C09B29/00 , C09B29/048 , C09B29/36 , D06P1/18
Abstract: Thiazole azo dyes of the formula … … in which… X is nitrogen or the radical C-R where R is cyano, halogen, alkoxycarbonyl or thiocyanato,… R is cyano, chlorine, optionally substituted C1-C6-alkyl, optionally substituted phenyl, optionally substituted thienyl, optionally substituted pyridyl or optionally substituted alkylthio-, -sulphinyl- or -sulphonyl,… R is optionally substituted alkyl, cycloalkyl, optionally substituted phenyl, furyl, optionally substituted thienyl or pyridyl and… R and R are, independently of one another, optionally substituted alkyl or R and R together with the nitrogen atom connecting them are a heterocyclic radical, and the use of these dyes for colouring textile fibres.
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公开(公告)号:DE4207745A1
公开(公告)日:1993-09-16
申请号:DE4207745
申请日:1992-03-11
Applicant: BASF AG
Inventor: LAUTH GUENTER DR , HOELDERICH WOLFGANG DR , WAGENBLAST GERHARD DR , ALBERT BERNHARD DR , LAMM GUNTHER DR , REICHELT HELMUT DR , GRUND CLEMENS DR , GRUETTNER-MERTEN SABINE DR
IPC: C01B25/36 , C01B25/45 , C01B33/26 , C01B37/04 , C01B37/06 , C01B37/08 , C01B39/00 , C01B39/02 , C09B63/00 , C09D7/00
Abstract: Crystalline molecular sieves containing one or more chromophores of the mono or polyazo dye class having no acid groups, and their use as colorants.
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公开(公告)号:DE4142696A1
公开(公告)日:1993-07-01
申请号:DE4142696
申请日:1991-12-21
Applicant: BASF AG
Inventor: LAMM GUNTHER DR , MAYER UDO DR , REICHELT HELMUT DR , ZEIDLER GEORG
Abstract: Polyazo dyes of the formula in free form or as the copper, chromium, iron, cobalt or nickel complex, where p denotes 1 or 2 and q denotes 0 or 1, and R , R , R , R , R , R , R , R , X , X and the rings A and B in each case have the meaning mentioned in the description, and the use of the novel polyazo dyes for dyeing leather.
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公开(公告)号:DE3780076D1
公开(公告)日:1992-08-06
申请号:DE3780076
申请日:1987-04-28
Applicant: BASF AG
Inventor: DEHNERT JOHANNES DR , LAMM GUNTHER DR , LOEFFLER HERMANN
IPC: C07D213/85 , C07D409/12 , C07D417/12 , C09B29/00 , C09B29/036 , C09B29/34 , C09B29/36 , C09B29/42
Abstract: Benzene (1-azo-5), 3-cyanothiophen (2-azo-5), 4-cyano-isothiazole (5-azo-5) and 5-nitro-, 5-alkoxycarbonyl-, 5-cyano- or 5-formyl-thiazole (2-azo-5) 6-amino- 2-acyloxy(alkoxy) alkylamino-4-methyl- 3-cyano-pyridine cpds. of formula (I), and Benzene (1-azo-5), 4-cyano-isothiazole (5-azo-5) and 2-(m)ethoxycarbonyl- 3-methyl- 4-cyano- thiophen (5-azo-5) 2(6)-amino- 6(2)-hydroxyalkoxyalkylamino or -acyloxyalkoxyalkylamino- 4-methyl- 3-cyano- pyridine cpds. of formula (II) are new. In the formulae, D = a substd. benzene, 3-cyano-thiophen, 4-cyano-isothiazole or substd. thiazole gp. of formulae (a-d); D1 = a substd. benzene, 4-cyano- isothiazole or 2-(m)ethoxycarbonyl -3-methyl-4-cyano -thiophen gp. of formulae (e-q); R1 = H, 1-4C alkyl, 1-4C alkoxy, 2-4C alkyl or 1-8C acyloxy-2-4C-alkyl; R2 = alkylene, opt. with O in the chain; T = the radical of a 1-8C aliphatic monocarboxylic acid; B1 = 1-4C alkyl or a phenyl or benzyl gp., opt. substd. by Me, MeO or Cl; B2 = B1, halogen, CN or 1-5C alkoxycarbonyl; X = H, NO2, CN, 1-9C-alkoxy- or -alkylaminocarbonyl, CF3 or (m)ethylsulphonyl; X2 = NO2 or 1-5C alkoxycarbonyl; X3 = X2, CN or formyl; Y = H, Cl, Br, Me, MeO or EtO; Z = H, Cl, Br, CN or 1-9C alkoxycarbonyl; at least one of X, Y and Z not = H; in (II), e.g. one of A1 and A2 = R3-OH or R3-OT1 and the other = H; R3 = C2H4OC2H4, (CH2)3O(CH2)3 or (CH2)3O(CH2)4; T1 = the radical of a 1-4C aliphatic monocarboxylic acid; X4 = NO2, CN or (m)ethylsulphonyl; Y2 = H, Cl or Br; Z2 = H, CN or 1-5C alkoxycarbonyl; B3 = 1-3C alkyl, benzyl or phenyl; R4 = Me or Et.
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公开(公告)号:DE4018067A1
公开(公告)日:1991-12-12
申请号:DE4018067
申请日:1990-06-06
Applicant: BASF AG
Inventor: SENS RUEDIGER DR , REICHELT HELMUT DR , GRUETTNER SABINE DR , ETZBACH KARL-HEINZ DR , LAMM GUNTHER DR
Abstract: Use of azo dyes I for thermal transfer printing, in which the substituents have the following meaning: X is a radical IIa or IIb where R is H; C1-C6-alkyl or phenyl which can carry C1-C4-alkyl, C1-C2-alkoxy, chlorine, bromine or cyano as substituents; R is H; C1-C4-alkyl, C1-C4-alkoxy, chlorine or bromine; n is 1 or 2; K is the radical of a coupling component II H-K III from the aniline, aminonaphthaline, pyrazole, diaminopyridine, hydroxypyridone or tetrahydroquinoline series.
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公开(公告)号:DE3929698A1
公开(公告)日:1991-03-14
申请号:DE3929698
申请日:1989-09-07
Applicant: BASF AG
Inventor: SENS RUEDIGER DR , SCHEFCZIK ERNST DR , ETZBACH KARL-HEINZ DR , LAMM GUNTHER DR , REICHELT HELMUT DR , WIESENFELDT MATTHIAS DR
IPC: C09B26/02 , B41M5/26 , B41M5/385 , B41M5/388 , B41M5/39 , C07D471/04 , C09B23/00 , C09B23/04 , C09B23/16 , C09B53/00 , C09B55/00 , C09B57/00 , D06P5/00 , D06P5/13
Abstract: Triazolopyridine dyes useful for thermal transfer of methine dyes have the formula (I) where R1 is C1-C20-alkyl, which may be substituted and interrupted by one or more oxygen atoms, or is substituted or unsubstituted phenyl or hydroxyl, R2 is a 5- or 6-membered carbocyclic or heterocyclic ring which may be substituted and benzofused, R3 is cyano, carbamoyl, carboxyl or C1-C4-alkoxycarbonyl, R4 is oxygen or a radical of the formula where L1 is in each case C1-C6-alkyl which may be interrupted by 1 or 2 oxygen atoms, and X is CH or nitrogen.
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