84.
    发明专利
    未知

    公开(公告)号:DE59200949D1

    公开(公告)日:1995-01-26

    申请号:DE59200949

    申请日:1992-05-29

    Applicant: BASF AG

    Abstract: Process for the preparation of I acid urea of the formula in which 7-amino-4-hydroxynaphthalene-2-sulphonic acid (I acid) is subjected to partial reaction with urea in an inert solvent at a temperature from 100 to 140 DEG C and a pressure from atmospheric pressure to 10 bar, unreacted I acid is precipitated in an acidic medium and removed, and, if appropriate, I acid urea is separated from the resulting neutralised solution by adding salt.

    87.
    发明专利
    未知

    公开(公告)号:DE4211782A1

    公开(公告)日:1993-10-14

    申请号:DE4211782

    申请日:1992-04-08

    Applicant: BASF AG

    Abstract: Method of preparing di- or triarylmethane dyes by oxidation of di- or triarylmethanes in the presence of a diluent and of an oxygen-transferring catalyst which contains a complexed heavy metal ion, or of a catalyst based on molybdenic acid and vanadium compounds, wherein the oxidising agent used is peroxomonosulphuric acid or salts thereof.

    88.
    发明专利
    未知

    公开(公告)号:DE59001835D1

    公开(公告)日:1993-07-29

    申请号:DE59001835

    申请日:1990-04-24

    Applicant: BASF AG

    Abstract: 3-Aminophenylpentane-1,5-diones of the formula I (I) where R1 and R2 are, independently of one another, hydrogen, C1-C8-alkyl, C4-C8-cycloalkyl, cyano-C2-C4-alkyl, hydroxy-C2-C4-alkyl, chloro-C2-C4-alkyl, phenyl-C1-C2-alkyl which can be substituted by chlorine, or phenyl which can be substituted by clorine or methyl, or R1 and R2 form, together with the nitrogen to which they are bonded, a heterocyclic radical which can contain further hetero atoms, R3 is hydrogen, fluorine, chlorine, C1-C2-alkyl or C2-C5-alkoxy or, if R3 is ortho to -NRR2, R3 and R2 together form C2-C4-alkylene, which can be substituted, or 1,2-phenylene and A is naphthyl or a radical of the formula II (II) where X is hydrogen, fluorine, chlorine, bromine, C1-C5-alkyl, hydroxyl, C1-C5-alkoxy, phenoxy, phenyl-C1-C2-alkoxy, cyano or phenyl and n is 1 or 2, with the proviso that R1 and R2 are not both methyl when A is phenyl, are described.

    90.
    发明专利
    未知

    公开(公告)号:DE3866520D1

    公开(公告)日:1992-01-09

    申请号:DE3866520

    申请日:1988-11-14

    Applicant: BASF AG

    Abstract: 62 New polyethylene-imine-contg. azo-dyestuffs are claimed ((D-N=N-K-)yX-)mP (I) (P=polyethylene-imine) where D is an aromatic or heteroaromatic gp. with no sulphonic acid gp. the diazo-component, and K the coupling component, a naphthol, aminopyridine or pyrazolone contg. at most one sulphonic acid gp., or a deriv. of aceto-acetic acid; y=1 or 2; X, if y=1 can be a covalent bond or a bridging gp., or, if y=2, a bridging gp. e.g. X=(II) where q=0-4; (III) where R7=H, CH3; (IV) where R8= mono- or dialloylamino, alkoxy 1-4C halogen, or a further diazo component.

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