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    PREPARATION OF (METH)ACROLEIN AND/OR (METH)ACRYLIC ACID BY HETEROGENEOUSLY CATALYZED PARTIAL OXIDATION OF C3 AND/OR C4 PRECURSOR COMPOUNDS IN A REACTOR HAVING THERMOPLATE MODULES
    1.
    发明专利
    PREPARATION OF (METH)ACROLEIN AND/OR (METH)ACRYLIC ACID BY HETEROGENEOUSLY CATALYZED PARTIAL OXIDATION OF C3 AND/OR C4 PRECURSOR COMPOUNDS IN A REACTOR HAVING THERMOPLATE MODULES 未知

    公开(公告)号：MY137914A

    公开(公告)日：2009-03-31

    申请号：MYPI20042961

    申请日：2004-07-23

    Applicant: BASF AG

    Inventor： OLBERT GERHARD ,  HECHLER CLAUS DR

    IPC: B01J19/24 ,  C07C45/35 ,  C07C51/215 ,  C07C51/25

    Abstract: A PROCESS IS PROPOSED FOR PARTIAL OXIDATION IN THE GAS PHASE OF C3 AND/OR C4 PRECURSOR COMPOUNDS TO (METH) ACROLEIN AND/OR (METH) ACRYLIC ACID IN THE PRESENCE OF A HETEROGENEOUS PARTICULATE CATALYST IN A REACTOR HAVING - ONE OR MORE CUBOIDAL THERMOPLATE MODULES (1) WHICH ARE EACH FORMED FROM TWO OR MORE RECTANGULAR THERMOPLATES (2) ARRANGED PARALLEL TO EACH OTHER WHILE IN EACH CASE LEAVING A GAP (3) WHICH CAN BE FILLED WITH THE HETEROGENOUS PARTICULATE CATALYST AND IS FLOWED THROUGH BY THE FLUID REACTION MIXTURE; THE HEAT OF REACTION BEING ABSORBED BY A HEAT CARRIER WHICH FLOWS THROUGH THE THERMOPLATES (2) AND THUS AT LEAST PARTLY EVAPORATING, AND ALSO HAVING- A PREDOMINANTLY CYLINDRICAL SHELL (4,15,16) WHICH RELEASES THE PRESSURE AT THE THERMOPLATE MODULES, COMPLETELY SURROUNDS THEM AND COMPRISES A CYLINDER JACKET (4) AND HOODS (15,16) WHICHS EAL IT AT BOTH ENDS AND WHOSE LONGITUDINAL AXIS IS ALIGNED PARALLEL TO THE PLANE OF THE THERMOPLATES (2), AND ALSO HAVING - ONE OR MORE SEALING ELEMENTS (7,23) WHICH ARE ARRANGED IN SUCH A WAY THAT THE FLUID REACTION MIXTURE, APART FROM FLOWING THROUGH THE REACTOR INTERIOR SPACES BOUNDED BY THE HOODS (15,16) , ONLY FLOWS THROUGH THE GAP (3).FIGURE 1

    3.
    发明专利
    未知

    公开(公告)号：DE4205471A1

    公开(公告)日：1993-08-26

    申请号：DE4205471

    申请日：1992-02-22

    Applicant: BASF AG

    Inventor： GOSCH HANS-JUERGEN DR ,  RUST HARALD ,  FISCHER ROLF DR ,  HECHLER CLAUS DR ,  PINKOS ROLF DR

    IPC: C07C29/80 ,  C07C29/82 ,  C07C31/20

    Abstract: A process for isolating 1,4-butanediol from mixtures obtained by catalytic hydrogenation of maleic acid esters, fumaric acid esters and/or succinic acid esters, which in addition to 1,4-butanediol contain tetrahydrofuran, water, C1-C4-alcohols, succinic acid diesters, hydroxybutyric acid esters, succinic acid alkyl hydroxyalkyl esters, gamma-butyrolactone and butyric acid esters.

    6.
    发明专利
    未知

    公开(公告)号：ES2052287T3

    公开(公告)日：1994-07-01

    申请号：ES91101832

    申请日：1991-02-09

    Applicant: BASF AG

    Inventor： STABEL UWE DR ,  GOSCH HANS-JUERGEN DR ,  FISCHER ROLF DR ,  HARDER WOLFGANG DR ,  HECHLER CLAUS DR

    IPC: B01J21/16 ,  C07B61/00 ,  C07B63/04 ,  C07D307/08

    Abstract: A process is claimed for the prodn of THF from mixts (I) contg THF, butane-1,4-diol (II), gamma-butyrolactone (III), succinate esters and alcohols, which are obtd by the catalytic hydrogenation of maleic, succinic or fumaric acid, or esters thereof, or maleic or succinic anhydride, in the presence of alcohols; the process comprises distn of the THF, alcohols and water, heating the residue at 100-250 deg C in the presence of a layer silicate (IV), distn of the THF and water formed in the reaction, and sepn of THF from the distillate. More specifically, (I) are produced by hydrogenation of maleic anhydride (MA) in the presence of butanols, and contain THF, butanol, propanol, (II), (III), dibutyl succinate (V) and water; distn of (I) before treatment with (IV) gives THF, propanol, butanol and water; traces of catalyst components are removed from the mixt before treatment with (IV).

    PROCESS FOR PREPARING PHTHALIC ANHYDRIDE
    7.
    发明专利
    PROCESS FOR PREPARING PHTHALIC ANHYDRIDE 未知

    公开(公告)号：MY140990A

    公开(公告)日：2010-02-12

    申请号：MYPI20056087

    申请日：2005-12-21

    Applicant: BASF AG

    Inventor： HECHLER CLAUS DR ,  OLBERT GERHARD

    IPC: C07C51/265

    Abstract: A PROCESS IS PROPOSED FOR PREPARING PHTHALIC ANHYDRIDE BY CATALYTIC PARTIAL OXIDATION OF OXYLENE AND/OR NAPHTHALENE WITH A GAS COMPRISING OXYGEN IN A PLANT COMPRISING -TWO OR MORE REACTION ZONES COOLED WITH A COOLANT, -ONE OR MORE DEVICES ARRANGED BETWEEN THE REACTION ZONES FOR INTERMEDIATE COOLING OF THE REACTION MIXTURE BETWEEN THE REACTION ZONES, THE TEMPERATURE OF THE COOLANT ON ENTRY INTO THE SECOND OR INTO THE FURTHER REACTION ZONES DECREASING COMPARED TO THE TEMPERATURE OF THE COOLANT ON ENTRY INTO THE FIRST REACTION ZONE, WHEREIN THE TEMPERATURE OF THE COOLANT ON ENTRY INTO THE FIRST REACTION ZONE IS MORE THAN 20º HIGHER THAN THE TEMPERATURE OF THE COOLANT ON ENTRY INTO THE SECOND OR INTO THE FURTHER REACTION ZONES.

    8.
    发明专利
    未知

    公开(公告)号：ES2086142T3

    公开(公告)日：1996-06-16

    申请号：ES93101992

    申请日：1993-02-09

    Applicant: BASF AG

    Inventor： GOSCH HANS-JURGEN DR ,  RUST HARALD ,  FISCHER ROLF DR ,  HECHLER CLAUS DR ,  PINKOS ROLF DR

    IPC: C07C29/80 ,  C07C29/82 ,  C07C31/20

    Abstract: A process for isolating 1,4-butanediol from mixtures obtained by catalytic hydrogenation of maleic acid esters, fumaric acid esters and/or succinic acid esters, which in addition to 1,4-butanediol contain tetrahydrofuran, water, C1-C4-alcohols, succinic acid diesters, hydroxybutyric acid esters, succinic acid alkyl hydroxyalkyl esters, gamma-butyrolactone and butyric acid esters.

    9.
    发明专利
    未知

    公开(公告)号：DE59101524D1

    公开(公告)日：1994-06-09

    申请号：DE59101524

    申请日：1991-02-09

    Applicant: BASF AG

    Inventor： STABEL UWE DR ,  GOSCH HANS-JUERGEN DR ,  FISCHER ROLF DR ,  HARDER WOLFGANG DR ,  HECHLER CLAUS DR

    IPC: B01J21/16 ,  C07B61/00 ,  C07B63/04 ,  C07D307/08

    Abstract: A process is claimed for the prodn of THF from mixts (I) contg THF, butane-1,4-diol (II), gamma-butyrolactone (III), succinate esters and alcohols, which are obtd by the catalytic hydrogenation of maleic, succinic or fumaric acid, or esters thereof, or maleic or succinic anhydride, in the presence of alcohols; the process comprises distn of the THF, alcohols and water, heating the residue at 100-250 deg C in the presence of a layer silicate (IV), distn of the THF and water formed in the reaction, and sepn of THF from the distillate. More specifically, (I) are produced by hydrogenation of maleic anhydride (MA) in the presence of butanols, and contain THF, butanol, propanol, (II), (III), dibutyl succinate (V) and water; distn of (I) before treatment with (IV) gives THF, propanol, butanol and water; traces of catalyst components are removed from the mixt before treatment with (IV).

    REACTOR FOR PARTIAL OXIDATIONS HAVING THERMOPLATE MODULES
    10.
    发明专利
    REACTOR FOR PARTIAL OXIDATIONS HAVING THERMOPLATE MODULES 未知

    公开(公告)号：MY150013A

    公开(公告)日：2013-11-15

    申请号：MYPI20042960

    申请日：2004-07-23

    Applicant: BASF AG

    Inventor： OLBERT GERHARD ,  HECHLER CLAUS DR

    IPC: B01J19/00 ,  B01J19/24 ,  B01J19/32 ,  C07C45/35 ,  C07C51/215 ,  C07C51/25 ,  F28D9/00 ,  F28F9/00

    Abstract: A REACTOR IS PROPOSED FOR PARTIAL OXIDATIONS OF A FLUID REACTION MIXTURE IN THE PRESENCE OF A HETEROGENEOUS PATRICULATE CATALYST, COMPRISING ONE OR MORE CUBOIDAL THERMOPLATE MODULES (1) WHICH ARE EACH FORMED FROM TWO OR MORE RECTANGULAR THERMOPLATES (2) ARRANGED PARALLEL TO EACH OTHER WHILE IN EACH CASE LEAVING A GAP (3) WHICH CAN BE FILLED WITH THE HETEROGENEOUS PARTICULATE CATALYST AND IS FLOWED THROUGH BY THE FLUID REACTION MIXTURE; THE HEAT OF REACTION BEING ABSORBED BY A HEAT CARRIER WHICH FLOWS THROUGH THE THERMOPLATES (2) AND THUS AT LEAST PARTLY EVAPORATES, AND ALSO HAVING A PREDOMINANTLY CYLINDRICAL SHELL (4,15,16) WHICH RELEASES THE PRESSURE AT THE THERMOPLATE MODULES, COMPLETELY SURROUNDS THEM AND COMPRISES A CYLINDER JACKET (4) AND HOODS (15,16) WHICH SEAL IT AT BOTH ENDS AND WHOSE LONGITUDINAL AXIS IS ALIGNED PARALLEL TO THE PLANE OF THE THERMOPLATES (2), AND ALSO HAVING ONE OR MORE SEALING ELEMENTS (7, 23) WHICH ARE ARRANGED IN SUCH A WAY THAT THE FLUID REACTION MIXTURE, APART FROM FLOWING THROUGH THE REACTOR INTERIOR SPACES BOUNDED BY THE HOODS (15,16), ONLY FLOWS THROUGH THE GAP (3).

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