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    Method for producing e-oxime ether of phenylglyoxylic ester
    1.
    发明专利
    Method for producing e-oxime ether of phenylglyoxylic ester 审中-公开
    用于生产苯氧基酯的E型氧化物的方法

    公开(公告)号：JP2003002867A

    公开(公告)日：2003-01-08

    申请号：JP2002143979

    申请日：2002-05-20

    Applicant: Basf Ag ,  ビーエーエスエフ アクチェンゲゼルシャフト

    Inventor： ISAK HEINZ ,  KEIL MICHAEL ,  WOLF BERND ,  WINGERT HORST

    IPC: C07C67/313 ,  C07B61/00 ,  C07C59/68 ,  C07C59/84 ,  C07C67/31 ,  C07C69/708 ,  C07C69/716 ,  C07C249/04 ,  C07C249/08 ,  C07C249/12 ,  C07C251/48

    CPC classification number: C07C251/48

    Abstract: PROBLEM TO BE SOLVED: To provide a method for easily producing an E-oxime ether isomer of a phenylglyoxylic ester.
    SOLUTION: The method for producing the E-oxime ether represented by formula (I) (wherein, X and Y are each a halogen, a 1-4C alkyl, a 1-4C alkoxy, trifluoromethyl, and a 1-1-5C alkyl-(2-5C alkenyl)-hydroxyimino-1-5C alkyl-(2-5C alkenyl)-hydroxyimino; (m) is an integer of 0-54; (n) is an integer of 0-53) is characterized by converting the E-oxime ether represented by formula (IIa) (wherein, substituents are the same as defined above) to a salt by using a base in the presence of an organic diluent and reacting the product with a methylation agent of CH
    3 (wherein, X is Cl, Br, or the like).
    COPYRIGHT: (C)2003,JPO

    Abstract translation: 要解决的问题：提供一种容易地生产苯基乙醛酸酯的肟基醚异构体的方法。 解决方案：制备由式（I）表示的E-肟醚的方法（其中X和Y各自为卤素，1-4C烷基，1-4C烷氧基，三氟甲基和1-1-5C烷基 - （2-5C烯基） - 羟基亚氨基-1C-C 1-5烷基 - （2-5C烯基） - 羟基亚氨基;（m）是0-54的整数;（n）是0-53的整数） 由式（IIa）表示的E-肟醚（其中取代基与上述定义相同）与盐在有机稀释剂存在下使用碱反应，并使产物与甲基化试剂CH3（其中X， 是Cl，Br等）。

    New halomethylbenzoyl cyanide
    2.
    发明专利
    New halomethylbenzoyl cyanide 有权
    新的甲基苯甲酰氯

    公开(公告)号：JP2006188531A

    公开(公告)日：2006-07-20

    申请号：JP2006052375

    申请日：2006-02-28

    Applicant: Basf Ag ,  ビーエーエスエフ アクチェンゲゼルシャフトBASF Aktiengesellschaft

    Inventor： ISAK HEINZ ,  WETTLING THOMAS ,  KEIL MICHAEL ,  WOLF BERND ,  DOETZER REINHARD

    IPC: C07C255/40 ,  C07C253/14 ,  C07C255/32

    CPC classification number: C07C255/40 ,  C07C253/14

    Abstract: PROBLEM TO BE SOLVED: To provide a new halomethylbenzoyl cyanide industrially useful as an important intermediate product for the synthesis of a plant protection agent. SOLUTION: The halomethylbenzoyl cyanide expressed by formula I' is produced by the reaction of a halomethylbenzoyl chloride with an alkali metal cyanide or a transition metal cyanide. In the formula, X is a halogen atom, a 1-4C alkyl, a 1-4C alkoxy, trifluoromethyl, -C(1-5C alkyl)=N-O-(1-5C alkyl) or -C(1-5C alkyl)=N-O-(2-5C alkenyl); m is 0-4; and Y is chloromethyl or bromomethyl. COPYRIGHT: (C)2006,JPO&NCIPI

    Abstract translation: 要解决的问题：提供工业上可用作合成植物保护剂的重要中间产物的新的卤代甲基苯甲酰氰。 解决方案：由式I'表示的卤代甲基苯甲酰氰由卤代甲基苯甲酰氯与碱金属氰化物或过渡金属氰化物的反应产生。 在该式中，X是卤素原子，1-4C烷基，1-4C烷氧基，三氟甲基，-C（1-5C烷基）= NO-（1-5C烷基）或-C（1-5C烷基） = NO-（2-5C烯基）; m为0-4; Y是氯甲基或溴甲基。 版权所有（C）2006，JPO＆NCIPI

    METHOD FOR PRODUCING 2-HALOGEN-PYRIDINE-CARBOXYLIC ACID AMIDES
    6.
    发明专利
    METHOD FOR PRODUCING 2-HALOGEN-PYRIDINE-CARBOXYLIC ACID AMIDES 未知

    公开(公告)号：PL370556A1

    公开(公告)日：2005-05-30

    申请号：PL37055602

    申请日：2002-10-31

    Applicant: BASF AG

    Inventor： MAYER HORST ,  GOLSCH DIETER ,  ISAK HEINZ ,  SCHROEDER JOCHEN

    IPC: C07D213/81 ,  C07D213/82

    Abstract: The invention relates to a process for preparing 2-halopyridinecarboxamides of primary aromatic monoamines I which have a substituent other than hydrogen in the ortho-position to the amino group by reaction of 2-halopyridinecarbonyl chloride II with the aromatic monoamine I, which comprises carrying out the reaction in a solvent mixture comprising water and at least one water-immiscible organic solvent in the presence of none or less than 10 mol %, based on the 2-halopyridinecarbonyl chloride II, of a base other than I or II.

    8.
    发明专利
    未知

    公开(公告)号：BR0113303A

    公开(公告)日：2003-12-30

    申请号：BR0113303

    申请日：2001-08-16

    Applicant: BASF AG

    Inventor： ISAK HEINZ ,  SENDHOFF NORBERT ,  TZ FRANZ SCH ,  THERRE J RG ,  LLER MICHAEL DR GEM ,  PRANKE DIRK ,  MUNZINGER MANFRED ,  WECK ALEXANDER ,  BURKART KIRSTEN

    IPC: A01N25/12 ,  A01N43/88 ,  C07D285/34

    Abstract: Described is a process for the preparation of a particulate tetrahydro-3,5-dimethyl-1,3,5-thiadiazine-2-thione product by combining a first aqueous solution comprising methylammonium N-methyldithiocarbamate with a second aqueous solution comprising formaldehyde, followed by separation and drying of the resulting solid, which comprises combining the first and the second aqueous solutions in such a way that the ratio between the concentrations of dithiocarbamate functions and of formaldehyde is essentially constant in the reaction mixture over time during the duration of the reaction.

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