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    2.
    发明专利
    未知

    公开(公告)号：DE19500760A1

    公开(公告)日：1996-07-18

    申请号：DE19500760

    申请日：1995-01-13

    Applicant: BASF AG

    Inventor： SCHAEFER PETER DR ,  HAMPRECHT GERHARD DR ,  HEISTRACHER ELISABETH DR ,  KLINTZ RALF DR ,  KOENIG HARTMANN DR ,  WALTER HELMUT DR ,  WESTPHALEN KARL-OTTO DR ,  MISLITZ ULF DR

    IPC: C07D213/24 ,  A01N43/40 ,  C07D213/61 ,  C07D401/12 ,  C07D405/12 ,  C07D409/12 ,  C07D213/28

    Abstract: The invention concerns substituted 2-phenylpyridines of formula (I), in which: n = 0, 1; R , R and R represent H, OH, SH, NO2, NH2, CN, COOH, CONH2, halogen, alkyl, alkyl halide, alkoxy, alkoxy halide, alkyl amino, dialkyl amino, alkyl thio, alkyl thio halide, alkoxy carbonyl, amino carbonyl, alkylamino carbonyl, dialkylamino carbonyl; R represents H, OH, SH, NO2, NH2, CN, halogen, alkyl, alkyl halide, alkoxy, alkoxy halide, alkylthio, alkylthio halide, alkyl sulphinyl, alkyl sulphinyl halide, alkylsulphonyl, alkylsulphonyl halide; R represents H, CN or halogen; R , R represent H or halogen; X represents -CH2- or -CO-; R , R , R , R represent H, NO2, CN, halogen, alkyl, alkyl halide, alkoxy, alkoxy halide; R represents H, OH, NO2, NH2, NHOH, CN, CHO, COOH, COCL, CONH2, 1-pyrrolidinyl carbonyl, 1-piperidinyl carbonyl, 4-morpholinyl carbonyl, 2-hydroxy carbonyl-pyrrolidine-1-yl-carbonyl, halogen or various organic groups; R represents H, NO2, NH2, NHOH, alkylsulphonyl amino, dialkylsulphonyl amino, alkylsulphonyl amino halide, alkoxy carbonyl-alkyl halide, alkoxycarbonyl-alkenyl halide. The invention also concerns salts of these compounds. Excluded are variants of formula (I) in which R , R , R and R all represent hydrogen or R and R or R and R represent fluorine. The said compounds can be used as herbicides and for drying out and defoliating plants.

    5.
    发明专利
    未知

    公开(公告)号：DE4236880A1

    公开(公告)日：1994-05-05

    申请号：DE4236880

    申请日：1992-10-31

    Applicant: BASF AG

    Inventor： KLINTZ RALF DR ,  HAMPRECHT GERHARD DR ,  HEISTRACHER ELISABETH DR ,  SCHAEFER PETER DR ,  KARDORFF UWE DR ,  WESTPHALEN KARL-OTTO DR ,  GERBER MATTHIAS DR ,  WALTER HELMUT DR

    IPC: A01N37/46 ,  A01N43/40 ,  C07C233/07 ,  C07C233/34 ,  C07C233/54 ,  C07C323/60 ,  C07C327/38 ,  C07D211/84 ,  C07D211/86 ,  C07D211/88 ,  C07D211/90 ,  C07D211/96 ,  C07D221/04 ,  C07D221/20 ,  C07D401/10 ,  C07D413/10 ,  C07D417/10 ,  C07D521/00

    Abstract: Substituted N-phenylglutarimides (I), wherein X , X = O, S; R = halogen, NO2, CN, CF3; R = H, halogen; R , R , R = H, halogen, CN, alkyl, cycloalkyl, alkenyl, alkinyl, alkyl halide, alkoxy, alkoxy halide, alkyl thio, alkyl thio halide, cyanoalkyl, alkoxy carbonyl, possibly substituted phenyl or benzyl, or 2 substituents of a C atom of the glutarimide ring are linked via a possibly substituted chain, or 2 substituents of adjacent C atoms of the glutarimide ring are linked via a possibly substituted chain; A = CHR -CHR -CO-B or CR =CR -CO-B; R = H, C1-C6-alkyl or C1-C6-alkyl halide; R = halogen, alkyl halide, OH, alkoxy or alkyl carbonyl alkoxy; R = H, halogen, CN, alkyl, alkyl halide, OH, alkoxy, alkyl carbonyl, alkoxy carbonyl or alkyl carbonyloxy; B = H, alkyl, alkenyl, alkinyl, alkyl halide, cycloalkyl, alkoxy alkyl, dialkoxy alkyl, alkyl thioalkyl, OR , SR , NR , R ; R = H, alkyl, alkenyl, alkinyl, cycloalkyl, alkyl halide, cyanoalkyl, alkenyl halide, alkoxy carbonyl alkyl, alkoxyalkyl, alkyl thioalkyl, alkylimino, alkylimino alkyl, possibly substituted phenyl or benzyl; R , R = H, alkyl, alkenyl, alkinyl, cycloalkyl, alkyl halide, alkyl carbonyl, alkoxy carbonyl, alkoxy alkyl, possibly substituted phenyl, or R und R together with the common N atom = saturated or unsaturated 4- to 7- membered heterocycle with 1-2 other heteroatoms, as well as salts of (I) that are tolerable to plants; their preparation and use as herbicides and desiccants/defoliants, as well as preproducts for preparing the N-phenylglutarimides (I).

    6.
    发明专利
    未知

    公开(公告)号：DE59310185D1

    公开(公告)日：2001-08-02

    申请号：DE59310185

    申请日：1993-04-20

    Applicant: BASF AG

    Inventor： KLINTZ RALF DR ,  HEISTRACHER ELISABETH DR ,  SCHAEFER PETER DR ,  HAMPRECHT GERHARD DR ,  PLATH PETER DR ,  KARDORFF UWE DR ,  GERBER MATTHIAS DR ,  WESTPHALEN KARL-OTTO DR ,  WALTER HELMUT DR

    IPC: C07D317/30 ,  A01N37/30 ,  A01N37/32 ,  A01N37/34 ,  A01N37/46 ,  A01N43/08 ,  A01N43/12 ,  A01N43/16 ,  A01N43/18 ,  A01N43/28 ,  A01N43/32 ,  A01N43/38 ,  A01N43/40 ,  A01N43/74 ,  A01N43/78 ,  C07C233/57 ,  C07C233/60 ,  C07C233/61 ,  C07C233/62 ,  C07C233/63 ,  C07C237/42 ,  C07C251/48 ,  C07C251/60 ,  C07C255/13 ,  C07C255/24 ,  C07C255/42 ,  C07C255/46 ,  C07C255/58 ,  C07C271/62 ,  C07D209/48 ,  C07D295/185 ,  C07D307/12 ,  C07D307/90 ,  C07D309/06 ,  C07D335/02 ,  C07D339/06 ,  C07D339/08 ,  C07D401/10 ,  C07D413/06 ,  C07D413/10 ,  C07D417/06 ,  C07D417/10

    Abstract: Substd. cyclohexene-1,2-dicarboxylic acid derivs. of formula (I), and their salts are new. Where T = CONR1R2 or CN; R1, R2 = H; R, 3-6C alkenyl, or 3-6C alkynyl, all opt. substd. by 1-3 halo, CN, NH2, SH, OH, OR, RSO, RSO2, RCO, COOH, ROCO, RNH, (R)2N, RNHCO, (R)2NCO, (RO)(HO)PO, (RO)2PO, or Ar); or Ar' when R1 is H or R, R2 may also be OH, RO, 3-6C alkenyloxy, 3-6C alkynyloxy, 3-7C cycloalkoxy 5-7 cycloalkenyloxy, 1-6C haloalkoxy, 3-6C halo alkenyloxy, 3-7C cycloalkyl-1-6C alkoxy, RCOO, 1-6C cyanoalkoxy, etc.; NR1R2 = a 3-8 membered non-aromatic heterocycle contg. 1-3N atoms and/or one O or S atom and opt. 1-2 CO gps., the ring being opt. substd. by 1-3R; Ar = phenyl or a 3-8 membered heterocycle (contg. 1-4 heteroatoms selected from 1-4N, 1O or 1S) both opt. substd. on every substitutable atom by OH, halo, CN, NO2, CF3, R or RO; Ar' as Ar except that the heterocycle contains 1-4 heteroatoms selected from 1-4N, 1-20 and 1-2S, and only C-atoms may be substd. R = 1-6C alkyl; R3 = H or R; R4 = H or halo; R5 = H, halo, NO2, CN or CF3; R6 = a 3-8 membered heterocycle (contg. 1-4 heteroatoms selected from 1-4N, 1-2O and 1-2S, and in which 1-2 CH2 gps. are opt. replaced by CO), opt. C-substd. by R, 2-6C alkenyl, 2-6C alkynyl, RO, RS, 3-6C alkenyloxy, 3-6C alkynyloxy, 3-6C alkenylthio, 3-6C alkynylthio, ROCO, NO2, NH2, halo, 1-4C alkylamino, di(1-4C)alkylamino, CN, 1-6C cyanoalkyl, 1-6C haloalkyl or 1-6C haloalkyloxy; ACN, ACOB, OR9, C(O)R10, C(S)R10, C(NR16)R10, A = straight chain 2-4C alkenylene or 2-4C alkynylene, both opt. substd. by 1-2 halo, CN, R, 1-6C haloalkyl, OH, RO, RCOO, ROCO or RCO; B = H, R, 3-6C alkenyl, 3-6C alkynyl, 1-6C haloalkyl, 3-7C cycloalkyl, OR17, SR17, phenyl (opt. substd. by 1-3R, 2-6C alkenyl, halo, CN, NO2, 1-6C haloalkyl, RO or ROCO), 1-6C alkoxy-1-6C alkyl, di(1-6C alkoxy)-1-6C alkyl, 1-6C alkylthio-1-6C alkyl or NR18R19; R17 = H, R, 3-6C alkenyl, 3-6C alkynyl, 3-6C cycloalkyl, 1-6C haloalkyl, 1-6C cyanoalkyl, 3-6C haloalkenyl, ROCO, 1-6C alkoxy(1-6C)alkyl, 1-6C alkoxycarbonyl (1-6C) alkyl, 1-6C alkoxyimino(1-6C)alkyl, or phenyl (opt. substd. by 1-3 R, 2-6C alkenyl, halo, CN, NO2, 1-6C haloalkyl, RO or ROCO); R18, R19 = H, R, 3-6C alkenyl, 3-6C alkynyl, 3-6C cycloalkyl, 1-6C haloalkyl, RCO, ROCO, 1-6C alkoxy (1-6C)alkyl, or phenyl (opt. substd. by 1-3R, 3-6C alkenyl, halo, CN, NO2, RO or ROCO); R9 = 1-6C cyanoalkyl RQ, 1-6C haloalkyl, 3-6C haloalkenyl, 3-6C alkynyl, 3-6C haloalkynyl, 1-6 alkoxycarbonyl-2-6C alkyl, ROQOCOQ, 1-6C alkoxyimino (1-6C)alkyl, or phenyl, phenyl-Q, 3-8 membered heterocyclyl or heterocyclyl-Q (where the heterocycles contain 1-4 heteroatoms, etc.; R10 = H, CN, R, 3-6C alkenyl, 3-6C alkynyl, 1-6C haloalkyl, 3-7C cycloalkyl, ROCO, ROCOQ, or phenyl (opt. substd. by 1-3 halo, CN, NO2, R, 3-6C alkenyl, 1-6C haloalkyl, RO or ROCO); R16 = H, R, 3-6C alkenyl, 3-6C alkynyl, 3-7C cycloalkyl, 1-6C haloalkyl, phenyl (opt. substd. by 1-3R, halo, CN, 2-6C alkenyl, NO2, 1-6C haloalkyl, 1-6C alkoxy, or ROCO), ROQ, OH, RO, 3-6C alkenyloxy, 3-6C alkynyloxy, 5-7C cycloalkoxy, 5-7C cycloalkenyloxy, etc.; R5+R6 = an opt. unsatd. 3-5 membered carbon chain which opt. contains 1-2O, S, N, CO or 1-6C alkoximino gps. and which is opt. substd. by 1-2 CN, NO2, NH2, halo, R, 1-6C haloalkyl, 2-6C alkenyl, 2-6C alkynyl, 1-6C cyanoalkyl, RCOQ, phenyl-Q or 3-8 membered heterocyclyl-1-6C alkyl, where the heterocycle is opt. unsatd. and contains 1-4 heteroatoms selected from 1-4N, 1-20 and 1-2S; provided that when T is CONR1R2 then R9 is not 3-6C alkynyl and R16 is not 1-6C alkoxy, and when T is CN then R9 is not 1-6C haloalkoxy.

    N-acylated (hetero)aromatic hydroxylamine derivatives
    7.
    发明专利
    N-acylated (hetero)aromatic hydroxylamine derivatives 未知

    公开(公告)号：DE19738864A1

    公开(公告)日：1999-03-11

    申请号：DE19738864

    申请日：1997-09-05

    Applicant: BASF AG

    Inventor： KLINTZ RALF DR ,  GOETZ NORBERT DR ,  KEIL MICHAEL DR ,  HEILIG MANFRED DR ,  WINGERT HORST DR ,  VOGELBACHER UWE JOSEF DR ,  WAHL JOSEF ,  WITTERICH FRANK DR

    IPC: C07C259/04 ,  C07D231/20 ,  C07C239/10

    Abstract: N-acylated (hetero)aromatic hydroxylamine derivatives are prepared by hydrogenation of the corresponding nitro compound in the presence of an inert, aprotic solvent and an aliphatic amine. N-acylated(hetero)aromatic hydroxylamine derivatives of formula (1) are prepared by hydrogenation of a (hetero)aromatic nitro compound of formula (2) in the presence of a hydrogenation catalyst. The hydrogenation is carried out in a mixture at an inert, aprotic solvent and an aliphatic amine followed by removal of the amine by distillation or extraction to yield a crude hydroxylamine without intermediate isolation that is N-acylated to form the compound of formula (3) and optionally by o-alkylation of form the compound of formula (4), R = 1-4 C alkoxycarbonyl, alkylcarbonyl, alkylaminocarbonyl, di(1-4 C alkyl)aminocarbonyl; R = H or 1-6 C alkyl; R = H, halogen, cyano, 1-4 C alkyl, 1-4 C haloalkyl, 1-4 C alkoxy, 1-4 C alkyl-CRd=N-O-1-4 C alkyl, 1-4 C alkoxycarbonyl, -CH2O-N=C(Ra)-C(Rb)=N-O-Rc or A or B; A = -O-, -CH2-, -O-CH2, CH2O-, -CH2OCO-, -CH=CH-, -CH=N-O-, -CH2-O-N=C (Ra) or a single bond; B = phenyl, napthyl, pyridinyl, pyrazinyl, pyrinidinyl, pyridazinyl, pyrazolyl, imidazolyl, oxazolyl, isoxazolyl, thiazolyl, isothiazolyl, 1,2,4-triazolyl; 1,2,3 triazolyl, furanyl, thienyl, pyrrolyl or 3-7 C cycloalkyl, optionally substituted with 1-3 Ri groups. Ri = H, halogen, cyano, 1-4 C alkyl, 1-4 C haloalkyl, 1-4 C alkoxy, 1-4 C alkyl-CR =N-O-1-4 C alkyl, 1-4 C alkoxycarbonyl, 1-4 C alkylaminocarbonyl, 1-4 C dialkylaminocarbonyl, 1-4 C alkylcarbonylamino, 1-4 C alkylcarbonyl-1; 4-alkylamino or phenyl, optionally substituted by halogen or 1-4 C alkyl Rd = H, 1-4 C alkyl, 2-4 C alkoxy or 2-4 C alkenyl; Ra, Rc = H, halogen, cyano, 1-4 C alkyl, 1-4 C alkoxy, 1-4 C alkylthio, cyclopropyl or trifluoromethyl; Rb = 1-4 C alkyl, 2-4 C alkenyl, 3-6 C cycloalkyl, phenyl, hetaryl or heterocyclyl R = halogen, 1-4 C alkyl, 1-4 C haloalkyl or 1-4 C alkoxycarbonyl X = N or CH; n = 0, 1, 2 or 3.

    8.
    发明专利
    未知

    公开(公告)号：DE19500758A1

    公开(公告)日：1996-07-18

    申请号：DE19500758

    申请日：1995-01-13

    Applicant: BASF AG

    Inventor： SCHAEFER PETER DR ,  HAMPRECHT GERHARD DR ,  HEISTRACHER ELISABETH DR ,  KLINTZ RALF DR ,  KOENIG HARTMANN DR ,  HARREUS ALBRECHT DR ,  GOETZ NORBERT DR ,  WALTER HELMUT DR ,  WESTPHALEN KARL-OTTO DR ,  MISLITZ ULF DR

    IPC: C07D213/24 ,  A01N43/40 ,  C07D213/61 ,  C07D405/10 ,  C07D405/12 ,  C07D401/12 ,  A01N43/34

    Abstract: The invention concerns substituted 2-phenylpyridines of formula (I), in which: n = 0, 1; R , R and R represent H, OH, SH, NO2, NH2, CN, COOH, CONH2, halogen, alkyl, alkyl halide, alkoxy, alkoxy halide, alkyl amino, dialkyl amino, alkyl thio, alkyl thio halide, alkoxy carbonyl, amino carbonyl, alkylamino carbonyl, dialkylamino carbonyl; R represents H, OH, SH, NO2, NH2, CN, halogen, alkyl, alkyl halide, alkoxy, alkoxy halide, alkylthio, alkyl thio halide, alkyl sulphinyl, alkyl sulphinyl halide, alkylsulphonyl, alkyl halide sulphonyl; R represents H, CN or halogen; R , R represent H or halogen; R represents H, OH, NO2, CN, CF3-SO2-O-, halogen, alkyl, alkyl halide, alkoxy, alkoxy halide; X represents -CO-, -O-C(R , R )-CO-, -S-(R , R )-CO-, -CH2-CH(R )-CO-, -CH=C(R )-CO-; R , R represent H or alkyl; R represents H, halogen or alkyl; Z represents optionally substituted tetrahydrofurane-3-yl or -C(R , COR )-CH2-COR ; R represents H or alkyl; R and R represent OH, NH2, pyrrolidinyl, piperidinyl, morpholinyl, alkoxy, alkenyloxy, alkinyloxy, alkoxyalkoxy, cycloalkyloxy, alkylamino, dialkylamino, cycloalkylamino, dicycloalkylamino, alkenylamino, alkinylamino, or alternatively together represent -N(R )-N(R )-, -N(R )-; R , R represent H or alkyl; R represents H, alkyl, alkenyl, alkinyl, alkoxy, alkenyloxy. The invention also concerns salts of these compounds and the use of the compounds and salts as herbicides and for drying out and defoliating plants.

    10.
    发明专利
    未知

    公开(公告)号：DE4429006A1

    公开(公告)日：1996-02-22

    申请号：DE4429006

    申请日：1994-08-16

    Applicant: BASF AG

    Inventor： HEISTRACHER ELISABETH DR ,  BUSSCHE-HUENNEFELD CHRISTOPH D ,  HAMPRECHT GERHARD DR ,  KLINTZ RALF DR ,  SCHAEFER PETER DR ,  WESTPHALEN KARL-OTTO DR ,  GERBER MATTHIAS DR ,  WALTER HELMUT DR

    IPC: A01N43/653 ,  C07D249/12 ,  C07D403/12 ,  C07D413/12 ,  A01N43/647

    Abstract: Substituted triazolinones of formula (I) are disclosed, in which R , R represent C1-C6 alkyl or C1-C6 alkyl halide; R represents H or a halogen; R represents CN, a halogen, C1-C6 alkyl, C1-C6 alkyl halide, C1-C6 alkoxy or C1-C6 alkoxyl halide; R represents NO2, CN or hydrogen; R represents -OR , -SR , -N(R )-R or -N(R )-OR ; R represents H, C1-C6 alkyl, C3-C6 alkenyl, C3-C6 alkinyl, C3-C6 cycloalkyl, C1-C6 alkyl halide, cyano-C1-C6 alkyl, C1-C6 alkoxy-C1-C6-alkyl, C1-C6 alkylthio-C1-C6-alkyl, C1-C6 alkoxycarbonyl-C1-C6-alkyl, C1-C6-alkylaminocarbonyl-C1-C6-alkyl, Di-(C1-C6-alkyl)-aminocarbonyl-C1-C6 alkyl, C1-C6 alkyloxyamino-C1-C6 alkyl, Di-(C1-C6-alkoxy)-C2-C6-alkyl, Di-(C1-C6-alkylthio)-C2-C6 alkyl, C3-C6 alkenyl halide, (as required) substituted phenyl or benzyl; R , R , R represent C1-C6 alkylcarbonyl, C1-C6 alkylcarbonyl halide or one of the possible R groups; R + R represent a halide 4 to 6-membered C chain in which one methylene unit can be replaced by oxygen or C1-C4 alkylamino. Also disclosed are the salts of compounds of formula (I). Use as herbicides, for desiccation and defoliation of plants.

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