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    CONTINUOUS DISTILLATION OF THERMOLABILE MONOMER
    4.
    发明专利
    CONTINUOUS DISTILLATION OF THERMOLABILE MONOMER 失效

    公开(公告)号：JP2000309568A

    公开(公告)日：2000-11-07

    申请号：JP12276799

    申请日：1999-04-28

    Applicant: BASF AG

    Inventor： DUPUIS JACQUES ,  WINTER MANFRED ,  KROENER MICHAEL

    IPC: B01D3/10 ,  B01D3/34 ,  C07C231/24 ,  C07C233/03 ,  C07D207/26 ,  C07D207/267

    Abstract: PROBLEM TO BE SOLVED: To provide an improved method for distilling a thermolabile monomer. SOLUTION: A thermolabile monomer and formaldehyde are continuously and individually fed into a lower part of a distillation tower up to its middle part in a liquid state; the formaldehyde is vaporized by means of an evaporator in the bottom of the tower; the formaldehyde is discharged from the bottom of the tower together with components having higher boiling point than the thermolabile monomer; the formaldehyde is refilled by adding fresh formaldehyde; the thermolabile monomer is removed from a side discharging port formed at the upper third of the distillation tower; the distillation is controlled so that the monomer contains formaldehyde in an amount of less than 5 wt.%; and a product flow containing components having lower boiling points than the thermolabile monomer is removed from the top of the distillation tower.

    DISTILLATE OF N-VINYLFORMAMIDE
    5.
    发明专利
    DISTILLATE OF N-VINYLFORMAMIDE 失效

    公开(公告)号：JPH1081654A

    公开(公告)日：1998-03-31

    申请号：JP18101797

    申请日：1997-07-07

    Applicant: BASF AG

    Inventor： KROENER MICHAEL ,  SCHMIDT WILLI ,  OFTRING ALFRED ,  PROLL THEO ,  HARTMANN HEINRICH

    IPC: C07C231/24 ,  C07C67/00 ,  C07C231/00 ,  C07C233/00 ,  C07C233/03 ,  C07C233/15 ,  C08F26/00 ,  C08F126/02

    Abstract: PROBLEM TO BE SOLVED: To provide a method for purifying N-vinylformamide capable of producing high-quality N-vinylformamide for making a polymer having especially high molecular weight having a K value by Fikentscher's method larger than 200. SOLUTION: This N-vinylformamide distillate is obtained by fractional distillation of N-formamide using a column under reduced pressure. The distillation is continuously carried out in the presence of formamide under 0.5-30 millibar measured at the top of the column. The distillation is controlled so that N- vinylformamide having 1-6wt.% formamide content as the distillate is obtained to give the objective N-vinylformamide for producing an N-vinylformamide polymer having a K value larger than 200, containing 1-6wt.% formamide.

    LIGHT EMITTING COMPOUND FOR ELECTROLUMINESCENT APPLICATIONS
    6.
    发明申请
    LIGHT EMITTING COMPOUND FOR ELECTROLUMINESCENT APPLICATIONS 审中-公开
    用于电致发光应用的发光化合物

    公开(公告)号：WO2006119800A8

    公开(公告)日：2008-03-20

    申请号：PCT/EP2005052090

    申请日：2005-05-09

    Applicant: UNIV BRAUNSCHWEIG TECH ,  BASF AG ,  JOHANNES HANS-HERMANN ,  KOWALSKY WOLFGANG ,  AMMERMANN SVEN ,  KROENER MICHAEL

    Inventor： JOHANNES HANS-HERMANN ,  KOWALSKY WOLFGANG ,  AMMERMANN SVEN ,  KROENER MICHAEL

    IPC: C09K11/06 ,  H01L51/50

    CPC classification number: C07F15/0033 ,  C07F15/006 ,  C07F15/0086 ,  C09K11/06 ,  C09K2211/1007 ,  C09K2211/1011 ,  C09K2211/1029 ,  C09K2211/1033 ,  C09K2211/1037 ,  C09K2211/1048 ,  C09K2211/1051 ,  C09K2211/185 ,  H01L51/0084 ,  H01L51/0085 ,  H01L51/0087 ,  H01L51/009 ,  H01L51/5016 ,  H05B33/14 ,  Y02E10/549

    Abstract: The present invention refers to light emitting compounds, especially to phosphorescent compounds useful for electroluminescent applications, for example forming a layer in OLEDs and laser applications to emit visible light when excited by electric current. The compounds of the present invention comprise a core structure according to general formula (I), wherein Met = Ir, Pt, Pd, Ru, Rh, Re, or Os with n =1-3, m = 3-n for Ir, Ru, Rh, Re or Os and with n = l or 2, m = 2-n for Pt or Pd, wherein r and s are independently positive natural numbers, preferably varying by a maximum of 2, more preferably identical, wherein groups U and V can be selected independently from a chemical bond, any substituted or unsubstituted aromatic or non-aromatic poly- or mono-cyclic group, alkyl, a double bond, a triple bond, nitrogen, oxygen, sulfur, selenium, telluride, NR with R selected from hydrogen, alkyl, aryl or heteroaryl, wherein Ar3 is an aromatic or non-aromatic moiety which allows the formation of chemical bonds to groups U and V, respectively, from neighbouring atoms contained in moiety Ar3, A1 and wherein formula (II) is a saturating ligand.

    Abstract translation: 本发明涉及发光化合物，特别是涉及用于电致发光应用的磷光化合物，例如在由电流激发时在OLED中形成层和激光应用以发射可见光。 本发明的化合物包含通式（I）的核心结构，其中n = 1-3，其中Met = Ir，Pt，Pd，Ru，Rh，Re或Os，对于Ir为m = 3-n， Ru，Rh，Re或Os，对于Pt或Pd，n = 1或2，m = 2-n，其中r和s独立地为正的自然数，优选最多为2，更优选相同，其中基团U 和V可以独立于化学键选择，任何取代或未取代的芳族或非芳族多环或单环基团，烷基，双键，三键，氮，氧，硫，硒，碲化物，NR与 R选自氢，烷基，芳基或杂芳基，其中Ar 3是芳族或非芳族部分，其允许分别与部分Ar3，A1中包含的相邻原子形成与基团U和V的化学键，并且其中式（II ）是饱和配体。

    8.
    发明专利
    未知

    公开(公告)号：DE4007312C2

    公开(公告)日：2000-04-27

    申请号：DE4007312

    申请日：1990-03-08

    Applicant: BASF AG

    Inventor： MOENCH DIETMAR ,  KROENER MICHAEL ,  FREUDENBERG ENRIQUE ,  HARTMANN HEINRICH ,  SENDHOFF NORBERT

    IPC: C08F2/10 ,  C08F8/12 ,  C08F26/00 ,  C08F26/02 ,  D21H21/06 ,  D21H21/10 ,  D21H21/12 ,  D21H21/18

    Abstract: N-vinylformamide is polymerized with or without other water-soluble monoethylenically unsaturated monomers and with or without water-insoluble monoethylenically unsaturated monomers in not less than 30% strength by weight aqueous monomer solutions in the presence of a polymerization initiator at not more than 150 degrees C. in a kneader by a method in which the polymerization is carried out to such an extent that the initially formed water-containing polymer gel disintegrates into fine particles and the finely divided polymer obtainable in this manner is hydrolyzed, preferably in the kneader, so that not less than 0.1 mol % of the N-vinylformamide units present in the polymer are converted into vinylamine units. The polymers obtainable in this manner dissolve readily in water. The aqueous solutions are used, for example, in papermaking and tertiary oil production.

    9.
    发明专利
    未知

    公开(公告)号：AT147764T

    公开(公告)日：1997-02-15

    申请号：AT94900084

    申请日：1993-10-29

    Applicant: BASF AG

    Inventor： HARTMANN HEINRICH ,  DENZINGER WALTER ,  KROENER MICHAEL ,  NILZ CLAUDIA

    IPC: C08F8/00 ,  B01D15/04 ,  B01J20/26 ,  B01J39/20 ,  C08F226/02

    Abstract: PCT No. PCT/EP93/03019 Sec. 371 Date Apr. 25, 1995 Sec. 102(e) Date Apr. 25, 1995 PCT Filed Oct. 29, 1993 PCT Pub. No. WO94/11408 PCT Pub. Date May 26, 1994Abstract of the Disclosure: Insoluble, only slightly swellable polymers containing amino groups, which can be obtained from popcorn polymers containing units of the structure (I) where R and R1 are H or C1-C4-alkyl, by eliminating the group R-CO- from at least 2% of the incorporated units of the structure I, with the formation of units of the structure II (II) a process for the preparation of the amino-containing popcorn polymers by polymerizing N-vinylcarboxamides and, if desired, other monoethylenically unsaturated monomers copolymerizable therewith with from 0.1 to 10% by weight, based on the monomers used in the polymerization, of a compound containing at least two ethylenically unsaturated non-conjugated double bonds as crosslinking agent, with exclusion of oxygen and polymerization initiators, to form popcorn polymers, and elimination of formyl groups from at least 2% of the copolymerized N-vinylcarboxamides, and the use of the resulting insoluble, only slightly swellable polymers containing amino groups as ion exchangers or adsorber resins for metal ions are described.

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