Production of pigmented resin powders
    1.
    发明授权
    Production of pigmented resin powders 失效
    着色树脂粉的生产

    公开(公告)号:US3879335A

    公开(公告)日:1975-04-22

    申请号:US28026272

    申请日:1972-08-14

    Applicant: BASF AG

    CPC classification number: C09D5/03 C09B63/00 C09B67/0003 C09B67/0095

    Abstract: Production of pigmented resin powders by finely dispersing dispersions of pigments in solutions of polymeric materials in at least one organic solvent in water containing a protective colloid while supplying mixing energy, and removing the solvent. A preferred method is to introduce one or more jets of water containing protective colloid at the rate of 5 to 100 m/sec into animpulse exchange chamber together with the dispersion issuing in the immediate vicinity of the orifice(s), and to remove the solvent. The method avoids crosslinking and provides pigmented resin powders of consistently reproducible color which are suitable for conventional powdered-resin coating methods.

    Abstract translation: 通过将颜料的分散体在含有保护胶体的水中的至少一种有机溶剂中精细分散在聚合物材料的溶液中同时提供混合能量并除去溶剂来生产着色树脂粉末。 一种优选的方法是将一种或多种含有保护胶体的水,以5-100m / sec的速率引入到脉冲交换室中,同时在紧邻孔口处发出分散体,并除去溶剂 。 该方法避免交联,并提供适合于常规粉末 - 树脂涂覆方法的颜色一致的可再现颜色的着色树脂粉末。

    Reactor for gas/liquid reaction or gas/liquid/solid reaction
    2.
    发明专利
    Reactor for gas/liquid reaction or gas/liquid/solid reaction 有权
    气体/液体反应或气体/液体/固体反应的反应器

    公开(公告)号:JP2005046837A

    公开(公告)日:2005-02-24

    申请号:JP2004195749

    申请日:2004-07-01

    Abstract: PROBLEM TO BE SOLVED: To provide a reactor which is more economical than a conventional reactor by using a gas distributor with a simple structure and a reactor which is used for a gas/liquid reaction or a gas/liquid/solid reaction without being hardly influenced by improper reaction caused by pulsatory motions.
    SOLUTION: A reactor having a vertical longitudinal axis, an inlet for liquid or liquid/solid feed stream in the upper side region of the reactor and an inlet 3 for gas stream in the lower side region of the reactor is used for gas/liquid reaction or gas/liquid/solid reaction, and the gas flow is transferred through a gas distribution module 9 which is mainly made from straight pipe-like parts 14 and 15.
    COPYRIGHT: (C)2005,JPO&NCIPI

    Abstract translation: 要解决的问题:提供一种比常规反应器更经济的反应器,其通过使用具有简单结构的气体分布器和用于气/液反应或气/液/固体反应的反应器而没有 几乎不受脉动运动引起的不当反应的影响。 解决方案:具有垂直纵向轴线的反应器,在反应器的上侧区域中的液体或液体/固体进料流的入口和用于气体的下侧区域中的气流的入口3用于气体 /液体反应或气体/液体/固体反应,气流通过主要由直管状部分14和15制成的气体分配模块9传送。(C)2005,JPO&NCIPI

    CONTINUOUS PRODUCTION OF POLYTETRAHYDROFURAN BY TRANSESTERIFICATION CASCADE CAPABLE OF BREAKING AIR BUBBLE

    公开(公告)号:JPH11158263A

    公开(公告)日:1999-06-15

    申请号:JP27181698

    申请日:1998-09-25

    Applicant: BASF AG

    Abstract: PROBLEM TO BE SOLVED: To provide a process whereby a hydroxyl-contg. polymer, esp. a hydroxyl-terminated polytetrahydrofuran, is produced from the corresponding alkoxy-contg. polymer by the transesterification with an alcohol continuously in a mass of at least 100% of the nominal capacity without being obstructed by the occurrence of air bubbles. SOLUTION: This process continuously produces a hydroxyl-contg. polymer, esp. a hydroxyl-terminated polytetrahydrofuran, from the corresponding acyloxy- contg. polymer by the transesterification with an alcohol in at least one stirring reactor (I, II, III, or IV). Air bubbles occurring in the transesterification are broken by introducing the bubbles in the tangential direction at a suitable velocity into circular cylindrical containers 5, 13, esp. into cyclone separators, and thus formed liq. phase is returned through a pipe 3, 3' to at least one stirring reactor (I, II, III, or IV) in order to be recycled. The recycling is pref. done at stirring reactor cascades, and the subunit of each reactor is or subunits of at least two reactors are each individually connected to the circular cylindrical containers, esp. the cyclone separators.

    IMPROVED METHOD FOR PRODUCING BIPHENOLS FROM MONOPHENOLS
    4.
    发明申请
    IMPROVED METHOD FOR PRODUCING BIPHENOLS FROM MONOPHENOLS 审中-公开
    改进工艺用于生产双酚关单酚

    公开(公告)号:WO2006106123A3

    公开(公告)日:2007-01-18

    申请号:PCT/EP2006061352

    申请日:2006-04-05

    CPC classification number: C07C37/11 C07C39/15

    Abstract: The invention relates to a method for producing biphenols of general formula (I) by reacting monophenols of general formula (II), wherein the radicals R1, R2 and R3 independently represent hydrogen, alkyl, aryl or arylalkyl, with 1 - 10 C-atoms, in the presence of an oxidation agent in a reactor. Said method is characterised in that a) the reactor does not contain any stationary integrated components which act as a current agitator, b) a maximum of 0,6 mol of oxidation agents are used per mol of monophenol, and c) the oxidation agent is added in a continuous or discontinuous manner in a plurality of portions within a time span of between 10 min - 24 hours, whereby the amount of oxidation agent which is added per time unit is not constant over the entire tine span, but is varied.

    Abstract translation: 一种用于在一个存在下,通过式(II)其中基团R1,R2和R3独立地是氢,烷基,芳基或芳烷基的碳原子数1〜10中的一元酚的反应由通式(I)制备双酚过程 氧化剂在反应器中,其特征在于:a)反应器含有不作为挡板作用固定设备,b)中的最大0.6摩尔的氧化剂是每单酚的一倍摩尔使用的,和c)在一段10分钟至24氧化剂 小时或者连续,或间歇地在几个部分中,加入,引入氧化剂的每单位量不随时间恒定的整个期间而被改变。

    6.
    发明专利
    未知

    公开(公告)号:AT364432T

    公开(公告)日:2007-07-15

    申请号:AT04015447

    申请日:2004-07-01

    Applicant: BASF AG

    Abstract: A reactor, used for reactions between liquid/gas, or gases/liquids/solids, and has a vertical longitudinal axis with an educt feed pipe in the upper part of the reactor. Incoming gas (3) enters via an aperture in the base (5), and is distributed via a gas distributor module (9) that consists solely of straight pipes (14, 15). The gas distributor module has no curved or bent pipes. All pipes within the module are cylindrical and of circular cross section. Pipe sections are joined at right angles to each other. Horizontal distributor pipes (15) are at 40-90% of reactor chamber (4) depth.

    7.
    发明专利
    未知

    公开(公告)号:DE10329491A1

    公开(公告)日:2005-01-27

    申请号:DE10329491

    申请日:2003-07-01

    Applicant: BASF AG

    Abstract: A reactor, used for reactions between liquid/gas, or gases/liquids/solids, and has a vertical longitudinal axis with an educt feed pipe in the upper part of the reactor. Incoming gas (3) enters via an aperture in the base (5), and is distributed via a gas distributor module (9) that consists solely of straight pipes (14, 15). The gas distributor module has no curved or bent pipes. All pipes within the module are cylindrical and of circular cross section. Pipe sections are joined at right angles to each other. Horizontal distributor pipes (15) are at 40-90% of reactor chamber (4) depth.

    8.
    发明专利
    未知

    公开(公告)号:DE59906105D1

    公开(公告)日:2003-07-31

    申请号:DE59906105

    申请日:1999-04-22

    Applicant: BASF AG

    Abstract: A process for the continuous production of 1,3-dioxolan-2-ones such as ethylene carbonate or propylene carbonate by reacting a corresponding oxirane with carbon dioxide in the liquid phase in the presence of a catalyst comprises conducting the reaction in a two-part reactor in whose first part the reaction is taken with backmixing to a conversion of not less than 80% of the oxirane II and in whose second part the reaction is completed under nonbackmixing conditions, and passing the carbon dioxide in countercurrent to the oxirane II in the entire reactor.

    PROCESS AND APPARATUS FOR THE MANUFACTURE OF FIBRIDS OF THERMOPLASTICS MATERIALS

    公开(公告)号:CA1044868A

    公开(公告)日:1978-12-26

    申请号:CA164617

    申请日:1973-02-23

    Applicant: BASF AG

    Abstract: A process for the manufacture of fibrids of a thermoplastic organic polymer material which comprises extruding strands of molten thermoplastic organic polymer material through orifices of die means/and introducing a propulsive jet of liquid flowing from a nozzle located in the center of said die means at a velocity of from 10 to 100 meters per second and flowing in the same direction as said strands with in a liquid-filled zone surrounding said orifices, passing said strands, the propulsive jet and entrained liquid immediately and directly into and through a tubular impulse exchange zone having a mean diameter of from 2 to 20 times the diameter of said nozzle of said propulsive jet and a length of from 2 to 30 times its hydraulic diameter to provide shear stresses acting on said strands within said impulse exchange zone, and causing said strands of thermoplastic organic polymer material to solidify by the cooling of said melt by said liquid and to be broken up into fibrids by said shear stresses within said impulse exchange zone. The invention also relates to an apparatus for carrying out the above process. This apparatus consists of a container filled with liquid, a nozzle for melt of said thermoplastic organic polymer material and which surrounds a nozzle or nozzles for the propulsive jet projecting parallel into said container and a tube having a diameter from 2 to 20 times the diameter of the nozzles for the propulsive jet and having a length from 2 to 30 times its hydraulic diameter, said tube being disposed at a short distance from the die orifices coaxially with an imaginary extension of the axis of the die so that said tube can accommodate the propulsive jet and the extruded thermoplastic organic polymer material leaving said die orifices. The orifices for the molten plastics material comprise a circle of round nozzles disposed around a propulsive nozzle or in the form of arcuate slots disposed concentrically with said propulsive nozzle.

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