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    Method of continuous hydrogenation, or amination by hydrogenation
    1.
    发明专利
    Method of continuous hydrogenation, or amination by hydrogenation 有权
    连续加氢方法或氢化方法

    公开(公告)号：JP2011178800A

    公开(公告)日：2011-09-15

    申请号：JP2011098268

    申请日：2011-04-26

    Applicant: Basf Se ,  ビーエーエスエフ ソシエタス・ヨーロピアBasf Se

    Inventor： HOFFER BRAM WILLEM ,  VOSS HARTWIG ,  SCHWAB EKKEHARD DR ,  RHEUDE UDO DR ,  KAIBEL GERD DR ,  HAAKE MATHIAS ,  EBERHARDT JAN ,  MICHAEL KARCHER

    IPC: C07C45/62 ,  C07B61/00 ,  C07C47/228 ,  C07D265/30

    CPC classification number: C07C45/62 ,  C07C47/228 ,  C07C49/04 ,  C07C47/02

    Abstract: PROBLEM TO BE SOLVED: To provide a method for continuously hydrogenating an unsaturated compound with integrated advantages including a high space-time yield, a high conversion ratio with improved methodological versatility, and small investment cost.
    SOLUTION: The method for continuously hydrogenating unsaturated compounds involves: (a) particles of a first hydrogenation catalyst are suspended in a liquid phase in which an unsaturated compound is dissolved, the liquid phase, in the presence of a hydrogenous gas at a first partial hydrogen pressure and at a first temperature, is conducted through a conductive pipe 4 to a packed bubble column reactor in cocurrent counter to the direction of gravity, (c) the effluent from the bubble column reactor is sent to a gas-liquid separation tank 8, (d) the liquid phase from step (c) is sent to a crossfiltration 12 to obtain a retentate 11 and a filtrate 13, (e) the retentate is recycled to step (b), and (f) the filtrate, in the presence of a hydrogenous gas at a second partial hydrogen pressure and at a second temperature, is passed over a bed 18 of a second hydrogenation catalyst.
    COPYRIGHT: (C)2011,JPO&INPIT

    Abstract translation: 待解决的问题：提供一种以具有高空时收益率，高转化率，改进的方法多功能性以及小投资成本的综合优势连续氢化不饱和化合物的方法。 解决方案：不连续氢化不饱和化合物的方法包括：（a）将第一氢化催化剂的颗粒悬浮在其中溶解有不饱和化合物的液相中，液相在氢气存在下在 第一部分氢气压力和第一温度通过导电管4传导到与重力方向相反并流的气泡塔式反应器，（c）来自泡罩塔反应器的流出物被送入气 - 液分离 罐8中，（d）将来自步骤（c）的液相送至交叉滤液12，得到滞留物11和滤液13，（e）将渗余物循环至步骤（b），（f）滤液， 在第二部分氢气压力和第二温度下在氢气存在下，通过第二氢化催化剂的床18。 版权所有（C）2011，JPO＆INPIT

    METHOD FOR PRODUCING AMINES FROM SUGAR ALCOHOLS
    4.
    发明申请
    METHOD FOR PRODUCING AMINES FROM SUGAR ALCOHOLS 审中-公开
    从糖醇制备胺的方法

    公开(公告)号：WO2009027249A3

    公开(公告)日：2009-06-18

    申请号：PCT/EP2008060742

    申请日：2008-08-15

    Applicant: BASF SE ,  ERNST MARTIN ,  HOFFER BRAM WILLEM ,  MELDER JOHANN-PETER

    Inventor： ERNST MARTIN ,  HOFFER BRAM WILLEM ,  MELDER JOHANN-PETER

    IPC: C07C209/16 ,  C07C211/10 ,  C07C211/11 ,  C07D241/02 ,  C07D295/00

    CPC classification number: C07C209/16 ,  C04B24/122 ,  C04B28/02 ,  C07C213/02 ,  C07D241/04 ,  C07D295/02 ,  C07D295/023 ,  C07C211/09 ,  C07C211/10 ,  C07C211/11 ,  C07C215/08

    Abstract: The invention relates to a method for producing amines by reacting sugar alcohols with hydrogen and an amination agent, selected from the group containing ammonia, primary and secondary amines, in the presence of a catalyst at a temperature of between 100°C and 400°C and at a pressure of between 1 and 40 MPa (10 to 400 bar). The catalyst preferably contains a metal or several metals or one or more oxygen-containing compounds of metals in groups 8 and/or 9 and/or 10 and/or 11 of the periodic table of elements. Preferably, the sugar alcohol is obtained by the hydrogenation of the corresponding sugars. The invention also relates to the use of the reaction product as an additive in cement or concrete production and in other application areas.

    Abstract translation: 本发明涉及一种通过糖醇与氢气和选自氨，伯和仲胺中选择的胺化剂反应制备胺的方法，在催化剂的存在下，在100℃的温度至400℃和压力 1至40MPa（10至400巴）。 催化剂优选含有一种或多种金属或一种或多种元素周期表第8和/或9族和/或10和/或11族金属的含氧化合物。 糖醇优选通过相应糖的氢化获得。 本发明还涉及反应产物作为水泥或混凝土生产和其它应用中的添加剂的用途。

    HYDROGENATING CATALYSTS, PRODUCTION AND USE THEREOF
    5.
    发明申请
    HYDROGENATING CATALYSTS, PRODUCTION AND USE THEREOF 审中-公开
    加氢催化剂，生产和使用

    公开(公告)号：WO2010089266A3

    公开(公告)日：2010-12-23

    申请号：PCT/EP2010051143

    申请日：2010-02-01

    Applicant: BASF SE ,  WIGBERS CHRISTOF WILHELM ,  STEINER JOCHEN ,  ERNST MARTIN ,  HOFFER BRAM WILLEM ,  SCHWAB EKKEHARD ,  MELDER JOHANN-PETER

    Inventor： WIGBERS CHRISTOF WILHELM ,  STEINER JOCHEN ,  ERNST MARTIN ,  HOFFER BRAM WILLEM ,  SCHWAB EKKEHARD ,  MELDER JOHANN-PETER

    IPC: B01J23/78 ,  B01J23/83 ,  B01J27/18 ,  B01J27/185 ,  B01J35/04 ,  B01J37/02 ,  C07C209/48 ,  C07C211/11 ,  C07C211/12 ,  C07C211/36 ,  C07C253/30 ,  C07C255/24

    CPC classification number: B01J23/78 ,  B01J23/83 ,  B01J27/1853 ,  B01J35/04 ,  B01J37/0201 ,  B01J37/0205 ,  B01J37/0215 ,  B01J37/0234 ,  C07C209/48 ,  C07C253/30 ,  C07C2601/14 ,  C07C211/11 ,  C07C211/12 ,  C07C211/36 ,  C07C255/24

    Abstract: The invention relates to a method for improving the catalytic properties of a catalyst that exists in the form of a structured monolith and comprises one or more elements selected from the group comprising cobalt, nickel and copper, wherein the catalyst is brought into contact with one or more base compounds selected from the group of alkali, earth alkali and rare earth metals. The invention further relates to a method for hydrogenating compounds comprising at least one unsaturated carbon-carbon, carbon-nitrogen or carbon-oxygen compound, in the presence of a catalyst comprising one or more elements selected from the group comprising cobalt, nickel and copper, wherein the catalyst exists in the form of a structured monolith, characterized in that the catalyst is brought into contact with one or more base compounds selected from the group of alkali, earth alkali and rare earth metals. In addition, the invention relates to the use of a base compound selected from the group of alkali, earth alkali and rare earth metals for improving the catalytic properties of a catalyst, comprising copper and/or cobalt and/or nickel, wherein the catalyst exists in the form of a structured monolith.

    Abstract translation: 本发明涉及一种用于改善的催化剂，其存在于结构化的整料和或多种元素的选自由钴，镍的含有基团和铜中选择的形式的催化性质，其中与所述催化剂的一种或多种基本 选自碱金属，碱土金属和稀土金属的选择的化合物所接触。 本发明还涉及一种方法，用于包含在催化剂的存在下对含至少一个不饱和碳 - 碳，碳 - 氮或碳 - 氧键的化合物的氢化的组中选择的一种或多种元素自由钴，镍 和铜，其中，所述催化剂是在结构化的单块形式，其特征在于，所述催化剂与选自碱金属，碱土和在接触稀土金属中的一种或多种碱性化合物接触。 此外，本发明是使用选自碱金属，碱土金属和稀土金属中选出的碱性化合物，以提高催化剂的催化性能而言，包含铜和/或钴和/或镍，其特征在于，以结构化的形式的催化剂 整料是存在的。

    8.
    发明专利
    未知

    公开(公告)号：AT448191T

    公开(公告)日：2009-11-15

    申请号：AT06793777

    申请日：2006-09-25

    Applicant: BASF SE

    Inventor： CAUWENBERGE GUNTHER ,  MELDER JOHANN-PETER ,  EVERS HOLGER ,  GERLACH TILL ,  KIESSLICH FRANK ,  SCHWAB EKKEHARD ,  HOFFER BRAM WILLEM

    IPC: C07C209/16 ,  C07C211/10

    Abstract: Processes comprising: providing a starting material comprising monoethanolamine; and reacting the starting material with ammonia in the presence of a heterogeneous transition metal catalyst to form a reaction product comprising one or more ethylene amines; wherein the catalyst comprises a catalytically active composition, which prior to treatment with hydrogen, comprises a mixture of oxygen-containing compounds of aluminum, copper, nickel and cobalt; and wherein the catalyst is present as one or more shaped catalyst particles selected from spheres, extrudates, pellets and other geometries, wherein the sphere or extrudate has a diameter of

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