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    PROCESS FOR MAKING LITHIATED TRANSITION METAL OXIDES
    2.
    发明申请
    PROCESS FOR MAKING LITHIATED TRANSITION METAL OXIDES 审中-公开
    制备过渡金属氧化物的方法

    公开(公告)号：WO2016083205A3

    公开(公告)日：2016-07-21

    申请号：PCT/EP2015076941

    申请日：2015-11-18

    Applicant: BASF SE

    Inventor： VOLKOV ALEKSEI ,  SCHULZ-DOBRICK MARTIN ,  SCHRÖDLE SIMON ,  LAMPERT JORDAN

    IPC: H01M4/36 ,  C01G53/00 ,  H01M4/505 ,  H01M4/525 ,  H01M4/58

    CPC classification number: H01M4/364 ,  C01G53/50 ,  C01P2004/50 ,  C01P2004/51 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2006/11 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/40 ,  H01M4/505 ,  H01M4/525 ,  H01M4/5825 ,  H01M4/623 ,  H01M4/625 ,  H01M10/0525 ,  H01M2004/028

    Abstract: The present invention is directed towards a process for making a lithiated transition metal oxide, said process comprising the following steps: (a) providing a precursor selected from mixed oxides, hydroxides, oxyhydroxides, and carbonates of nickel and at least one transition metal selected from manganese and cobalt, wherein at least 45 mole-% of the cations of the precursor are Ni cations, (b) mixing said precursor with at least one lithium salt selected from LiOH, Li2O, Li2CO3, and LiNO3, thereby obtaining a mixture, (c) adding at least one phosphorus compound of general formula (I) XyH3-yPO4 (I) wherein X is selected from NH4 and Li, y is 1 or 2, to the mixture obtained in step (b), wherein steps (b) and (c) may be performed consecutively or simultaneously, treating the mixture so obtained at a temperature in the range of from 650 to 950°C.

    Abstract translation: 本发明涉及一种制备锂化过渡金属氧化物的方法，所述方法包括以下步骤：（a）提供一种选自镍的混合氧化物，氢氧化物，羟基氧化物和碳酸盐的前体和至少一种选自以下的过渡金属： 锰和钴，其中前体的至少45摩尔％的阳离子是Ni阳离子，（b）将所述前体与至少一种选自LiOH，Li 2 O，Li 2 CO 3和LiNO 3的锂盐混合，从而得到混合物（ c）向步骤（b）中获得的混合物中加入至少一种其中X选自NH 4和Li，y为1或2的通式（I）XyH 3-y PO 4（I）的磷化合物，其中步骤（b） 和（c）可以连续或同时进行，在650-950℃的温度范围内处理如此获得的混合物。

    PROCESS FOR THE PREPARATION OF CRYSTALLINE LITHIUM-, VANADIUM- AND PHOSPHATE-COMPRISING MATERIALS
    5.
    发明申请
    PROCESS FOR THE PREPARATION OF CRYSTALLINE LITHIUM-, VANADIUM- AND PHOSPHATE-COMPRISING MATERIALS 审中-公开
    用于制备晶体锂，钒和磷酸盐包覆材料的方法

    公开(公告)号：WO2009043730A3

    公开(公告)日：2009-10-29

    申请号：PCT/EP2008062428

    申请日：2008-09-18

    Applicant: BASF SE ,  HIBST HARTMUT ,  ROBERTS BRIAN ,  LAMPERT JORDAN ,  BRAMNIK KIRILL

    Inventor： HIBST HARTMUT ,  ROBERTS BRIAN ,  LAMPERT JORDAN ,  BRAMNIK KIRILL

    IPC: C01B25/45 ,  H01M4/58 ,  H01M10/36

    CPC classification number: C01B25/45 ,  H01M4/5825 ,  H01M10/0525

    Abstract: The present invention relates to a process for the preparation of compounds of general formula (I) Lia-bM1 bV2-cM2 c(PO4)x (I) with M1: Na, K, Rb and/or Cs, M2: Ti, Zr, Nb, Cr, Mn, Fe, Co, Ni, Al, Mg and/or Sc, a: 1.5 - 4.5, b: 0 - 0.6, c: 0 - 1.98 and x: number to equalize the charge of Li and V and M1 and/or M2, if present, wherein a-b is > 0, by providing an essentially aqueous mixture comprising at least one lithium-comprising compound, at least one vanadium-comprising compound in which vanadium has the oxidation state +5 and/or +4, and at least one M1-comprising compound, if present, and/or at least one M2-comprising compound, if present, and at least one reducing agent which is oxidized to at least one compound comprising at least one phosphorous atom in oxidation state +5, drying and calcining.

    Abstract translation: 本发明涉及制备具有M1：Na，K，Rb和/或Cs，M2：Ti，Zr的通式（I）Lia-bM1 bV2-cM2 c（PO4）x（Ⅰ）的化合物的方法 ，Nb，Cr，Mn，Fe，Co，Ni，Al，Mg和/或Sc，a：1.5〜4.5，b：0 - 0.6，c：0 - 1.98和x： 和M1和/或M2（如果存在），其中ab> 0，通过提供基本上含水的混合物，其包含至少一种含锂化合物，至少一种含钒化合物，其中钒具有+5和/或 +4，和至少一种含M1化合物（如果存在）和/或至少一种含M2化合物（如果存在）和至少一种还原剂被氧化成至少一种包含至少一个磷原子的化合物 氧化态+5，干燥和煅烧。

    PROCESS FOR THE PREPARATION OF POROUS LITHIUM-, VANADIUM AND PHOSPHATE-COMPRISING MATERIALS
    6.
    发明申请
    PROCESS FOR THE PREPARATION OF POROUS LITHIUM-, VANADIUM AND PHOSPHATE-COMPRISING MATERIALS 审中-公开
    制备多孔含锂，钒和磷酸盐材料的方法

    公开(公告)号：WO2009043729A3

    公开(公告)日：2009-10-29

    申请号：PCT/EP2008062427

    申请日：2008-09-18

    Applicant: BASF SE ,  HIBST HARTMUT ,  ROBERTS BRIAN ,  LAMPERT JORDAN ,  BRAMNIK KIRILL

    Inventor： HIBST HARTMUT ,  ROBERTS BRIAN ,  LAMPERT JORDAN ,  BRAMNIK KIRILL

    IPC: C01B25/45 ,  H01M4/136 ,  H01M4/58

    CPC classification number: C01B25/45 ,  H01M4/136 ,  H01M4/5825

    Abstract: The present invention relates to a process for the preparation of compounds of general formula (I) : Lia-bM1 bV2-cM2 c(PO4)x; wherein M1, M2, a, b, c and x have the following meanings: M1: Na, K, Rb and/or Cs, M2: Ti, Zr, Nb, Cr, Mn, Fe, Co, Ni, Al, Mg and/or Sc, a: 1.5 - 4.5, b: 0 - 0.6, c: 0 - 1.98 and x: number to equalize the charge of Li and V and M1 and/or M2, if present, wherein a-b is > 0, to a compound according to general formula (I) as defined above, to spherical agglomerates and/or particles comprising at least one compound of general formula (I) as defined above, to the use of such a compound for the preparation of a cathode of a lithium ion battery or an electrochemical cell, and to a cathode for a lithium ion battery, comprising at least one compound as defined above.

    Abstract translation: 本发明涉及制备通式（I）化合物的方法：Lia-bM1 bV2-cM2 c（PO4）x; 其中M1，M2，a，b，c和x具有以下含义：M1：Na，K，Rb和/或Cs，M2：Ti，Zr，Nb，Cr，Mn，Fe，Co，Ni，Al，Mg 和/或Sc，a：1.5-4.5，b：0-0.6，c：0-1.98和x：使Li和V以及M1和/或M2的电荷（如果存在）相等的数量，其中ab> 涉及如上所定义的根据通式（I）的化合物，包含至少一种如上所定义的通式（I）的化合物的球形附聚物和/或颗粒，涉及这种化合物用于制备阴极的用途 锂离子电池或电化学电池以及用于锂离子电池的阴极，其包含至少一种如上定义的化合物。

    PROCESS FOR THE PREPARATION OF CRYSTALLINE LITHIUM-, VANADIUM- AND PHOSPHATE-COMPRISING MATERIALS
    7.
    发明专利
    PROCESS FOR THE PREPARATION OF CRYSTALLINE LITHIUM-, VANADIUM- AND PHOSPHATE-COMPRISING MATERIALS 未知

    公开(公告)号：CA2701145A1

    公开(公告)日：2009-04-09

    申请号：CA2701145

    申请日：2008-09-18

    Applicant: BASF SE

    Inventor： HIBST HARTMUT ,  ROBERTS BRIAN ,  LAMPERT JORDAN ,  BRAMNIK KIRILL

    IPC: C01B25/45 ,  H01M4/58 ,  H01M10/36

    Abstract: The present invention relates to a process for the preparation of compounds of general formula (I) Lia-bM1 bV2-cM2 c(PO4)x (I) with M1: Na, K, Rb and/or Cs, M2: Ti, Zr, Nb, Cr, Mn, Fe, Co, Ni, Al, Mg and/or Sc, a: 1.5 - 4.5, b: 0 - 0.6, c: 0 - 1.98 and x: number to equalize the charge of Li and V and M1 and/or M2, if present, wherein a-b is > 0, by providing an essentially aqueous mixture comprising at least one lithium-comprising compound, at least one vanadium-comprising compound in which vanadium has the oxidation state +5 and/or +4, and at least one M1-comprising compound, if present, and/or at least one M2-comprising compound, if present, and at least one reducing agent which is oxidized to at least one compound comprising at least one phosphorous atom in oxidation state +5, drying and calcining.

    PROCESS FOR THE PREPARATION OF POROUS LITHIUM-, VANADIUM AND PHOSPHATE-COMPRISING MATERIALS
    8.
    发明专利
    PROCESS FOR THE PREPARATION OF POROUS LITHIUM-, VANADIUM AND PHOSPHATE-COMPRISING MATERIALS 未知

    公开(公告)号：CA2701144A1

    公开(公告)日：2009-04-09

    申请号：CA2701144

    申请日：2008-09-18

    Applicant: BASF SE

    Inventor： HIBST HARTMUT ,  ROBERTS BRIAN ,  LAMPERT JORDAN ,  BRAMNIK KIRILL

    IPC: C01B25/45 ,  H01M4/136 ,  H01M4/58

    Abstract: The present invention relates to a process for the preparation of compounds of general formula (I) : Lia-bM1 bV2-cM2 c(PO4)x; wherein M1, M2, a, b, c and x have the following meanings: M1: Na, K, Rb and/or Cs, M2: Ti, Zr, Nb, Cr, Mn, Fe, Co, Ni, Al, Mg and/or Sc, a: 1.5 - 4.5, b: 0 - 0.6, c: 0 - 1.98 and x: number to equalize the charge of Li and V and M1 and/or M2, if present, wherein a-b is > 0, to a compound according to general formula (I) as defined above, to spherical agglomerates and/or particles comprising at least one compound of general formula (I) as defined above, to the use of such a compound for the preparation of a cathode of a lithium ion battery or an electrochemical cell, and to a cathode for a lithium ion battery, comprising at least one compound as defined above.

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