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    FINELY DIVIDED STARCH-CONTAINING POLYMER DISPERSIONS, METHOD FOR THE PRODUCTION THEREOF AND USE THEREOF AS SIZING AGENT IN PAPER MANUFACTURING
    1.
    发明申请
    FINELY DIVIDED STARCH-CONTAINING POLYMER DISPERSIONS, METHOD FOR THE PRODUCTION THEREOF AND USE THEREOF AS SIZING AGENT IN PAPER MANUFACTURING 审中-公开
    佳作，强度含聚合物分散体，方法的生产和使用作为纸生产施胶剂

    公开(公告)号：WO2011039185A3

    公开(公告)日：2011-05-26

    申请号：PCT/EP2010064357

    申请日：2010-09-28

    Applicant: BASF SE ,  SONG ANJA ,  KERN HOLGER ,  ARNOLD PETRA

    Inventor： SONG ANJA ,  KERN HOLGER ,  ARNOLD PETRA

    IPC: C08F2/24 ,  C08F212/08 ,  D21H17/34

    CPC classification number: C08F2/24 ,  C08F220/16 ,  D21H17/34 ,  D21H21/16 ,  C08F212/08 ,  C08F2220/1825 ,  C08F220/06 ,  C08F2220/1858

    Abstract: The invention relates to finely divided starch-containing polymer dispersions, which can be obtained by the radically initiated emulsion polymerization of ethylenically unsaturated monomers in the presence of at least one redox initiator and starch, wherein the ethylenically unsaturated monomers used are (a) 30 to 60% by weight of at least one optionally substituted styrol, (b) 1 to 60% by weight of at least one acrylic acid-C1-C12-alkyl ester and/or methacrylic acid-C1-C12-alkyl ester, (c) 0 to 10% by weight of at least one other ethylenically unsaturated copolymerizable monomer, and the starch used is (d) 15 to 40% by weight of at least one degraded starch having a molar mass Mw of 1000 to 65000 g/mol, wherein the sum (a) + (b) + (c) + (d) = 100% and relates to the total solid matter content, and wherein the polymerization is carried out in the presence of at least 0.01% by weight, relative to the monomers used, of at least one terpene-containing polymerization regulator. The invention further relates to a method for producing the finely divided starch-containing polymer dispersions by means of the emulsion polymerization of monomers (a), (b) and (c) using redox initiators in the presence of (d) degraded starch and at least 0.01% by weight, relative to the monomers used, of at least one terpene-containing polymerization regulator, and to the use of the finely divided starch-containing polymer dispersions as a sizing agent for paper, paperboard and cardboard.

    Abstract translation: 细碎，含淀粉的聚合物分散体，其是由在至少一种氧化还原引发剂和淀粉的存在下烯属不饱和单体的自由基乳液聚合获得，使用如烯属不饱和单体（a）30至60重量％的至少一个任选取代的苯乙烯％，（B）1 到60重量的甲基丙烯酸C1-C12烷基酯中的至少一种丙烯酸C 1 -C 12烷基酯，和/或（c）0至10重量％的至少一种其他烯属不饱和可共聚单体的％和厚度（d）的百分比 15至40重量％采用具有MoImasse Mw为1000的至少一个降解淀粉至65,000克/摩尔，其中，所述总和（A）+（b）+（C）+（D）= 100％ 并且是指总固体含量，并且其中在至少0.01重量％的存在下的聚合，基于单体使用的，中的至少一种含萜烯的聚合调节剂进行，程序 对于由单体（a），（b）和（c）与（d）中的存在的氧化还原引发剂的乳液聚合制备细碎，含淀粉的聚合物分散体的降解淀粉和至少0.01重量％，基于所使用的单体，至少一种的 聚合调节剂，以及使用细碎，含淀粉的聚合物分散体作为纸张，纸板和卡纸板的含萜烯的。

    Dispersiones de polímeros, acuosas, catiónicas, de partículas finas, métodos para su preparación y uso de las mismas
    2.
    发明专利
    Dispersiones de polímeros, acuosas, catiónicas, de partículas finas, métodos para su preparación y uso de las mismas 未知

    公开(公告)号：ES2405607T3

    公开(公告)日：2013-05-31

    申请号：ES10724434

    申请日：2010-06-01

    Applicant: BASF SE

    Inventor： SONG ANJA ,  KERN HOLGER

    IPC: D21H21/16 ,  C08F2/28 ,  C08F220/06 ,  C08F220/18 ,  C08F220/34 ,  C08F220/56 ,  C08F257/02 ,  C08F285/00 ,  C09J151/00

    Abstract: Dispersiones de polímero acuosas, catiónicas, de partículas finas, con partículas dispersadas de unagranulometría (tamaño de partícula) promedio de 5 a 250 nm, las cuales pueden obtenerse mediante polimerizaciónpor emulsión de monómeros etilénicamente insaturados en una solución acuosa de un prepolímero catiónico encalidad de dispersante, caracterizadas porque primero se produce el prepolímero catiónico en presencia deiniciadores de polimerización polimerizando (a) 15 a 40 % en peso de una mezcla de al menos dos (met)acrilatos diferentes que tienen respectivamente ungrupo amino y/o grupo amonio cuaternario, y/o (met)acrilamidas que portan respectivamente un grupo amino y/ogrupo amonio cuaternario, (b) 40 a 85 % en peso de al menos un estireno opcionalmente sustituido, (c) 0,5 a 5 % en peso de al menos un monómero etilénicamente insaturado que contiene grupos ácidos y (d) 0 a 20 % en peso de al menos un monómero etilénicamente insaturado, no iónico, distinto de (b),donde la suma de (a) + (b) + (c) + (d) >= 100 % en peso, en una polimerización en solución en un solvente parcial ototalmente miscible con agua, la solución/dispersión del prepolímero se mezcla luego con agua, y porque acontinuación en la solución acuosa del prepolímero se realiza una polimerización por emulsión en presencia deiniciadores de polimerización de una mezcla de monómeros de (i) 0 a 29 % en peso de al menos un estireno opcionalmente sustituido, (ii) 50 a 100 % en peso de al menos un (met)acrilato de C1 a C18, (iii) 0 a 30 % en peso de al menos un éster vinílico de ácidos carboxílicos de C1-C30 lineales o ramificados y (iv) 0 a 30 % en peso de al menos un monómero etilénicamente insaturado, no iónico, diferente de (i), (ii) y (iii),donde la suma de (i) + (ii) + (iii) + (iv) >= 100 % en peso, y la polimerización en solución y/o polimerización poremulsión se realiza opcionalmente en presencia de 0 a 10 % en peso de al menos un regulador de polimerización.

    Dispersiones de polímero de partícula fina que contienen almidón, procedimiento para su producción y uso como agente de encolado en la producción de papel
    6.
    发明专利
    Dispersiones de polímero de partícula fina que contienen almidón, procedimiento para su producción y uso como agente de encolado en la producción de papel 未知

    公开(公告)号：ES2494490T3

    公开(公告)日：2014-09-15

    申请号：ES10759637

    申请日：2010-09-28

    Applicant: BASF SE

    Inventor： SONG ANJA ,  KERN HOLGER ,  ARNOLD PETRA

    IPC: C08F2/24 ,  C08F212/08 ,  D21H17/34

    Abstract: Dispersiones de polímero de partícula fina que contienen almidón, que se pueden obtener mediante polimerización en emulsión iniciada por radicales de monómeros etilénicamente insaturados en presencia de al menos un iniciador redox y almidón, caracterizadas por que como monómeros etilénicamente insaturados se usan (a) del 30 al 60 % en peso de al menos un estireno dado el caso sustituido, (b) del 1 al 60 % en peso de al menos un éster de alquilo C1-C12 de ácido acrílico y/o éster de alquilo C1-C12 de ácido metacrílico, (c) del 0 al 10 % en peso de al menos otro monómero copolimerizable etilénicamente insaturado, y como almidón (d) del 15 al 40 % en peso de al menos un almidón degradado, que tiene un peso molecular Mw de 1000 a 65000 g/mol, siendo la suma (a) + (b) + (c) + (d) >= 100 % referida al contenido total de sólidos, y llevándose a cabo la polimerización en presencia de al menos el 0,01 % en peso, referido a los monómeros usados, de al menos un regulador de polimerización que contiene terpeno.

    AQUEOUS POLYMER DISPERSION OBTAINABLE BY FREE-RADICALLY INITIATED EMULSION POLYMERIZATION IN THE PRESENCE OF LIGNOSULFONATE
    7.
    发明专利
    AQUEOUS POLYMER DISPERSION OBTAINABLE BY FREE-RADICALLY INITIATED EMULSION POLYMERIZATION IN THE PRESENCE OF LIGNOSULFONATE 未知

    公开(公告)号：CA2864370A1

    公开(公告)日：2013-08-22

    申请号：CA2864370

    申请日：2013-02-11

    Applicant: BASF SE

    Inventor： AL-HELLANI RABIE ,  CIMPEANU CARMEN-ELENA ,  SCHMIDT-THUMMES JURGEN ,  LAWRENZ DIRK ,  GEORGIEVA KRISTINA ,  SONG ANJA

    IPC: C08F2/22 ,  C08F2/44

    Abstract: Described is an aqueous polymer dispersion comprising a chain growth addition polymer obtainable via free-radically initiated emulsion polymerization from ethylenically unsaturated, free-radically polymerizable monomers, wherein the chain growth addition polymer is formed to an extent of not less than 60 wt% from primary monomers selected from vinylaromatic compounds, conjugated aliphatic dienes, vinyl esters of saturated C1- to C20-carboxylic acids, esters of acrylic acid or of methacrylic acid with monohydric C1- to C20-alcohols, aliphatic hydrocarbons having 2 to 8 carbon atoms and one or two double bonds, or mixtures thereof, wherein the monomers are polymerized in the presence of lignosulfonate and wherein the chain growth addition polymer is branched or crosslinked. Also described is a process for preparing the aqueous polymer dispersion. The polymer dispersion is useful for preparing paper coating compositions.

    FINELY DIVIDED STARCH-CONTAINING POLYMER DISPERSIONS, METHOD FOR THE PRODUCTION THEREOF AND USE THEREOF AS SIZING AGENT IN PAPER MANUFACTURING
    8.
    发明专利
    FINELY DIVIDED STARCH-CONTAINING POLYMER DISPERSIONS, METHOD FOR THE PRODUCTION THEREOF AND USE THEREOF AS SIZING AGENT IN PAPER MANUFACTURING 未知

    公开(公告)号：ZA201203113B

    公开(公告)日：2013-06-26

    申请号：ZA201203113

    申请日：2012-04-30

    Applicant: BASF SE

    Inventor： SONG ANJA ,  KERN HOLGER ,  ARNOLD PETRA

    IPC: D21H20060101 ,  C08F20060101

    Abstract: Finely divided, starch-containing polymer dispersions which are obtainable by free radical emulsion polymerization of ethylenically unsaturated monomers in the presence of at least one redox initiator and starch, (a) from 30 to 60% by weight of at least one optionally substituted styrene, (b) from 1 to 60% by weight of at least one C1-C12-alkyl acrylate and/or C1-C12-alkyl methacrylate, (c) from 0 to 10% by weight of at least one other ethylenically unsaturated copolymerizable monomer, being used as ethylenically unsaturated monomers and (d) from 15 to 40% by weight of at least one degraded starch which has a molar mass Mw of from 1000 to 65 000 g/mol being used as the starch, the sum (a)+(b)+(c)+(d) being 100% and being based on the total solids content, and the polymerization being carried out in the presence of at least 0.01% by weight, based on the monomers used, of at least one terpene-containing chain-transfer agent, processes for the preparation of the finely divided, starch-containing polymer dispersions by emulsion polymerization of the monomers (a), (b) and (c) with redox initiators in the presence of (d) degraded starch and at least 0.01% by weight, based on the monomers used, of at least one terpene-containing chain-transfer agent, and use of the finely divided, starch-containing polymer dispersions as sizes for paper, board and cardboard.

    FINELY DIVIDED STARCH-CONTAINING POLYMER DISPERSIONS, METHOD FOR THE PRODUCTION THEREOF AND USE THEREOF AS SIZING AGENT IN PAPER MANUFACTURING
    10.
    发明专利
    FINELY DIVIDED STARCH-CONTAINING POLYMER DISPERSIONS, METHOD FOR THE PRODUCTION THEREOF AND USE THEREOF AS SIZING AGENT IN PAPER MANUFACTURING 未知

    公开(公告)号：CA2775239C

    公开(公告)日：2013-12-17

    申请号：CA2775239

    申请日：2010-09-28

    Applicant: BASF SE

    Inventor： SONG ANJA ,  KERN HOLGER ,  ARNOLD PETRA

    IPC: C08F2/24 ,  C08F212/08 ,  D21H17/34

    Abstract: The invention relates to finely divided starch-containing polymer dispersions, which can be obtained by the radically initiated emulsion polymerization of ethylenically unsaturated monomers in the presence of at least one redox initiator and starch, wherein the ethylenically unsaturated monomers used are (a) 30 to 60% by weight of at least one optionally substituted styrol, (b) 1 to 60% by weight of at least one acrylic acid-C1-C12-alkyl ester and/or methacrylic acid-C1-C12-alkyl ester, (c) 0 to 10% by weight of at least one other ethylenically unsaturated copolymerizable monomer, and the starch used is (d) 15 to 40% by weight of at least one degraded starch having a molar mass Mw of 1000 to 65000 g/mol, wherein the sum (a) + (b) + (c) + (d) = 100% and relates to the total solid matter content, and wherein the polymerization is carried out in the presence of at least 0.01% by weight, relative to the monomers used, of at least one terpene-containing polymerization regulator. The invention further relates to a method for producing the finely divided starch-containing polymer dispersions by means of the emulsion polymerization of monomers (a), (b) and (c) using redox initiators in the presence of (d) degraded starch and at least 0.01% by weight, relative to the monomers used, of at least one terpene-containing polymerization regulator, and to the use of the finely divided starch-containing polymer dispersions as a sizing agent for paper, paperboard and cardboard.

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