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公开(公告)号:KR20200128004A
公开(公告)日:2020-11-11
申请号:KR20207024392
申请日:2019-02-18
Applicant: BASF SE
Inventor: KALO BENEDIKT , MAEURER TORSTEN , VOGELSANG REGINA
IPC: H01M4/36 , H01M4/505 , H01M4/525 , H01M4/62 , H01M10/052
Abstract: 코팅된전극활물질의제조방법으로서, 상기방법은: (a) 일반식 Li1+xTM1-xO2 에따른미립자전극활물질을제공하는단계로서, TM 은 Ni, Co, 및임의로 Mn, 및임의로 Mg, Al, Ba, Ti 및 Zr로부터선택된적어도하나의금속의조합이고, x 는 0 내지 0.2의범위이고, TM 의전이금속의적어도 15 몰% 는 Ni 인, 상기미립자전극활물질을제공하는단계, (b) 상기전극활물질을 M1 의화합물로처리하는단계로서, M1 은용매의유무에관계없이, Li, Al, B, Mg, Si, Sn 으로부터, 그리고전이금속으로부터, 또는전술한것 중적어도 2 개의조합으로부터선택되며, 상기 M1 의화합물은자체적으로캐소드활물질로작용하지않는, 상기전극활물질을처리하는단계, (c) 임의로, 상기미립자전극활물질상에침착되지않는 M1 의화합물을제거하는단계, (d) 단계 (b) 또는 (c) 후에얻은물질을, 해당되는경우, 로터리킬른또는진자킬른에서 300 내지 800 ℃의온도로가열하여후처리를수행하는단계를포함한다.
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2.
公开(公告)号:MX382707B
公开(公告)日:2025-03-13
申请号:MX2015010048
申请日:2015-08-03
Applicant: BASF SE
Inventor: PARVULESCU ANDREI-NICOLAE , RUSLIM FRANKY , UHL GEORG , LÜTZEL HANS-JÜRGEN , CZAJKA PAWEL , VOGELSANG REGINA , BAYER ROBERT , SCHLOSSER ROBERT , MÜLLER ULRICH
Abstract: Un proceso para preparar material zeolítico que contiene boro sin aluminio que comprende la estructura marco MWW (BMWW), que comprende (a) sintetizar hidrotérmicamente el BMWW de una mezcla de síntesis que contiene agua, una fuente de silicio, una fuente de boro y un compuesto de plantilla MWW obteniendo el BMWW en su licor madre, donde el licor madre tiene un pH de más de 9; (b) ajustar el pH del licor madre, obtenido en (a) y que contiene el BMWW, hasta un valor en el rango de 6 a 9; (c) separar el BMWW del licor madre con pH ajustado obtenido en (b) por filtración en un dispositivo de filtración.
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公开(公告)号:CA3144899A1
公开(公告)日:2021-02-04
申请号:CA3144899
申请日:2020-07-24
Applicant: BASF SE
Inventor: ROHDE WOLFGANG , GERKE BIRGIT , VOGELSANG REGINA , VOGES MATTHIAS , SCHIERLE-ARNDT KERSTIN , SEELER FABIAN , ADERMANN TORBEN
Abstract: A process for the recovery of one or more transition metals and lithium from waste lithium ion batteries or parts thereof is disclosed. The process comprising the steps of (a) providing a particulate material containing a transition metal compound and/or transition metal, wherein the transition metal is selected from the group consisting of Ni and Co, and wherein further at least a fraction of said Ni and/or Co, if present, are in an oxidation state lower than +2, e.g. in the metallic state; which particulate material further contains a lithium salt; (b) treating the material provided in step (a) with a polar solvent and optionally an alkaline earth hydroxide; (c) separating the solids from the liquid, optionally followed by a solid-solid separation step; and (d) treating the solids containing the transition metal in a way to dissolve at least part of the Ni and/or Co, typically using a mineral acid, provides good separation of lithium in high purity and of transition metal useful for the production of battery cathode active materials.
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公开(公告)号:CA3144716A1
公开(公告)日:2021-02-04
申请号:CA3144716
申请日:2020-07-24
Applicant: BASF SE
Inventor: ROHDE WOLFGANG , GERKE BIRGIT , SCHIERLE-ARNDT KERSTIN , VOGES MATTHIAS , VOGELSANG REGINA , SEELER FABIAN , SMITH GARETH , ADERMANN TORBEN
Abstract: A process for the recovery of one or more transition metals and lithium from waste lithium ion batteries or parts thereof is disclosed. The process comprising the steps of (a) providing a particulate material containing a transition metal compound and/or transition metal, wherein the transition metal is selected from the group consisting of Ni and Co, and wherein further at least a fraction of said Ni and/or Co, if present, are in an oxidation state lower than +2, e.g. in the metallic state; which particulate material further contains a lithium salt; (b) treating the material provided in step (a) with a polar solvent and optionally an alkaline earth hydroxide; (c) separating the solids from the liquid, optionally followed by a solid-solid separation step; and (d) treating the solids containing the transition metal in a smelting furnace to obtain a metal melt containing Ni and/or Co provides good separation of transition metal as alloy and of lithium in high purity.
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5.
公开(公告)号:SG11201505945UA
公开(公告)日:2015-08-28
申请号:SG11201505945U
申请日:2014-02-05
Applicant: BASF SE
Inventor: PARVULESCU ANDREI-NICOLAE , MÜLLER ULRICH , LÜTZEL HANS-JÜRGEN , UHL GEORG , BAYER ROBERT , VOGELSANG REGINA , SCHLOSSER ROBERT , RUSLIM FRANKY , CZAJKA PAWEL
Abstract: A process for preparing an aluminum-free boron containing zeolitic material comprising the framework structure MWW (BMWW), comprising (a) hydrothermally synthesizing the BMWW from a synthesis mixture containing water, a silicon source, a boron source, and an MWW template compound obtaining the BMWW in its mother liquor, the mother liquor having a pH above 9; (b) adjusting the pH of the mother liquor, obtained in (a) and containing the BMWW, to a value in the range of from 6 to 9; (c) separating the BMWW from the pH-adjusted mother liquor obtained in (b) by filtration in a filtration device.
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公开(公告)号:ES2390364T3
公开(公告)日:2012-11-12
申请号:ES07122809
申请日:2007-12-11
Applicant: BASF SE
Inventor: VOGELSANG REGINA , KAESHAMMER STEFAN DR , EIDEN ULRICH , BRAND ALEXANDRA DR , TUTTELBERG LEMBIT , STAFFEL WOLFGANG
IPC: C07D207/267
Abstract: Procedimiento para la obtención de un compuesto N-vinílico seleccionado a partir de N-vinilamidas cíclicas y vinilamidas no cíclicas de la fórmula I donde R1 representa un átomo de H o un grupo alquilo con 1 a 4 átomos de carbono, y R2 representa un grupo alquilo con 1 a 10 átomos de carbono, mediante vinilación de un compuesto con al menos un átomo de nitrógeno, a continuación denominado compuesto de manera abreviada, con acetileno, caracterizado porque - el compuesto se hace reaccionar con un hidróxido alcalino antes de la vinilación en una zona de reacción, y - el tiempo de residencia medio del hidróxido alcalino y del compuesto en la zona de reacción es menor que 6 minutos.
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公开(公告)号:AU2020323677A1
公开(公告)日:2022-02-17
申请号:AU2020323677
申请日:2020-07-24
Applicant: BASF SE
Inventor: ROHDE WOLFGANG , GERKE BIRGIT , VOGELSANG REGINA , VOGES MATTHIAS , SCHIERLE-ARNDT KERSTIN , SEELER FABIAN , ADERMANN TORBEN
Abstract: A process for the recovery of one or more transition metals and lithium from waste lithium ion batteries or parts thereof is disclosed. The process comprising the steps of (a) providing a particulate material containing a transition metal compound and/or transition metal, wherein the transition metal is selected from the group consisting of Ni and Co, and wherein further at least a fraction of said Ni and/or Co, if present, are in an oxidation state lower than +2, e.g. in the metallic state; which particulate material further contains a lithium salt; (b) treating the material provided in step (a) with a polar solvent and optionally an alkaline earth hydroxide; (c) separating the solids from the liquid, optionally followed by a solid-solid separation step; and (d) treating the solids containing the transition metal in a way to dissolve at least part of the Ni and/or Co, typically using a mineral acid, provides good separation of lithium in high purity and of transition metal useful for the production of battery cathode active materials.
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公开(公告)号:PL2953897T3
公开(公告)日:2022-01-03
申请号:PL14703571
申请日:2014-02-05
Applicant: BASF SE
Inventor: PARVULESCU ANDREI-NICOLAE , MÜLLER ULRICH , LÜTZEL HANS-JÜRGEN , UHL GEORG , BAYER ROBERT , VOGELSANG REGINA , SCHLOSSER ROBERT , RUSLIM FRANKY , CZAJKA PAWEL
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