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    FORMED PRODUCT BASED ON SILICON DIOXIDE, PRODUCTION AND USE THEREOF, SUPPORTED CATALYST FOR PRODUCTION OF VINYL ACETATE MONOMER, PRODUCTION AND USE OF THE SUPPORTED CATALYST
    1.
    发明专利
    FORMED PRODUCT BASED ON SILICON DIOXIDE, PRODUCTION AND USE THEREOF, SUPPORTED CATALYST FOR PRODUCTION OF VINYL ACETATE MONOMER, PRODUCTION AND USE OF THE SUPPORTED CATALYST 失效

    公开(公告)号：JP2000086335A

    公开(公告)日：2000-03-28

    申请号：JP18081099

    申请日：1999-06-25

    Applicant: DEGUSSA

    Inventor： TACKE THOMAS DR ,  SCHINKE PETER ,  ROTGERINK HANS LANSINK DR ,  KRAUSE HELMFRIED

    IPC: C04B35/16 ,  B01J19/30 ,  B01J20/10 ,  B01J21/08 ,  B01J35/02 ,  C04B35/632 ,  C04B35/64 ,  C07C67/055 ,  C07C69/15

    Abstract: PROBLEM TO BE SOLVED: To minimize the pressure drop, give the small bulk density and a relatively large outer surface area and permit improved mass transfer and heat transfer by forming stays or spokes extending from the inner wall of the hollow cylinder toward the center for strengthening the inside or forming a plurality of passageways. SOLUTION: The molded body of a wheel shape has an outer diameter d1 of 1-25 mm, the ratio of height to the outer diameter d1 of 0.2-5, the wall thickness [(d1-d2)×0.5] of 0.05-0.5×d1, the thickness of the stay or spoke d3 of 0.05-0.3×d1 and the number of the stays or spokes or the passageways of at least 3. The molded body is formed by kneading the base of silicon dioxide produced by thermal decomposition, forming the silicon dioxide by means of a single or twine screw extruder and strand-pressing formed silicon dioxide into a hollow cylinder in a wheel shape. Then, the strand-pressed produce is cut in a desired thickness and they are heat-treated at 400-1,200 deg.C for 30 minutes-10 hours. The molded body is allowed to carry a catalytically active component such as Pd/alkali/Au system or the like to give the objective supported catalyst that attains the high space time yield and the high selectivity in the production of vinyl acetate.

    POSTTREATMENT OF 1-(N2-((3754/24)S)-ETHOXYCARBONYL)-3-PHENYLPROPYL)-N6-TRIFLUOROACETYL)-L-LYSYL-L-PROLINE
    2.
    发明专利
    POSTTREATMENT OF 1-(N2-((3754/24)S)-ETHOXYCARBONYL)-3-PHENYLPROPYL)-N6-TRIFLUOROACETYL)-L-LYSYL-L-PROLINE 失效

    公开(公告)号：JPH1171394A

    公开(公告)日：1999-03-16

    申请号：JP17487698

    申请日：1998-06-22

    Applicant: DEGUSSA

    Inventor： TANNER HERBERT ,  DRAUZ KARLHEINZ ,  STINGL KLAUS DR ,  SATOR GERHARD DR ,  BETHGE HORST ,  MOELLER ROLAND ,  TACKE THOMAS DR ,  REHREN CLAUS DR

    IPC: C07K1/36 ,  C07K5/02 ,  C07K5/068

    Abstract: PROBLEM TO BE SOLVED: To obtain the subject compound useful as an intermediate or the like for producing a blood pressure regulator by posttreating a crude substance from a production process for a specific N-substituted-L-lysyl-L-proline with liquid or supercritical CO2 . SOLUTION: A crude substance from a production process for a 1-[N2-((S)- ethoxycarbonyl)-3-phenylpropyl)-N6-trifluoroacetyl]-L-lysyl-L-proline (LPE) in which the LPE is enriched and present is precharged into an extraction container C and supercritical CO2 or liquid CO2 prepared by making liquid CO2 flow from a collection container D to a pump P1 , compressing the liquid CO2 to an extraction pressure and heating the compressed liquid CO2 to an extraction temperature with a heat exchanger E1 is fed to the extraction container C to dissolve an extractible substance in the CO2 during the passage thereof through the extraction container C. The CO2 loaded with the dissolved substance is then led to a separator S and the pressure or temperature or both are changed to deposit the extracted substance. Thereby, the LPE which is an intermediate for an inhibitor of angiotensin converting enzymes effectively useful as a blood pressure regulator is obtained in a short time.

    CATALYTIC REACTION OF ORGANIC COMPOUND
    8.
    发明专利
    CATALYTIC REACTION OF ORGANIC COMPOUND 失效

    公开(公告)号：JPH10316592A

    公开(公告)日：1998-12-02

    申请号：JP12867898

    申请日：1998-05-12

    Applicant: DEGUSSA

    Inventor： TACKE THOMAS DR ,  ROEDER STEFAN ,  BEUL INGE ,  LAPORTE STEFFEN ,  PANSTER PETER DR

    IPC: B01J23/44 ,  C07B35/02 ,  C07B61/00 ,  C07C51/36 ,  C07C67/303 ,  C11B3/00 ,  C11C3/12

    Abstract: PROBLEM TO BE SOLVED: To provide a method, for continuously carrying out a catalytic reaction of one or more organic compounds contained in starting materials which are formed together with an unfavorable accompanying material. SOLUTION: A desirable organic compound in starting materials is intentionally extracted using a condensed fluid, optionally another reaction component being added, and an extract consisting of the condensed fluid and the compound as a reaction mixture is brought on a catalyst, the organic compound is catalytically reacted using the catalyst to convert the compound into a production mixture consisting of individual products of catalytic reaction, the product mixture is separated from the reaction mixture, and the fluid used above is optionally returned to the extraction process. As shown by low sulfur content and clearly improved acid value, extremely high purity of the extract is achieved.

    9.
    发明专利
    未知

    公开(公告)号：AT215845T

    公开(公告)日：2002-04-15

    申请号：AT99112026

    申请日：1999-06-22

    Applicant: DEGUSSA

    Inventor： TACKE THOMAS DR ,  SCHINKE PETER ,  ROTGERINK HERMANUS LANSINK DR ,  KRAUSE HELMFRIED

    IPC: C04B35/16 ,  B01J19/30 ,  B01J20/10 ,  B01J21/08 ,  B01J35/02 ,  C04B35/632 ,  C04B35/64 ,  C07C67/055 ,  C07C69/15

    Abstract: Moldings based on silica having a hollow cylindrical configuration with internal reinforcing stays or spokes leading from an inner wall of a hollow cylinder to the center of the molding or in the form of miniliths having passageway channels therethrough, are produced by homogenizing silica with methyl hydroxyethyl cellulose, wax and/or polyethylene glycol. Water and optionally aqueous alkaline ammonia solution are added, and the mixture is subjected to kneading and forming, extruding, optionally cutting the extrudate to the desired length by means of a cutting device, drying at a temperature from 20 to 150° C., and annealing for a period from 30 minutes to 10 hours at a temperature of 400 to 1200° C. The moldings can be used as catalyst supports for the production of unsaturated esters from olefins, organic acids and oxygen in the gas phase and and can be used in particular for the production of vinyl acetate monomer.

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