Abstract:
The invention relates to a pressure vessel, having: a reaction chamber (2) as a pressure space for the initiation and/or facilitation of chemical and/or physical pressure reactions of samples (P) accommodated in the reaction chamber (2); a fluid inlet (20) with a feed valve (21) which is adjustable between an open position, for the feed of a fluid, preferably a flushing gas, into the reaction chamber (2), and a closed position, for stopping the feed of the fluid; a fluid outlet (30) with a discharge valve (31), which is adjustable between an open position, for the discharge of a fluid out of the reaction chamber (2), and a closed position, for stopping the discharge of the fluid out of the reaction chamber (2); and an oxygen sensor (33) for detecting an oxygen content in the reaction chamber (2). The pressure vessel (1) furthermore has a control device which is configured to control the feed valve (21) and the discharge valve (31) on the basis of the oxygen content detected by the oxygen sensor (33), such that the reaction chamber (2) is flushed via the feed and discharge valves (21, 31) situated in the open position, and at least the discharge valve (31) switches from the open position into the closed position as soon as a predetermined oxygen content is undershot. The invention also relates to a corresponding method.
Abstract:
A SCWO reactor fouling prevention and mitigation system that includes at least one feedstock tee which provides a feedstock to the SCWO reactor, at least one feedstock tee pressure sensor, such that each of the at least one feedstock tee has one of the at least one feedstock tee pressure sensor, at least one pressure sensor proximate a SCWO reactor inlet, and at least one pressure sensor proximate a SCWO reactor outlet. Also included is a controller which triggers a Clean In Place (CIP) procedure when there is a pressure difference between any two of the following, the SCWO reactor inlet, the at least one feedstock tee, and the SCWO reactor outlet. The CIP procedure includes washing a portion of the SCWO reactor with a fluid supplied through the at least one feedstock tee.
Abstract:
The present invention provides an automated experiment apparatus and an automated experiment method using the same for putting a sample into a pressure vessel and automatically performing a chemical and/or physical reaction of the sample under a predetermined temperature and pressure. According to the embodiments of the present disclosure, it is possible to automatically perform an experiment from the beginning to the end without intervention of an user. As a result, it is possible to prevent a risk of gas leakage and human exposure to a harmful gas due to a manual operation. The apparatus comprises a controller which is configured to automatically perform a reaction process under a predetermined temperature and pressure in a state in which a sample holding member is air-tightly fixed to a pressure vessel and the sample is accommodated in a sample receiving chamber of the pressure vessel.
Abstract:
Reactor for the synthesis of melamine from urea, in accordance with the high-pressure non-catalytic process, comprising: a vertical reactor body (1), at least one inlet (2) for the urea melt, a set of heating elements (3), and a central duct (7), said set of heating elements (3) being arranged inside said central duct.
Abstract:
Supercritical upgrading reactors and reactor systems for upgrading a petroleum-based compositions comprising one or more catalyst layers and, in some embodiments, one or more purging fluid inlets, where one or more catalyst layers at least partially sift and convert heavy hydrocarbon fractions to light hydrocarbon fractions to produce an upgraded supercritical reactor product. In some embodiments, upgrading reactor systems comprise one or more supercritical upgrading reactors and one or more supercritical standby reactors alternating functions such that a supercritical upgrading reactor is converted to a supercritical standby reactor and the supercritical standby reactor is converted to a supercritical upgrading reactor, where the supercritical upgrading reactor upgrades a combined feed stream while a supercritical standby reactor delivers a cleaning fluid into the supercritical standby reactor.
Abstract:
A slurry-transporting facility equipped with a plurality of pump-equipment circuits, whereby a stop of slurry supply to a transport destination at the time of switchover between the pump-equipment circuits for use is prevented to make an efficient operation possible. The slurry-transporting facility includes: pipe arrangements which branch out from a feed tank into the plurality of circuits; a transport pump provided in each of the pipe arrangement; a first valve provided upstream from the transport pump; a second valve provided downstream from the transport pump; and a uniting pipe arrangement formed by joining of the pipe arrangements at a predetermined position and connected to a LT heater. The uniting pipe arrangement is provided with a third valve configured to control the transportation of ore slurry to the LT heater and a pressure gauge configured to measure a pressure in the uniting pipe arrangement.
Abstract:
Compositions are provided that include having at least 95% by weight of a taxane, or a pharmaceutically acceptable salt thereof, where the particles have a mean bulk density between about 0.050 g/cm3 and about 0.15 g/cm3, and/or a specific surface area (SSA) of at least 18 m2/g, 20 m2/g, 25 m2/g, 30 m2/g, 32 m2/g, 34 m2/g, or 35 m2/g. Methods for making and using such compositions are also provided.
Abstract:
Provided is a discharge device for discharging pretreated biomass from a pressurized reactor. The device comprises: a vessel having an opening to a high pressure region at the top, and configured to be connected with a pressurized biomass pretreatment device; one or more inlet openings situated along the sides of the vessels through which water or liquid may be added; an orifice or valve at a lower part of said vessel, said orifice or valve being configured to eject pretreated biomass, optionally into a pipeline. The discharge device is characterised in that it comprises mechanical agitation means, said agitation means comprising an agitation element arranged in the interior of said vessel at a lower part of said vessel, and being configured to provide agitation of the content of said vessel, wherein said agitation means being adapted to withstand a pressure in the interior of a said vessel of 10 bar or more. The agitation means provides for a temperature equalization within a specific vertical range of heights of an aqueous slurry present in said vessel, thereby eliminating disadvantages of the prior art devices and methods.
Abstract:
A slurry-transporting facility equipped with a plurality of pump-equipment circuits, whereby a stop of slurry supply to a transport destination at the time of switchover between the pump-equipment circuits for use is prevented to make an efficient operation possible. The slurry-transporting facility includes: pipe arrangements which branch out from a feed tank into the plurality of circuits; a transport pump provided in each of the pipe arrangement; a first valve provided upstream from the transport pump; a second valve provided downstream from the transport pump; and a uniting pipe arrangement formed by joining of the pipe arrangements at a predetermined position and connected to a LT heater. The uniting pipe arrangement is provided with a third valve configured to control the transportation of ore slurry to the LT heater and a pressure gauge configured to measure a pressure in the uniting pipe arrangement.
Abstract:
Disclosed is a hydrothermal synthesis device for continuously preparing an inorganic slurry using a hydrothermal method. The hydrothermal synthesis device includes a mixer to mix at least one precursor solution for preparing an inorganic material, injected via at least one supply tube, to prepare an intermediate slurry, a connection tube provided at a side of the mixer, continuously discharging the prepared intermediate slurry to a reactor, and having an inner surface contacting a precursor solution mixture on which abrasive polishing has been performed, and the reactor performing hydrothermal reaction of the intermediate slurry supplied from the connection tube by receiving a liquid stream heated to supercritical or subcritical conditions using a heat exchanger and connected to the connection tube into which the intermediate slurry prepared from the mixer is introduced and to at least one injection tube into which the heated liquid stream is injected.