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    Metal-silica sol-gel materials
    31.
    发明授权
    Metal-silica sol-gel materials 失效
    金属硅溶胶凝胶材料

    公开(公告)号：US06391808B1

    公开(公告)日：2002-05-21

    申请号：US08226819

    申请日：1994-04-12

    Applicant: Albert E. Stiegman

    Inventor： Albert E. Stiegman

    IPC: C03L300

    CPC classification number: C03C3/06 ,  C03C1/006 ,  C03C14/00 ,  C03C2201/40 ,  C03C2214/08 ,  C03C2214/12

    Abstract: The present invention relates to a single phase metal-silica sol-gel glass formed by the co-condensation of a transition metal with silicon atoms where the metal atoms are uniformly distributed within the sol-gel glass as individual metal centers. Any transition metal may be used in the sol-gel glasses. The present invention also relates to sensor materials where the sensor material is formed using the single phase metal-silica sol-gel glasses. The sensor materials may be in the form of a thin film or may be attached to an optical fiber. The present invention also relates to a method of sensing chemicals using the chemical sensors by monitoring the chromatic change of the metal-silica sol-gel glass when the chemical binds to the sensor. The present invention also relates to oxidation catalysts where a metal-silica sol-gel glass catalyzes the reaction. The present invention also relates to a method of performing oxidation reactions using the metal-silica sol-gel glasses. The present invention also relates to organopolymer metal-silica sol-gel composites where the pores of the metal-silica sol-gel glasses are filled with an organic polymer polymerized by the sol-gel glass.

    Abstract translation: 本发明涉及通过过渡金属与硅原子的共缩合形成的单相金属硅溶胶 - 凝胶玻璃，其中金属原子作为各个金属中心均匀分布在溶胶 - 凝胶玻璃内。 任何过渡金属都可用于溶胶 - 凝胶玻璃。本发明还涉及使用单相金属硅溶胶凝胶玻璃形成传感器材料的传感器材料。 传感器材料可以是薄膜的形式，也可以附着在光纤上。 本发明还涉及当化学物质与传感器结合时，通过监测金属硅溶胶 - 凝胶玻璃的色度变化来使用化学传感器感测化学品的方法。本发明还涉及氧化催化剂，其中金属二氧化硅 溶胶 - 凝胶玻璃催化反应。 本发明还涉及使用金属硅溶胶 - 凝胶玻璃进行氧化反应的方法。本发明还涉及其中填充了金属硅溶胶 - 凝胶玻璃的孔的有机聚合物金属 - 硅溶胶 - 凝胶复合物 与溶胶 - 凝胶玻璃聚合的有机聚合物。

    Infrared absorbing glass, and it's fabrication method
    32.
    发明授权
    Infrared absorbing glass, and it's fabrication method 有权
    红外吸收玻璃，它的制作方法

    公开(公告)号：US06342460B1

    公开(公告)日：2002-01-29

    申请号：US09336678

    申请日：1999-06-21

    Applicant: Yoshinobu Akimoto ,  Hiroaki Kinoshita

    Inventor： Yoshinobu Akimoto ,  Hiroaki Kinoshita

    IPC: C03C304

    CPC classification number: C03C1/006 ,  C03B19/12 ,  C03B2201/40 ,  C03B2201/50 ,  C03C3/06 ,  C03C3/078 ,  C03C4/082 ,  C03C13/046 ,  C03C2201/30 ,  C03C2201/40 ,  C03C2201/50 ,  C03C2203/20 ,  Y10S501/905

    Abstract: The invention relates to a glass excellent in infrared absorption capability and corrosion resistance, and its fabrication process. A compound of divalent copper and a compound of a metal species for a network modifier oxide are introduced in a wet gel. Then, the wet gel is dipped in a dipping solution having a low solubility with respect to the compound of divalent copper and the compound of a metal species for a network modifier oxide for the precipitation in the wet gel of the divalent-t copper compound and the compound of a metal species for a network modifier oxide, followed by drying and firing. Thus, an infrared absorbing glass comprising 70 to 98 mol % of SiO2, 1 to 12 mol % of CuO and 1 to 18 mol % of a network modifier oxide other than CuO is fabricated.

    Abstract translation: 本发明涉及一种红外吸收能力和耐腐蚀性优异的玻璃及其制造工艺。 将二价铜的化合物和用于网络改性剂氧化物的金属物质的化合物引入湿凝胶中。 然后，将湿凝胶浸入相对于二价铜化合物的低溶解度的浸渍溶液和用于网络改性剂氧化物的金属物质的化合物，用于在二价铜化合物的湿凝胶中沉淀，以及 用于网络改性剂氧化物的金属物质的化合物，随后进行干燥和烧制。 因此，制造包含70〜98摩尔％的SiO 2，1〜12摩尔％的CuO和1〜18摩尔％的CuO以外的网络改性剂氧化物的红外线吸收玻璃。

    Method of producing optical quality glass having a selected refractive index
    34.
    发明授权
    Method of producing optical quality glass having a selected refractive index 失效
    制备具有选定折射率的光学品质玻璃的方法

    公开(公告)号：US6158244A

    公开(公告)日：2000-12-12

    申请号：US39450

    申请日：1998-03-16

    Applicant: John F. Poco ,  Lawrence W. Hrubesh

    Inventor： John F. Poco ,  Lawrence W. Hrubesh

    IPC: C03B8/02 ,  C03B19/12 ,  C03C1/00 ,  C03C3/06 ,  C03C11/00

    CPC classification number: C03C1/006 ,  C03B19/12 ,  C03C11/00 ,  C03C3/06 ,  C03C2201/32 ,  C03C2201/40 ,  C03C2201/42 ,  C03C2203/26

    Abstract: Optical quality glass having a selected refractive index is produced by a two stage drying process. A gel is produced using sol-gel chemistry techniques and first dried by controlled evaporation until the gel volume reaches a pre-selected value. This pre-selected volume determines the density and refractive index of the finally dried gel. The gel is refilled with solvent in a saturated vapor environment, and then dried again by supercritical extraction of the solvent to form a glass. The glass has a refractive index less than the full density of glass, and the range of achievable refractive indices depends on the composition of the glass. Glasses having different refractive indices chosen from an uninterrupted range of values can be produced from a single precursor solution.

    Abstract translation: 具有选择的折射率的光学品质的玻璃是通过两阶段干燥方法制造的。 使用溶胶 - 凝胶化学技术制备凝胶，并首先通过受控蒸发干燥直到凝胶体积达到预先选择的值。 该预选择的体积确定最终干燥的凝胶的密度和折射率。 在饱和蒸汽环境中用溶剂重新填充凝胶，然后通过超临界萃取溶剂再次干燥以形成玻璃。 玻璃的折射率小于玻璃的全密度，可实现折射率的范围取决于玻璃的组成。 可以从单一前体溶液产生具有从不间断值范围选择的折射率不同的玻璃。

    Doped silica glass
    35.
    发明授权
    Doped silica glass 失效
    掺杂二氧化硅玻璃

    公开(公告)号：US6136736A

    公开(公告)日：2000-10-24

    申请号：US858872

    申请日：1997-05-19

    Applicant: Mohan Rajaram ,  Curtis E. Scott

    Inventor： Mohan Rajaram ,  Curtis E. Scott

    IPC: C03C3/06 ,  H01J61/30 ,  C03C13/04

    CPC classification number: H01J61/302 ,  C03C3/06 ,  C03C2201/34 ,  C03C2201/40

    Abstract: A metal halide or mercury lamp including an arc tube comprised of a glass composition consisting essentially of at least 90 weight percent SiO.sub.2 and including between about 10 and 1000 parts per million of a trivalent element slected from the group consisting of Pr, Nd, Pm, Sm, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Ac, Th, Pa, U, Np, Pu, Am, Cm, Bk, Cf, Es, Fm, Md, No, Lr, Unq, Unp, Ga, and mixtures thereof such that the viscosity of the glass composition is greater than 10.sup.14.5 poise at 1100.degree. C.

    Abstract translation: 一种金属卤化物或汞灯，包括由玻璃组合物构成的电弧管，所述玻璃组合物基本上由至少90重量％的SiO 2组成，并且包括约10至1000ppm的三价元素，所述三价元素选自Pr，Nd，Pm， Sm，Gd，Tb，Dy，Ho，Er，Tm，Yb，Lu，Ac，Th，Pa，U，Np，Pu，Am，Cm，Bk，Cf，Es，Fm，Md，No，Lr，Unq， Unp，Ga及其混合物，使玻璃组合物的粘度在1100℃下大于1014.5泊。

    Fixation by ion exchange of toxic materials in a glass matrix
    39.
    发明授权
    Fixation by ion exchange of toxic materials in a glass matrix 失效
    通过玻璃基质中有毒物质的离子交换固定

    公开(公告)号：US4469628A

    公开(公告)日：1984-09-04

    申请号：US370437

    申请日：1982-04-21

    Applicant: Catherine J. Simmons ,  Joseph H. Simmons ,  Pedro B. Macedo ,  Theodore A. Litovitz

    Inventor： Catherine J. Simmons ,  Joseph H. Simmons ,  Pedro B. Macedo ,  Theodore A. Litovitz

    IPC: B01D15/00 ,  B01J39/02 ,  B01J39/10 ,  B01J39/14 ,  C02F1/42 ,  G21F9/12 ,  G21F9/16 ,  G21F9/30 ,  C09K3/00 ,  C09K11/04

    CPC classification number: C03C1/002 ,  B01J39/14 ,  C03C1/026 ,  C03C11/005 ,  C03C21/001 ,  C03C23/0095 ,  C03C3/06 ,  C03C3/061 ,  C03C3/089 ,  G21F9/12 ,  G21F9/305 ,  C03C2201/10 ,  C03C2201/20 ,  C03C2201/23 ,  C03C2201/3435 ,  C03C2201/40 ,  C03C2201/50

    Abstract: This invention relates to the immobilization of toxic, e.g., radioactive, materials in a silicate glass or silica gel matrix for extremely long periods of time. Toxic materials, such as radioactive wastes containing radioactive cations, which may be in the form of liquids, or solids dissolved or dispersed in liquids or gases, are incorporated into a glass or silica gel matrix, having alkali metal, Group Ib metal and/or ammonium cations bonded to silicon atoms of said glass or silica gel through divalent oxygen linkages, by a process which involves the ion exchange of said toxic or radioactive cations with said alkali metal, Group Ib metal and/or ammonium cations to bind said toxic or radioactive cations to silicon atoms of said glass or silica gel through said silicon-bonded divalent oxygen linkages. Thereafter, the resulting glass or silica gel now characterized by toxic or radioactive cations bonded to silicon atoms through divalent oxygen linkages can be stored, or packaged in suitable containers, or disposed of as by burial, and/or sintered to collapse the pores thereof.

    Abstract translation: 本发明涉及将硅酸盐玻璃或硅胶基质中的有毒的，例如放射性物质固定在极长时间内。 将含有放射性阳离子的放射性废物（其可以是液体的形式）或溶解或分散在液体或气体中的固体的有毒材料掺入玻璃或硅胶基质中，其具有碱金属，Ib族金属和/或 通过涉及所述有毒或放射性阳离子与所述碱金属，第Ib族金属和/或铵阳离子离子交换以结合所述有毒或放射性的方法的方法，通过二价氧键与所述玻璃或硅胶的硅原子键合的铵阳离子 通过所述硅键合的二价氧键与所述玻璃或硅胶的硅原子的阳离子。 此后，所得到的玻璃或硅胶的特征在于通过二价氧键与硅原子键合的有毒或放射性阳离子，可以储存或包装在合适的容器中，或通过埋置和/或烧结来处理以使其孔隙折叠。

    Thermally stable quartz glass
    40.
    发明授权
    Thermally stable quartz glass 失效
    耐热稳定的石英玻璃

    公开(公告)号：US4104045A

    公开(公告)日：1978-08-01

    申请号：US702835

    申请日：1976-07-06

    Applicant: Manfred Mansmann

    Inventor： Manfred Mansmann

    IPC: C03B37/01 ,  C03C3/06 ,  C03C3/076 ,  C03C13/00 ,  C04B35/622 ,  C03B37/00 ,  C03B32/00 ,  C04B35/64

    CPC classification number: C04B35/6224 ,  C03B37/011 ,  C03C13/00 ,  C03C3/06 ,  C03C2201/40 ,  C03C2203/22

    Abstract: Quartz glass of high thermal stability is produced from a SiO.sub.2 solution or sol which is substantially free of alkali and alkaline earth metal oxides and contains chromium and/or manganese in about 0.05 to 20% by weight of the SiO.sub.2 expressed as Cr.sub.2 O.sub.3 and Mn.sub.2 O.sub.3. The quartz glass upon heating above 1100.degree. C forms cristobalite having an average crystallite size of about 100 to 500 A. Articles therefrom retain their physical and mechanical properties at high temperatures. The materials are suited for producing fibers by the usual methods of spinning from solutions or sols and, as such, or as fibers they are suited for use in reinforcement and insulation and in making flameproof textiles.

    Abstract translation: 具有高热稳定性的石英玻璃由基本上不含碱金属和碱土金属氧化物的SiO 2溶液或溶胶制成，并且含有以Cr2O3和Mn2O3表示的约0.05至20重量％的铬和/或锰。 在1100℃以上加热的石英玻璃形成平均微晶尺寸为约100至500的方石石。其制品在高温下保持其物理和机械性能。 这些材料适用于通过从溶液或溶胶中旋转的通常方法，或者作为适合用于加强和绝缘以及制造防火织物的纤维来生产纤维。

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