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    Use of olefinic imines to scavenge sulfur species
    33.
    发明授权
    Use of olefinic imines to scavenge sulfur species 失效
    使用烯属亚胺清除硫物质

    公开(公告)号：US5567212A

    公开(公告)日：1996-10-22

    申请号：US430208

    申请日：1995-04-27

    Applicant: David R. Gentry ,  Gerald T. Pancio ,  Jerry J. Weers

    Inventor： David R. Gentry ,  Gerald T. Pancio ,  Jerry J. Weers

    IPC: C10G21/20 ,  C09K8/532 ,  C10G29/20 ,  C10L1/228 ,  C10L1/22

    CPC classification number: C10L1/2283 ,  C09K8/532 ,  C10G29/20

    Abstract: A method for scavenging sulfur species from a petroleum-derived medium is disclosed. The method comprises contacting the medium with sulfur species scavenging amount of an imine of the formula ##STR1## wherein x is an integer from 1 to 10, R' is an organic moiety having a number of valences equal to x, R.sub.1 is hydrogen or a mono-valent organic moieties and R is a mono-valent olefin moiety, provided that R and R.sub.1 contain a total of from about four to about forty carbon atoms. In an alternative embodiment, the imine is produced by a condensation reaction between an amine having at least one primary amino group and a carbonyl of the formula ##STR2## wherein R.sub.1 is hydrogen or a mono-valent organic moieties and R is a mono-valent olefin moiety, provided that R and R.sub.1 contain a total of from about four to about forty carbon atoms. In yet other embodiments, the imine is produced by a condensation reaction between an amine having at least one primary amino group and an aldehyde having at least one alpha-hydrogen in an aldehyde to primary amino group molar ratio of at least about 2:1, are also disclosed.

    Abstract translation: 公开了一种从石油衍生的介质中清除硫物质的方法。 该方法包括使培养基与清除硫的物质接触式为式的亚胺，其中x是1至10的整数，R'是具有等于x的价数的有机部分，R 1是氢或 一价有机部分，R是一价烯烃部分，条件是R和R 1含有总共约4至约40个碳原子。 在另一个实施方案中，亚胺是通过具有至少一个伯氨基的胺和式的羰基之间的缩合反应产生的，其中R1是氢或一价有机部分，R是一价的 烯烃部分，条件是R和R 1含有总共约4至约40个碳原子。 在其它实施方案中，亚胺通过具有至少一个伯氨基的胺与具有至少一个α-羟基的醛与醛与伯氨基摩尔比至少约2:1的缩合反应产生， 也被披露。

    Additives for aviation and similar fuels
    36.
    发明授权
    Additives for aviation and similar fuels 失效
    航空和类似燃料添加剂

    公开(公告)号：US4233035A

    公开(公告)日：1980-11-11

    申请号：US924718

    申请日：1978-07-14

    Applicant: Edward A. Allen ,  Peter C. Phillips ,  Terence Smithson

    Inventor： Edward A. Allen ,  Peter C. Phillips ,  Terence Smithson

    IPC: C07C45/46 ,  C07C45/51 ,  C07C47/565 ,  C07C49/83 ,  C10L1/228 ,  C10L1/23 ,  C10L1/22

    CPC classification number: C07C45/513 ,  C07C45/46 ,  C07C47/565 ,  C07C49/83 ,  C10L1/2283 ,  C10L1/23

    Abstract: A hydrocarbon fuel, especially a copper-sweetened aviation jet fuel, contains a metal deactivator which is an oxime of either an orthohydroxy aromatic ketone or .alpha.-hydroxy aliphatic ketone, or an imine of a diamine with an ortho hydroxy aromatic ketone, an alkyl substituted ortho hydroxy aromatic aldehyde or a -diketone. Preferred materials include oximes of 2-hydroxy-5-t-butyl benzophenone and 2-hydroxy-5-nonyl acetophenene and di-imines of ethylene and propylene diamines with benzoyl acetone, 5-t-octylsalicylaldehye or 2-hydoroxy-5-methyl butyrophenone.The metal de-activator is added in conventional proportions, typically about 5 to 10 ppm (by weight) to the fuel which may contain either conventional additives such as anti-static, anti-icing and corrosion inhibiting additives.

    Abstract translation: 碳氢化合物燃料，特别是铜加速的航空喷气燃料，含有金属钝化剂，它是邻羟基芳族酮或α-羟基脂族酮的肟或具有邻羟基芳族酮的二胺的亚胺，取代的烷基 邻羟基芳族醛或二酮。 优选的材料包括2-羟基-5-叔丁基二苯甲酮和2-羟基-5-壬基苯乙烯的肟和乙烯和丙烯二胺与苯甲酰丙酮，5-叔辛基水杨基阴离子或2-羟基-5-甲基 丁酰苯。 以常规比例添加金属去活化剂，通常为可含有常规添加剂如防静电，防结冰和腐蚀抑制添加剂的燃料的约5至10ppm（重量）。

    Multiple metal deactivators, method for preparing, and use thereof
    37.
    发明授权
    Multiple metal deactivators, method for preparing, and use thereof 失效
    多种金属钝化剂，其制备方法和用途

    公开(公告)号：US4087256A

    公开(公告)日：1978-05-02

    申请号：US758643

    申请日：1977-01-12

    Applicant: Theodore C. Shields

    Inventor： Theodore C. Shields

    IPC: C10L1/22 ,  C10L1/228

    CPC classification number: C10L1/2283 ,  C10L1/221

    Abstract: Disclosed is a reaction product and method for making same for use in supressing the ability of solubilized copper, iron, cobalt, nickel, chromium and manganese present in hydrocarbon liquids, such as gasoline and fuel oil, to catalyze oxidative degradation. The reaction product is obtained by reacting a 1,2-alkane diamine, a 2,4-dione and an ortho-hydroxy aromatic aldehyde, in stoichiometric proportions, preferably in an inert liquid medium. A preferred reaction product is that obtained by reacting ethylenediamine, 2,4-pentanedione and salicylaldehyde in a 1 to 1 to 1 mole ratio.

    Abstract translation: 公开了一种用于抑制存在于诸如汽油和燃料油的烃液体中溶解的铜，铁，钴，镍，铬和锰的溶解能力的反应产物和方法，用于催化氧化降解。 该反应产物是通过以化学计量比与1,2-烷烃二胺，2,4-二酮和邻羟基芳族醛反应而获得的，优选在惰性液体介质中。 优选的反应产物是以1:1-1摩尔比使乙二胺，2,4-戊二酮和水杨醛反应得到。

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