公开(公告)号：US10011735B2

公开(公告)日：2018-07-03

申请号：US14419324

申请日：2013-03-01

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Thomas P. Klun ,  Alan K. Nachtigal ,  Joseph C. Spagnola ,  Mark A. Roehrig ,  Jennifer K. Schnobrich ,  Guy D. Joly ,  Christopher S. Lyons

IPC: H01L51/00 ,  C09D143/04 ,  C07F7/18 ,  H01L51/52 ,  H01L51/44 ,  H01L51/10 ,  B05D3/06 ,  B32B27/30 ,  C08J7/04 ,  C09D133/14 ,  B05D1/00 ,  B05D3/10 ,  C08K3/34 ,  C09D135/02 ,  C23C14/08 ,  C23C14/34 ,  C23C16/40 ,  C23C16/44 ,  C08F130/08 ,  C09J133/14

CPC classification number: C09D143/04 ,  B05D1/60 ,  B05D3/067 ,  B05D3/068 ,  B05D3/101 ,  B32B27/308 ,  B32B2250/04 ,  B32B2307/7242 ,  B32B2307/7244 ,  C07F7/1804 ,  C08F130/08 ,  C08J7/045 ,  C08J2333/12 ,  C08K3/34 ,  C09D133/14 ,  C09D135/02 ,  C09J133/14 ,  C23C14/08 ,  C23C14/34 ,  C23C16/40 ,  C23C16/44 ,  H01L51/004 ,  H01L51/107 ,  H01L51/448 ,  H01L51/5253 ,  Y10T428/1064 ,  Y10T428/31507 ,  Y10T428/31551 ,  Y10T428/31609 ,  Y10T428/31663

Abstract: Diurethane (meth)acrylate-silane precursor compounds prepared by reacting a primary or secondary aminosilane with a cyclic carbonate to yield a hydroxylalkylene-carbamoylalkylene-alkoxysilanes (referred to as a “hydroxylcarbamoylsilane”), which is reacted with a (meth)acrylated material having isocyanate functionality, either neat or in solvent, and optionally with a catalyst, such as a tin compound. Also described are articles including a substrate, a base (co)polymer layer on a major surface of the substrate, an oxide layer on the base (co)polymer layer; and a protective (co)polymer layer on the oxide layer, the protective (co)polymer layer including the reaction product of at least one diurethane (meth)acrylate-silane precursor compound. The substrate may be a (co)polymer film or an electronic device such as an organic light emitting device, electrophoretic light emitting device, liquid crystal display, thin film transistor, or combination thereof. Methods of making the diurethane (meth)acrylate-silane and their use in composite films and electronic devices are described.

公开(公告)号：US09790396B2

公开(公告)日：2017-10-17

申请号：US14416303

申请日：2013-03-01

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Thomas P. Klun ,  Alan K. Nachtigal ,  Joseph C. Spagnola ,  Mark A. Roehrig ,  Jennifer K. Schnobrich ,  Guy D. Joly ,  Christopher S. Lyons

IPC: C09D143/04 ,  C07F7/18 ,  H01L51/00 ,  H01L51/52 ,  H01L51/44 ,  H01L51/10 ,  B05D3/06 ,  B32B27/30 ,  C08J7/04 ,  C09D133/14 ,  B05D1/00 ,  B05D3/10 ,  C08K3/34 ,  C09D135/02 ,  C23C14/08 ,  C23C14/34 ,  C23C16/40 ,  C23C16/44 ,  C08F130/08 ,  C09J133/14

CPC classification number: C09D143/04 ,  B05D1/60 ,  B05D3/067 ,  B05D3/068 ,  B05D3/101 ,  B32B27/308 ,  B32B2250/04 ,  B32B2307/7242 ,  B32B2307/7244 ,  C07F7/1804 ,  C08F130/08 ,  C08J7/045 ,  C08J2333/12 ,  C08K3/34 ,  C09D133/14 ,  C09D135/02 ,  C09J133/14 ,  C23C14/08 ,  C23C14/34 ,  C23C16/40 ,  C23C16/44 ,  H01L51/004 ,  H01L51/107 ,  H01L51/448 ,  H01L51/5253 ,  Y10T428/1064 ,  Y10T428/31507 ,  Y10T428/31551 ,  Y10T428/31609 ,  Y10T428/31663

Abstract: Urethane (multi)-(meth)acrylate (multi)-silane compositions, and articles including a (co)polymer reaction product of at least one urethane (multi)-(meth)acrylate (multi)-silane precursor compound. The disclosure also articles including a substrate, a base (co)polymer layer on a major surface of the substrate, an oxide layer on the base (co)polymer layer; and a protective (co)polymer layer on the oxide layer, the protective (co)polymer layer including the reaction product of at least one urethane (multi) (meth)acrylate (multi)-silane precursor compound. The substrate may be a (co)polymeric film or an electronic device such as an organic light emitting device, electrophoretic light emitting device, liquid crystal display, thin film transistor, or combination thereof. Methods of making urethane (multi)-(meth)acrylate (multi)-silane precursor compounds and their use in composite multilayer barrier films are also described. Methods of using such barrier films in articles selected from a solid state lighting device, a display device, and combinations thereof, are also described.

公开(公告)号：US20170283444A1

公开(公告)日：2017-10-05

申请号：US15528615

申请日：2015-12-14

Applicant: 3M INNOVATIVE PROPERTIES COMPANY

Inventor： Thomas P. Klun ,  Mark A. Roehrig ,  Joseph C. Spagnola ,  Alan K. Nachtigal ,  Charles J. Hoy ,  Richard J. Pokorny ,  William J. Hunt ,  Jason T. Petrin ,  Paul B. Armstrong ,  Suresh S. Iyer

IPC: C07F7/18 ,  C09C3/12 ,  C09D7/12 ,  C08F222/22

CPC classification number: C07F7/1804 ,  C08F222/22 ,  C08K3/36 ,  C08K5/3435 ,  C08K9/06 ,  C09C3/12 ,  C09D7/62

Abstract: Compounds having hindered amine and oxyalkyl amine light stabilizers can mitigate the adverse effects of actinic radiation, such as visible and ultraviolet light, in particular on substrates such as glass or ceramic substrates. Polymers derived from such compounds. Nanoparticles, substrates, such as glass or ceramic substrates, or both nanoparticles and substrates, having such compounds affixed thereto. Articles containing at least one of such polymers, nanoparticles, substrates, or compounds.