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    FACILITY AND METHOD FOR THE PRODUCTION OF ANHYDROUS FORMIC ACID
    1.
    发明申请
    FACILITY AND METHOD FOR THE PRODUCTION OF ANHYDROUS FORMIC ACID 审中-公开
    SYSTEM AND METHOD FOR WATER FREE FORMIC生产

    公开(公告)号：WO0155077A3

    公开(公告)日：2002-02-07

    申请号：PCT/EP0100748

    申请日：2001-01-24

    Applicant: BASF AG ,  AUER HEINZ ,  BESSLING BERND ,  HAMMER HANS ,  HASSE HANS ,  SAUER FRIEDRICH ,  VICARI MAXIMILIAN ,  WAGNER GERHARD ,  ADRIAN TILL

    Inventor： AUER HEINZ ,  BESSLING BERND ,  HAMMER HANS ,  HASSE HANS ,  SAUER FRIEDRICH ,  VICARI MAXIMILIAN ,  WAGNER GERHARD ,  ADRIAN TILL

    IPC: C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/00 ,  C22C38/42 ,  C22C38/44 ,  C07C53/02 ,  C22C19/05

    CPC classification number: C22C38/44 ,  C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/001 ,  C22C38/42 ,  C07C53/02

    Abstract: The invention concerns a device and a method for obtaining anhydrous or substantially anhydrous formic acid. Said device is partly or totally made of a zirconium-free material. A liquid of general formula (I) is used as extracting agent, wherein radicals R and R represent alkyl, cycloalkyl, aryl or aralkyl groups or R and R form together with the N atom a heterocyclic five or six-membered ring and in which only one of the radicals is an aryl group and in which R stands for hydrogen or a C1-C4-alkyl group. The device comprises the following equipment: (i) a synthesis reactor (6); (ii) a hydrolysis reactor (1); (iii) a first distillation device (2); (iv) a second distillation device (4); (v) an extraction device (3) and (vi) a third distillation device (5). The material has been selected from the group consisting of the following classes of materials: titanium-palladium alloys, nickel-based materials containing chrome, molybdenum, and/or wolfram and high-alloy, austenitic special chrome-nickel steels containing molybdenum.

    Abstract translation: 本发明涉及一种装置和用于获得无水或基本上无水的甲酸的方法。 该装置部分地或完全地由zirkoniumarmen材料构成。 作为提取手段是通式（I）的液体被使用，其中基团R <1>和R <2>表示或烷基，环烷基，芳基或芳烷基的基团R <1>和R <2>连同 的N原子形成杂环5或6元环，且其中仅一个基团是芳基和<3>，其中R是氢或C1-C4烷基。 该装置包括下列装置（I）的合成反应器（6），（II）的水解反应器（1），（iii）第一蒸馏装置（2），（iv）第二蒸馏装置（4），（v）的提取装置 （3）和（vi）第三蒸馏装置（5）。 所述材料是选自以下组的材料类钛 - 钯合金，铬，钼和/或含钨的镍基材料和含钼高合金化的奥氏体铬 - 镍特种钢。

    4.
    发明专利
    未知

    公开(公告)号：NO327850B1

    公开(公告)日：2009-10-05

    申请号：NO20023515

    申请日：2002-07-23

    Applicant: BASF AG

    Inventor： AUER HEINZ ,  HAMMER HANS ,  BESSLING BERND ,  HASSE HANS ,  SAUER FRIEDRICH ,  WAGNER GERHARD ,  ADRIAN TILL ,  VICARI MAXIMILIAN

    IPC: C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/00 ,  C22C38/42 ,  C22C38/44

    Abstract: The invention relates to an apparatus and a process for the preparation of anhydrous or substantially anhydrous formic acid. This apparatus is constructed partly or entirely of substantially zirconium-free materials. The extractant employed is a liquid of the general formula I where the radicals R 1 and R 2 are alkyl, cycloalkyl, aryl or aralkyl groups, or R 1 and R 2 jointly, together with the N atom, form a heterocyclic 5- or 6-membered ring, and only one of the radicals is an aryl group, and where R 3 is hydrogen or a C 1 -C 4 -alkyl group. The apparatus has a synthesis reactor ( 6 ), a hydrolysis reactor ( 1 ), three distillation devices ( 2,4,5 ) and an extraction device ( 3 ).

    طريقة لانتاج احادي ايثليين جليكول MONOETHYLENE GLYCOL عالي النقاء
    7.
    发明专利
    طريقة لانتاج احادي ايثليين جليكول MONOETHYLENE GLYCOL عالي النقاء 未知

    公开(公告)号：SA1059B1

    公开(公告)日：2006-07-31

    申请号：SA99200782

    申请日：1999-11-30

    Applicant: BASF AG

    Inventor： ADRIAN TILL ,  BEBLING BERND ,  HASSE HANS ,  VANSANT FRANS ,  THEIS GERHARD

    IPC: C07C29/10 ,  C07C29/76 ,  C07C29/80 ,  C07C31/20

    Abstract: الملخص: عمليةللإستخلاصالتقطيريلاحاديايثيلينجيكول monoethylene glycol منناتجالتحللالمائيلاكسيدالايثيلين ethylene oxide بواسطةنزعالماءبالضغطو نزعالماءتحتالتفريغو تقطيرالتنقيةالتالي،و تشتملعلىاعمدةلنزعالماءبالضغطاوعلىالاقليكونعمودنزعالماءتحتالضغطالاولمنالمجموهةالمتواحدة (٢و٣و٤) بهمنطقةنزعذاتمرحلةفلصلواحدةعلىالاقل، ويفضلانيكونبها٢ الى 10 مراحلفصل، وبصفةخاصةيفضلذات٣ الى٦ مراحلفصل، وتمازالةجزءمنالتيارالعليمنعمود (اعمدة) نزعالماءبالضغط (٣و ٤و ٥) الذيبهمنطقةنزع،منالنظام.،

    8.
    发明专利
    未知

    公开(公告)号：BR0307813A

    公开(公告)日：2004-12-21

    申请号：BR0307813

    申请日：2003-02-28

    Applicant: BASF AG

    Inventor： PESCHEL WERNER ,  ADRIAN TILL ,  RUST HARALD ,  TTCHER ARND B ,  HILLMER THOMAS ,  LLER ULRICH M ,  PAPP RAINER

    IPC: C07C5/11 ,  C07B61/00 ,  C07C29/04 ,  C07C35/08 ,  C07C13/20

    Abstract: A process for preparing cyclohexanol from benzene by: a) preparing cyclohexene by hydrogenating benzene in the presence of a catalyst, and b) preparing cyclohexanol by hydrating the cyclohexene in the presence of a catalyst, comprises: carrying out steps a) and b) in a reaction facility which has a bottom region at the lower end, a top region at the upper end, and a reaction zone between the top region and the bottom region which contains the catalyst according to steps a) and b), evaporating a portion of the benzene using the heat of reaction in the reaction zone, condensing it in the top region and returning it to the reaction zone, and withdrawing a reaction mixture containing cyclohexanol in the bottom region.

    CONTINUOUS METHOD FOR SEPARATING A CLESS THANSBGREATER THAN4LESS THAN/SBGREATER THAN CUT
    9.
    发明专利
    CONTINUOUS METHOD FOR SEPARATING A CLESS THANSBGREATER THAN4LESS THAN/SBGREATER THAN CUT 未知

    公开(公告)号：AU2003250133A1

    公开(公告)日：2004-02-16

    申请号：AU2003250133

    申请日：2003-07-22

    Applicant: BASF AG

    Inventor： HEIDA BERND ,  ADRIAN TILL ,  HILL THOMAS ,  KINDLER KLAUS

    IPC: B01D3/40 ,  C07C5/22 ,  C07C7/08

    Abstract: In a continuous process for fractionating a C4 fraction (C4) by extractive distillation using a selective solvent (LM) in an extractive distillation column (EDK), it is proposed that a dividing wall (TW) is installed in the longitudinal direction in the extractive distillation column (EDK) to form a first region (A), a second region (B) and a lower combined column region (C) and a top stream (C4H10) comprising the butanes is taken off from the first region (A), a top stream (C4H8) comprising the butenes is taken off from the second region (B) and a stream (C4H6) comprising the hydrocarbons from the C4 fraction which are more soluble in the selective solvent (LM) than are the butanes and the butenes is taken off from the lower combined column region (C).

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