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    Rylene dyes
    1.
    发明专利
    Rylene dyes 未知

    公开(公告)号：AU2003250173A8

    公开(公告)日：2004-04-08

    申请号：AU2003250173

    申请日：2003-07-25

    Applicant: BASF AG ,  MAX PLANCK GESELLSCHAFT

    Inventor： KOHL CHRISTOPHER ,  KRIEGER MATTHIAS ,  BOHM ARNO ,  SIGGEL LORENZ ,  BECKER STEFAN ,  MULLEN KLAUS

    IPC: G03G5/06 ,  C07D487/06 ,  C07D487/22 ,  C09B5/24 ,  C09B5/62 ,  C09C3/08 ,  C09D7/12 ,  C09D11/00 ,  C09B57/08

    Abstract: New mono- and bis-rylenedicarbimidyl-anthraquinone dyes (I) are claimed. New mono- and bis-rylenedicarbimidyl-anthraquinone dyes are of formula (I). R = H or (substituted) 1-30 C alkyl, 5-8 C cycloalkyl or (het)aryl; R' = Br, CN, -NR32 or (substituted) (het)aryloxy, (het)arylthio or 3-18 C alk-1-ynyl; R3 = H, 1-18 C alkyl or (substituted) (het)aryl; or NR32 = a 5-7-membered heterocyclic group; X, Y = H or together a 6-membered ring attached to a rylene ring system (Ia), in which X corresponds to the -NH- group and Y to the other free bond; n = 2, 3, 4 or may also be 1 if X and Y are a (Ia) group; and m = 0-6. The full definitions are given in the DEFINITIONS (Full Definitions) Field. Independent claims are also included for methods of preparing asymmetric (I; where X, Y = H) and symmetric and asymmetric (I, where X, Y = a 6-membered ring attached to arylene ring system).

    1,6,9,14-TETRASUBSTITUTED TERRYLENE TETRACARBOXYLIC ACID DIIMIDES
    5.
    发明专利
    1,6,9,14-TETRASUBSTITUTED TERRYLENE TETRACARBOXYLIC ACID DIIMIDES 未知

    公开(公告)号：AU2003238211A1

    公开(公告)日：2003-12-22

    申请号：AU2003238211

    申请日：2003-06-04

    Applicant: BASF AG

    Inventor： REUTHER ERIK ,  MULLEN KLAUS ,  BOHM ARNO ,  KRIEGER MATTHIAS

    IPC: C07D471/06 ,  C09B5/62 ,  C09K11/06

    Abstract: New 1,6,9,14-tetra-substituted terrylenetetracarbodiimides (I) are claimed, in which the 1,6-positions and 9,14-positions independently are substituted by bromo, cyano, (het)aryloxy, (het)arylthio, optionally substituted (hetero)-alk(en)yl or -alkynyl, N-heterocyclyleth(en)yl, N-heterocyclylethynyl or (substituted) amino. 1,6,9,14-Tetra-substituted terrylenetetracarbodiimides of formula (I) are new X, Y = Br, CN, (het)aryloxy or (het)arylthio (optionally mono- or poly-substituted by 1-12C alkyl, 1-12C alkoxy, -COOR1, -SO3R1, halogen, COOH, carboxy, CN, -CONHR2 and/or -NHCOR2), -L-R3, -N(R2)2; R, R' = H, 1-30C alkyl (optionally with -O-, -S-, -NR1-, -CO- and/or -SO2- group(s) in the chain and optionally mono- or poly-substituted by CN, 1-6 C alkoxy, aryl (optionally substituted by 1-18 C alkyl or 1-6 C alkoxy) and/or a 5-7-N-heterocyclic group, which may contain other hetero-atoms and may be aromatic), 5-8 C cycloalkyl (optionally with -O-, -S- and/or -NR1- group(s) in the C skeleton and/or mono- or poly-substituted by 1-6 C alkyl), (het)aryl (optionally mono- or poly-substituted by 1-18 C alkyl, 1-6 C alkoxy, CN, -CONHR2, -NHCOR2 and/or (het)arylazo, which may be substituted by 1-10 C alkyl, 1-6 C alkoxy or CN); L = 1,2-ethylene, 1,2-ethenylene or 1,2-ethynylene; R1 = H or 1-6C alkyl; R2 = H, 1-18C alkyl or (het)aryl, optionally substituted by 1-6 C alkyl, 1-6 C alkoxy, halogen, OH, carboxy or CN); R3 = 1-18C alkyl (optionally with -O-, -S-, -NR1-, -CO- and/or -SO2- group(s) in the chain and optionally substituted by -COOR1, -SO3R1, OH, CN, 1-6C alkoxy, aryl (optionally substituted by 1-18 C alkyl or 1-6 C alkoxy) and/or a 5-7-N-heterocyclic group, which may contain other hetero-atoms and may be aromatic). Independent claims are also included for methods of preparing (I).

    RYLENE DYES
    6.
    发明专利
    RYLENE DYES 未知

    公开(公告)号：AU2003250173A1

    公开(公告)日：2004-04-08

    申请号：AU2003250173

    申请日：2003-07-25

    Applicant: BASF AG

    Inventor： BOHM ARNO ,  SIGGEL LORENZ ,  BECKER STEFAN ,  MULLEN KLAUS ,  KOHL CHRISTOPHER ,  KRIEGER MATTHIAS

    IPC: G03G5/06 ,  C07D487/06 ,  C07D487/22 ,  C09B5/24 ,  C09B5/62 ,  C09C3/08 ,  C09D7/12 ,  C09D11/00 ,  C09B57/08

    Abstract: New mono- and bis-rylenedicarbimidyl-anthraquinone dyes (I) are claimed. New mono- and bis-rylenedicarbimidyl-anthraquinone dyes are of formula (I). R = H or (substituted) 1-30 C alkyl, 5-8 C cycloalkyl or (het)aryl; R' = Br, CN, -NR32 or (substituted) (het)aryloxy, (het)arylthio or 3-18 C alk-1-ynyl; R3 = H, 1-18 C alkyl or (substituted) (het)aryl; or NR32 = a 5-7-membered heterocyclic group; X, Y = H or together a 6-membered ring attached to a rylene ring system (Ia), in which X corresponds to the -NH- group and Y to the other free bond; n = 2, 3, 4 or may also be 1 if X and Y are a (Ia) group; and m = 0-6. The full definitions are given in the DEFINITIONS (Full Definitions) Field. Independent claims are also included for methods of preparing asymmetric (I; where X, Y = H) and symmetric and asymmetric (I, where X, Y = a 6-membered ring attached to arylene ring system).

    METHOD FOR CONVERTING PERYLEN-3,4:9,10-TETRACARBOXYLIC ACID DIIMIDES INTO A FORM SUITABLE FOR USE AS A FLUORESCENT DYE
    7.
    发明专利
    METHOD FOR CONVERTING PERYLEN-3,4:9,10-TETRACARBOXYLIC ACID DIIMIDES INTO A FORM SUITABLE FOR USE AS A FLUORESCENT DYE 未知

    公开(公告)号：AU2003236705A1

    公开(公告)日：2003-12-31

    申请号：AU2003236705

    申请日：2003-06-06

    Applicant: BASF AG

    Inventor： ERK PETER ,  SCHAFER SIMONE ,  BOHM ARNO ,  BLASCHKA PETER ,  ARMS HARALD ,  HELFER WILLI

    IPC: C09B67/10 ,  C09B67/48 ,  C09B5/62

    Abstract: A process for converting perylene-3,4:9,10-tetracarboximides of the general formula I in which R1 and R2 are each unbranched, branched or cyclic C1-C8-alkyl to a form suitable for use as fluorescent dyes, which comprises a) dissolving or suspending the perylene-3,4:9,10-tetracarboximides whose molecules have a molecular volume of ≦̸230 Å3 in an organic or inorganic solvent at from 0 to 250° C., b1) cooling the solution obtained in step a) to or below the crystallization temperature and, in the case of an organic solvent, if desired at the same time removing excess solvent until the first crystals form, or, in the case of an inorganic solvent, adding water or dilute aqueous solutions of the solvent until the first crystals form, and maintaining the solution at this temperature for further crystallization or b2) cooling the suspension obtained in step a) to or below the crystallization temperature when the temperature in step a) was above the crystallization temperature, and maintaining the suspension at this temperature for further crystallization, c) isolating the solvate crystals formed in step b) and d) then removing the solvent from the solvate crystals, and also novel crystalline forms of perylene-3,4:9,10-tetracarboxylic diimides.

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