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    New substituted bis(tetrakis(hydroxymethyl)phosphonium) salts are useful for the production of flame retardant polyurethane foams
    2.
    发明专利
    New substituted bis(tetrakis(hydroxymethyl)phosphonium) salts are useful for the production of flame retardant polyurethane foams 未知

    公开(公告)号：DE10304344A1

    公开(公告)日：2004-08-12

    申请号：DE10304344

    申请日：2003-02-03

    Applicant: BASF AG

    Inventor： BLEUEL ELKE ,  LEHMANN PIT ,  ROTERMUND UDO ,  SEITZ CHRISTIAN ,  BOEHME PETER

    IPC: C08G18/40 ,  C08G18/50 ,  C08G18/54 ,  C08K5/50 ,  C08G18/48 ,  C08G18/46

    Abstract: Substituted bis[tetrakis(hydroxymethyl)phosphonium] salts are new. Substituted bis[tetrakis(hydroxymethyl)phosphonium] salts (I) of formula (1) are new. [Image] A : -CH2 or CH2-CH-E; E : 1-8(1-4)C alkylene; R : an organic group which in polyurethane comprises the corresponding isocyanate or its reaction products or in a prepolymer is the group of the added isocyanate; w, x, y, z : 1-20. Independent claims are included for: (1) a process for the production of salts (I) by reaction of tetrakis(hydroxymethyl)phosphonium salts of formula (10) with alkylene oxides; (2) polyurethanes, preferably rigid polyurethane foams having at least one structure of formula (2) - (9) in its matrix; (3) an isocyanate or hydroxyl group containing prepolymer containing at least one structure of formula (2) - (9) and; (4) a process for the production of flame retardant polyurethanes by reaction of polyisocyanates with isocyanate-reactive compounds having at least 2 reactive hydrogen atoms in the presence of a compound of formula (1) or (10). [Image] [Image] D : -CH2 or -CH2-CH-E; B : anion; a : whole number ensuring electroneutrality.

    Agent for surface modification of fillers for polyamide composition comprises selected functionalized silane compounds
    5.
    发明专利
    Agent for surface modification of fillers for polyamide composition comprises selected functionalized silane compounds 未知

    公开(公告)号：DE19961973A1

    公开(公告)日：2001-06-28

    申请号：DE19961973

    申请日：1999-12-22

    Applicant: BASF AG

    Inventor： GASSAN MICHAEL ,  GUETTES BERND ,  SANDER MICHAEL ,  KRAUS RUPERT ,  PLAUMANN HEINZ ,  ROTERMUND UDO ,  BIEDERMANN ANJA ,  SEITZ CHRISTIAN ,  REICHELT MICHAEL ,  HEMPEL RENATE

    IPC: C08G12/40 ,  C08G18/76

    Abstract: An agent for the surface modification of fillers for polyamide compositions comprises: (A) an amino-functional silane, a bis-aminosilane a tertiary aminosilane or an oligomer of these; (B) a mixture of an amino-functional silane, bis-aminosilane and/or tertiary aminosilane and an alkyl-, alkenyl- or polyether-functional silane and optionally an oligomer of these; or (C) a mixture of an alkyl-functional silane and an alkenyl-functional silane and optionally an oligomer of these. An agent for the surface modification of fillers for polyamide compositions comprises either: (A) an agent comprising: (i) an amino-functional silane of formula (Ia); (ii) a bis-aminosilane (Ib); (iii) a tertiary aminosilane (Ic); or an oligomer of (Ia)-(Ic) with a degree of oligomerization (DO) of 2-20; (B) a mixture of: (i) a component comprising (a) an amino-functional silane of formula (IIa), (b) a secondary aminosilane (IIb) and/or (c) a tertiary aminosilane (IIc); and (ii) a component comprising either (a) an alkyl-functional silane of formula (III), (b) an alkenyl-functional silane of formula (IV), (c) a polyether-functional silane of formula (V); and optionally (iii) an oligomer of (IIa)-(IIc) and (III)-(V) with a DO of 2-20; or (C) a mixture of: (i) an alkyl-functional silane of formula (IIIa); and (ii) an alkyl-functional silane of formula (IV); and optionally (iii) an oligomer of (IIIa) and (IV) with a DO of 2-20. RNH-(CH2)3-Si(Me)x(Z)3-x (Ia) Z = 1-3C alkoxy, OH or Cl; x = 0 or 1; and R = 1-20C alkyl, 5-12C cycloalkyl or 6-12C aryl. R-Si(Me)x(Z)3-x (IIa) Z = 1-3C alkoxy, OH or Cl; x = 0 or 1; R = H2N((CH2)2NH)y(CH2)3; and y = 0-2. R'-Si(Me)x(Z)3-x (IIIa) Z = 1-3C alkoxy, OH or Cl; x = 0-1; and R' = optionally fluorinated 1-16C alkyl or cycloalkyl. CH2=CH(CH2)n-Si(Me)x(Z)3-x (IV) Z = 1-3C alkoxy, OH or Cl; x = 0 or 1; and n = 0-20. R(OCH2CHR')nO(CH2)mSi (Me)x(Z)3-x (V) z = 1-3C alkoxy, OH or Cl; x = 0 or ; R = 1-4C alkyl; R' = H or Me; n = 5-20; and m = 2 or 3. Independent claims are also included for the following: (1) a filler surface-modified with the above agent; (2) an article comprising the surface-modified filler; (3) a filled polyamide composition produced using the surface-modified filler; and (4) an article based on the filled polyamide composition.

    Production of rigid polyurethane foam with isocyanurate groups, used for insulation, involves reacting polyisocyanate with a special polyol mixture using PIR catalyst and a specific index
    8.
    发明专利
    Production of rigid polyurethane foam with isocyanurate groups, used for insulation, involves reacting polyisocyanate with a special polyol mixture using PIR catalyst and a specific index 未知

    公开(公告)号：DE10145458A1

    公开(公告)日：2003-04-03

    申请号：DE10145458

    申请日：2001-09-14

    Applicant: BASF AG

    Inventor： FALKE PETER ,  SEITZ CHRISTIAN ,  MALOTKI PETER VON ,  ROTERMUND UDO

    IPC: C08G18/22 ,  C08G18/48 ,  C08G18/76 ,  C08G18/16 ,  C08K7/06 ,  C08K7/24 ,  C08G18/79

    Abstract: Rigid polyurethane foam is produced from mixtures of (b1) polyfunctional polyether-ols with OH numbers of 40-800 (including at least one with OH no. above 150) and more than 30 wt% ethylene oxide based on total alkylene oxide and (b2) polyether-ols with OH nos. above 40 based mainly on propylene- and/or butylene oxide, using PIR catalysts and an index of 80-500. A method for the production of rigid polyurethane foam with urethane and mainly isocyanurate groups by reacting (a) optionally modified polyisocyanates with (b) a polyol mixture and optionally (c) other compounds with isocyanate-reactive hydrogen atoms, in presence of (d) water, (e) catalysts, (f) fire retardants, (g) blowing agents and optionally (f) other additives etc. The polyol mixture (b) comprises (b1) di- to octa-functional polyether-ol(s) based on ethylene oxide (EO) and optionally propylene oxide (PO) and/or butylene oxide (BO), with an EO content of more than 30 wt% based on total alkylene oxide and an OH number of 40-800 mg KOH/g (including at least one polyether-ol (b1.1) with an OH number of more than 150), and (b2) polyether-ol(s) with an OH number of more than 40, based on PO and/or BO and optionally EO, and the foam is produced with a characteristic index of 80-500 in presence of PIR catalysts.. An Independent claim is also included for rigid polyurethane foam as above obtained by this method.

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