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    New halomethylbenzoyl cyanide
    1.
    发明专利
    New halomethylbenzoyl cyanide 有权
    新的甲基苯甲酰氯

    公开(公告)号：JP2006188531A

    公开(公告)日：2006-07-20

    申请号：JP2006052375

    申请日：2006-02-28

    Applicant: Basf Ag ,  ビーエーエスエフ アクチェンゲゼルシャフトBASF Aktiengesellschaft

    Inventor： ISAK HEINZ ,  WETTLING THOMAS ,  KEIL MICHAEL ,  WOLF BERND ,  DOETZER REINHARD

    IPC: C07C255/40 ,  C07C253/14 ,  C07C255/32

    CPC classification number: C07C255/40 ,  C07C253/14

    Abstract: PROBLEM TO BE SOLVED: To provide a new halomethylbenzoyl cyanide industrially useful as an important intermediate product for the synthesis of a plant protection agent. SOLUTION: The halomethylbenzoyl cyanide expressed by formula I' is produced by the reaction of a halomethylbenzoyl chloride with an alkali metal cyanide or a transition metal cyanide. In the formula, X is a halogen atom, a 1-4C alkyl, a 1-4C alkoxy, trifluoromethyl, -C(1-5C alkyl)=N-O-(1-5C alkyl) or -C(1-5C alkyl)=N-O-(2-5C alkenyl); m is 0-4; and Y is chloromethyl or bromomethyl. COPYRIGHT: (C)2006,JPO&NCIPI

    Abstract translation: 要解决的问题：提供工业上可用作合成植物保护剂的重要中间产物的新的卤代甲基苯甲酰氰。 解决方案：由式I'表示的卤代甲基苯甲酰氰由卤代甲基苯甲酰氯与碱金属氰化物或过渡金属氰化物的反应产生。 在该式中，X是卤素原子，1-4C烷基，1-4C烷氧基，三氟甲基，-C（1-5C烷基）= NO-（1-5C烷基）或-C（1-5C烷基） = NO-（2-5C烯基）; m为0-4; Y是氯甲基或溴甲基。 版权所有（C）2006，JPO＆NCIPI

    REDUCTION OF THE CONTENT OF COMPOUNDS CONTAINING OXYGEN AND/OR NITROGEN IN MATERIAL FLOWS CONTAINING ISOBUTENE
    3.
    发明申请
    REDUCTION OF THE CONTENT OF COMPOUNDS CONTAINING OXYGEN AND/OR NITROGEN IN MATERIAL FLOWS CONTAINING ISOBUTENE 审中-公开
    还原氧含AND / OR氮肥连接。在异丁烯物资流通水平

    公开(公告)号：WO2004101477A2

    公开(公告)日：2004-11-25

    申请号：PCT/EP2004005200

    申请日：2004-05-14

    Applicant: BASF AG ,  WETTLING THOMAS ,  BORCHERS DIRK

    Inventor： WETTLING THOMAS ,  BORCHERS DIRK

    IPC: C07C7/13 ,  C07C7/00

    CPC classification number: C07C7/13 ,  C07C11/09

    Abstract: The invention relates to a method for reducing the content of compounds containing oxygen and/or nitrogen in material flows having an isobutene content of at least 10 wt. %. According to said method, the material flow is guided over a fixed bed of an acid-free zeolite having a mean pore size of between 0.3 and 1.5 nm, in a liquid phase, at a temperature T [in K] and at a linear speed v [in cm/min], the fixed bed having a dimension I [in cm] in the flow direction of the material flow, and T, v and I obeying the equation 2 l/v = 500 min. The inventive method prevents the formation of isobutene oligomers.

    Abstract translation: 公开了一种用于减少的含量的含氧和/或具有至少10重量％的异丁烯含量的流化合物，含氮其中所述线性在温度T在液相中的材料流[在K]并用的方法 速度v [在厘米/分钟]经过具有0.3的平均孔径的无酸沸石的固定床至1.5nm，其中在所述材料流动的延伸件1包括[以cm]和T，v和I的流动方向上的固定床 方程2 <（T-283 K）/ 10 K.> L / v <= 500分钟233。 的处理过程避免了异丁烯的形成。

    4.
    发明专利
    未知

    公开(公告)号：DE102005049236A1

    公开(公告)日：2007-04-19

    申请号：DE102005049236

    申请日：2005-10-14

    Applicant: BASF AG

    Inventor： RATH HANS PETER ,  MACH HELMUT ,  WETTLING THOMAS

    IPC: C08F2/06 ,  C08F4/14 ,  C08F10/10

    Abstract: The invention relates to a process for preparing polyisobutene having a mean molecular weight Mn of from 400 to 50 000, in particular from 500 to 10 000, by polymerizing isobutene in the presence of a BF3-containing complex catalyst, wherein the polymerization is carried out at least temporarily in the presence of one or more cyclic ethers.

    6.
    发明专利
    未知

    公开(公告)号：AT300560T

    公开(公告)日：2005-08-15

    申请号：AT01996562

    申请日：2001-11-16

    Applicant: BASF AG

    Inventor： WETTLING THOMAS ,  BORCHERS DIRK ,  VERRELST WIM ,  RATH HANS PETER

    IPC: B01J27/12 ,  B01J27/32 ,  B01J38/00 ,  B01J38/52 ,  C08F4/14 ,  C08F6/00 ,  C08F6/02 ,  C08F6/08 ,  C08F10/00

    Abstract: The invention relates to a method for deactivating and recovering boron trifluoride when producing polyisobutenes by means of cationic polymerization of isobutene or hydrocarbon streams containing isobutene in the liquid phase in the presence of boron trifluoride or in the form of a boron trifluoride catalyst complex. The catalyst complex is separated, essentially in the liquid phase, from the reactor discharge. The method comprises the following steps: a) removing from the polymerization reactor at -60 to 020 C., methanol, ethanol or a mixture of methanol and ethanol in such a quantity that an alcohol phase rich in boron trifluoride is formed; b) separating the alcohol phase according to (a) and, (c) optionally recycling the boron trifluoride of the alcohol phase obtained from (b) to the method in a suitable manner.

    Method for deactivating and recovering boron trifluoride when producing polyisobutenes
    8.
    发明专利
    Method for deactivating and recovering boron trifluoride when producing polyisobutenes 未知

    公开(公告)号：AU2185602A

    公开(公告)日：2002-05-27

    申请号：AU2185602

    申请日：2001-11-16

    Applicant: BASF AG

    Inventor： WETTLING THOMAS ,  BORCHERS DIRK ,  VERRELST WIM ,  RATH HANS PETER

    IPC: B01J27/12 ,  B01J27/32 ,  B01J38/00 ,  B01J38/52 ,  C08F4/14 ,  C08F6/00 ,  C08F6/02 ,  C08F6/08 ,  C08F10/00

    Abstract: The invention relates to a method for deactivating and recovering boron trifluoride when producing polyisobutenes by means of cationic polymerization of isobutene or hydrocarbon streams containing isobutene in the liquid phase in the presence of boron trifluoride or in the form of a boron trifluoride catalyst complex. The catalyst complex is separated, essentially in the liquid phase, from the reactor discharge. The method comprises the following steps: a) removing from the polymerization reactor at -60 to 020 C., methanol, ethanol or a mixture of methanol and ethanol in such a quantity that an alcohol phase rich in boron trifluoride is formed; b) separating the alcohol phase according to (a) and, (c) optionally recycling the boron trifluoride of the alcohol phase obtained from (b) to the method in a suitable manner.

    Method for producing polyisobutylenes
    9.
    发明专利
    Method for producing polyisobutylenes 未知

    公开(公告)号：AU8761201A

    公开(公告)日：2002-01-30

    申请号：AU8761201

    申请日：2001-07-13

    Applicant: BASF AG

    Inventor： WETTLING THOMAS ,  BORCHERS DIRK ,  VERRELST WIM ,  RATH HANS PETER

    IPC: C08F2/38 ,  C08F4/14 ,  C08F6/02 ,  C08F10/10

    Abstract: The production of polyisobutene by liquid-phase, cationic polymerization of isobutene in the presence of a boron trifluoride catalyst followed by the addition of a solid deactivator at a required point in time uses a deactivator (I) containing boron trifluoride-binding prim., sec., tert. and/or quat. nitrogen atoms, which is insoluble in the reaction mixture. In the production of polyisobutenes (PIB) by liquid-phase, cationic polymerization of isobutene or hydrocarbon streams containing isobutene in the presence of boron trifluoride as catalyst, the catalytic activity of the BF3 is partly or completely eliminated at a required point in time by means of a solid deactivator which contains BF3-binding prim., sec., tert. and/or quat. nitrogen atoms and is insoluble in the reaction mixture.

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