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公开(公告)号：KR101877778B1
公开(公告)日：2018-07-12
申请号：KR1020170179778
申请日：2017-12-26
Applicant: 한국화학연구원
IPC: C07D275/06 , A23L27/30
CPC classification number: C07D275/06 , A23L27/30 , A23V2002/00 , A23V2250/26
Abstract: 본원발명은톨루엔술폰아미드의개선된산화공정을이용한사카린의제조방법에대한것으로보다구체적으로는산화크롬(CrO)과과요오드산(HIO)을이용한 o-톨루엔술폰아미드의효율적인산화반응을통하여경제적이고효율적으로사카린을제조하는방법에대한것이다. 본원발명에따르면사카린의제조시 o-톨루엔술폰아미드산화공정에서고비용의단점이있는종래의방법을개선하여보다경제적이며높은수율로사카린을제조할수 있는장점이있다.
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公开(公告)号：KR101446018B1
公开(公告)日：2014-10-06
申请号：KR1020130113057
申请日：2013-09-24
Applicant: 한국화학연구원
CPC classification number: Y02E50/13 , C10L1/2222 , C10L1/08 , C10L1/18 , C10L2230/081
Abstract: The present invention relates to an antioxidant composition for biodiesel, and to an antioxidant composition having improved oxidation efficiency. The antioxidant composition for biodiesel includes a hydroquinone-base antioxidant, one or more base additive selected from triethylene tetra amine and triethylene pentamine. The antioxidant composition according to the present invention has an excellent effect of extremely increasing oxidation stability compared with independently using of an oxidation stabilizer.
Abstract translation: 本发明涉及用于生物柴油的抗氧化剂组合物和具有改善的氧化效率的抗氧化剂组合物。 用于生物柴油的抗氧化剂组合物包括氢醌基抗氧化剂，一种或多种选自三亚乙基四胺和三亚乙基五胺的基础添加剂。 与独立使用氧化稳定剂相比，本发明的抗氧化剂组合物具有极高的氧化稳定性的极好的效果。
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公开(公告)号：KR101367955B1
公开(公告)日：2014-02-26
申请号：KR1020110116916
申请日：2011-11-10
Applicant: 한국화학연구원 , 주식회사이맥솔루션 , 이맥바이오 주식회사
CPC classification number: Y02P20/582
Abstract: 본 발명은 바이오디젤용 하이드로퀴논계 산화방지제 화합물로 사용되는 2-tert-부틸 하이드로퀴논과 부틸 하이드록시아니솔의 제조방법에 관한 것으로 본 발명에 따른 제조방법은 반응온도와 시간을 조절하여 미반응된 하이드로퀴논과 용매를 재사용하여 부틸 하이드로퀴논과 부틸 하이드록시아니솔의 순도가 높고 간단하고 경제적이며 효율적인 방법이다.
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公开(公告)号：KR1020120114663A
公开(公告)日：2012-10-17
申请号：KR1020110032329
申请日：2011-04-07
Applicant: 한국화학연구원 , (주)인우코퍼레이션
IPC: G01N31/22 , G01N21/78 , C07C245/08 , G01N33/26
CPC classification number: C09B29/0088 , C09B29/0003 , C09B29/081 , C09B67/0083
Abstract: PURPOSE: A non-aqueous fluid marker containing N-benzyl-N-ethylaniline and a preparation method of the same are provided to improve the dissolution of the marker to non-aqueous fluid products. CONSTITUTION: A non-aqueous fluid marker contains N-benzyl-N-ethylaniline represented by chemical formula 1. In chemical formula 1, R is a C1 to C12 alkyl group, a C1 to C12 alkoxy group, a C1 to C12 hydroxyalkyl group, a C1 to C12 hydroxylalkoxyalkyl group, a C1 to C12 alkylphenyl group, a C1 to C12 alkoxyphenyl group, a nitro group, a cyan group, or a halogen atom. A preparation method of the non-aqueous fluid marker includes the following: an aniline derivative represented by chemical formula 3 is diazotized; and the diazotized aniline derivative is reacted with N-benzyl-N-ethylaniline represented by chemical formula 4.
Abstract translation: 目的：提供含有N-苄基-N-乙基苯胺的非水性流体标记物及其制备方法，以改善标记物对非水性流体产品的溶解性。 构成：非水性流体标记含有以化学式1表示的N-苄基-N-乙基苯胺。在化学式1中，R为C1〜C12烷基，C1〜C12烷氧基，C1〜C12羟烷基， C1〜C12羟烷氧基烷基，C1〜C12烷基苯基，C1〜C12烷氧基苯基，硝基，青基或卤素原子。 非水性流体标记物的制备方法包括：化学式3表示的苯胺衍生物被重氮化; 并将重氮化苯胺衍生物与由化学式4表示的N-苄基-N-乙基苯胺反应。
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Patent Agency Ranking
公开(公告)号：KR101190085B1
公开(公告)日：2012-10-12
申请号：KR1020090080590
申请日：2009-08-28
Applicant: 한국화학연구원
IPC: C07D403/10 , C07D209/08 , C08F263/08 , C08F257/00
Abstract: 본 발명은 광흡수제, 특히 근적외선 흡수 색소로 유용하게 사용할 수 있는 헵타메틴계 시아닌 화합물 및 이의 제조방법에 관한 것으로서, 더욱 상세하게는 2-클로로-3-(히드록시메틸렌)-5-(4-니트로페닐)시클로헥산카바알데히드를 중심으로, 양쪽에 인돌 유도체를 축합하여, 특정 치환기로 치환된 신규 화합물 및 이의 제조방법에 관한 것이다. 본 발명의 상기 화합물은 근적외선 흡수용 색소 및 고밀도 광기록용 매체의 성분으로 사용하기에 매우 적합하다.
근적외선, 헵타메틴계 시아닌, 인돌 유도체, 비스 포밀알데히드 유도체-
公开(公告)号：KR1020040082849A
公开(公告)日：2004-09-30
申请号：KR1020030017542
申请日：2003-03-20
IPC: C07C261/00
Abstract: PURPOSE: A spirobifluorene-based compound and a preparation method thereof are provided to improve luminous efficiency and processability due to good solubility in organic solvent. The compound is suitably applied as a blue light-emitting element with improved adhesiveness to a substrate, stability and service life. An organic light-emitting device using the novel spirobifluorene compound is also provided to improve the luminous efficiency, brightness and the purity and stability of colors. CONSTITUTION: The spirobifluorene-based compound has a structure of formula 1, wherein each R1 and R2 is a hydrogen atom, an alkoxy group having C1-20 or an alkyl group having C1-20; X is a fluorine atom, a cyano group or an amine group (-NRR, in which R is a hydrogen atom or an alkyl group having C1-20). The light-emitting device comprises a cathode, an anode and a light-emitting layer containing the spirobifluorene-based compound between the cathode and the anode.
Abstract translation: 目的：提供螺二芴类化合物及其制备方法，以提高发光效率和加工性，因为在有机溶剂中的溶解性良好。 该化合物适合作为具有改善的与基材的粘合性，稳定性和使用寿命的蓝色发光元件。 还提供了使用新型螺二芴化合物的有机发光装置，以提高发光效率，亮度和色彩的纯度和稳定性。 构成：螺二芴基化合物具有式1的结构，其中每个R 1和R 2是氢原子，具有C 1-20的烷氧基或具有C 1-20的烷基; X是氟原子，氰基或胺基（-NRR，其中R是氢原子或具有C1-20的烷基）。 发光装置包括阴极，阳极和在阴极和阳极之间含有基于螺二芴的化合物的发光层。
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公开(公告)号：KR100385299B1
公开(公告)日：2003-05-23
申请号：KR1020010002733
申请日：2001-01-17
Applicant: 한국화학연구원
IPC: C09B62/03
Abstract: PURPOSE: Provided is a water-insoluble dispersion-reactive dye having an acetoxy ethyl sulfone reactive group, which reduces pollution, dose not contain hazardous amine and metals, can be used in acidic and neutral condition, and is excellent in washing-fastness and properties. CONSTITUTION: The dispersion-reactive dye(formula 2) having the 4-aminophenyl-beta-acetoxy ethyl sulfone reactive group(formula 1) is produced by a process comprising the steps of: diazotizing the 4-aminophenyl-beta-acetoxy ethyl sulfone(formula 1); making a coupling solution by dissolving a coupler in water and concentrated hydrochloric acid; mixing the diazotized 4-aminophenyl-beta-acetoxy ethyl sulfone with the coupling solution at 0-5deg.C; adding a base to keep pH neutral condition and separating the produced dye. In the formula, R, R1, R2, and R3 are identically or differently hydrogen, alkyl, alkoxy, cyanoalkyl, amino acetyl, and amino ester.
Abstract translation: 用途：提供一种具有乙酰氧基乙基砜反应性基团的水不溶性分散体 - 活性染料，其可减少污染，不含有害胺和金属，可在酸性和中性条件下使用，并且具有优异的耐洗牢度和性能 。 构成：具有4-氨基苯基-β-乙酰氧基乙基砜反应性基团（式1）的分散体活性染料（式2）通过包括以下步骤的方法制备：将4-氨基苯基-β-乙酰氧基乙基砜（ 公式1）; 通过将偶合剂溶解在水和浓盐酸中制备偶联溶液; 在0-5℃将重氮化的4-氨基苯基-β-乙酰氧基乙基砜与偶联溶液混合; 加入碱以保持pH中性条件并分离产生的染料。 在该式中，R，R1，R2和R3相同或不同地为氢，烷基，烷氧基，氰基烷基，氨基乙酰基和氨基酯。
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公开(公告)号：KR100367142B1
公开(公告)日：2003-01-10
申请号：KR1020000061922
申请日：2000-10-20
Applicant: 한국화학연구원
IPC: C09B46/00
Abstract: PURPOSE: Provided are benzimidazolone-based yellow pigments which are excellent in solvent resistance and colorfastness to light and provides a high yield, and a method for preparing the same. CONSTITUTION: The benzimidazolone-based yellow pigments represented by formula 1 are characterized in that it is prepared by using amino benzimidazolone represented by formula 9, as a diazotized compound. In the formulas, R, R1 and R2 which are the same or different, are hydrogen, C1-C4 alkyl group, nitro(-NO2) group, C1-C2 alkoxy group, C1-C18 heterocycle, methyl ester(COOCH3) or halogen group such as chloro or bromo. The yellow pigments are prepared by the steps of (i) diazotizing amino benzimidazolone compound represented by formula 9; (ii) dissolving a coupler represented by formula 11 into a solvent; (iii) mixing two solutions obtained from the steps (i) and (ii) at 0-5 deg.C; and (iv) adding base to the solution mixed in the step(iii) to adjust pH to 6-7 with stirring. In the formula 11, R, R1 and R2 are the same as the above.
Abstract translation: 用途：本发明提供耐溶剂性和耐光性优异且提供高收率的苯并咪唑酮类黄色颜料及其制备方法。 构成：由式1表示的基于苯并咪唑酮的黄色颜料的特征在于其通过使用由式9表示的氨基苯并咪唑酮作为重氮化的化合物来制备。 在式中，相同或不同的R，R 1和R 2是氢，C 1 -C 4烷基，硝基（-NO 2），C 1 -C 2烷氧基，C 1 -C 18杂环，甲酯（COOCH 3）或卤素 如氯或溴。 所述黄色颜料通过以下步骤制备：（i）使由式9表示的氨基苯并咪唑酮化合物重氮化; （ii）将由式11表示的成色剂溶解于溶剂中; （iii）在0-5℃下将步骤（i）和（ii）中获得的两种溶液混合; 和（iv）向步骤（iii）中混合的溶液中加入碱以在搅拌下将pH调节至6-7。 在式11中，R，R1和R2与上述相同。
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公开(公告)号：KR1020020031450A
公开(公告)日：2002-05-02
申请号：KR1020000061923
申请日：2000-10-20
Applicant: 한국화학연구원
IPC: C09B46/00
Abstract: PURPOSE: Provided are pigment yellow based on quinoxaline which is ecofriendly and has excellent solvent resistance and colorfastness to light, and a method for preparing the same. CONSTITUTION: The pigment yellow based on quinoxaline represented by formula 1 is characterized in that it is prepared using aminoquinoxaline represented by formula 9, as a diazotized compound. In the formulas, R, R1 and R2 are the same or different, and hydrogen, C1-C4 alkyl group, nitro(-NO2), C1-C2 alkoxy group, C1-C18 heterocycle, methyl ester(COOCH3) or halogen group such as chloro or bromo. The pigment yellow is prepared by the steps of (i) diazotizing amino quinoxaline compound represented by formula 9; (ii) dissolving coupler represented by formula 11 into solvent; (iii) mixing two reaction solution obtained from the steps (i) and (ii) at 0-5 deg.C; and (iv) adding base to the solution mixed in the step(iii) to adjust pH to 6-7 with stirring. In the formula 11, R, R1 and R2 are the same as the above.
Abstract translation: 目的：提供基于喹喔啉的颜料黄，其是环保的并且具有优异的耐溶剂性和耐光色牢度及其制备方法。 构成：由式1表示的基于喹喔啉的颜料黄的特征在于使用由式9表示的氨基喹喔啉作为重氮化合物制备。 在式中，R 1，R 2和R 2相同或不同，氢，C 1 -C 4烷基，硝基（-NO 2），C 1 -C 2烷氧基，C 1 -C 18杂环，甲酯（COOCH 3） 作为氯或溴。 颜料黄由以下步骤制备：（i）重氮化由式9表示的氨基喹喔啉化合物; （ii）将由式11表示的成色剂溶解在溶剂中; （iii）在0-5℃下将由步骤（i）和（ii）获得的两种反应溶液混合; 和（iv）向步骤（iii）中混合的溶液中加入碱以在搅拌下将pH调节至6-7。 在式11中，R，R 1和R 2与上述相同。
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