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11.发明公开
公开(公告)号：KR1020110060591A
公开(公告)日：2011-06-08
申请号：KR1020090117213
申请日：2009-11-30
Applicant: 현대자동차주식회사 , 기아자동차주식회사 , 연세대학교 산학협력단
CPC classification number: D06M13/184 , B82Y30/00 , B82Y40/00 , C01B32/05 , C01B32/174 , C01B32/18 , C07D213/79 , C07D235/28 , C07D319/18 , D06M13/252 , D06M2101/40 , H01M4/92 , H01M4/926 , H01M8/1007 , Y02P70/56
Abstract: PURPOSE: A method for increasing the hydrophilicity of crystalline carbon and a method for manufacturing a platinum carrying catalyst using the same are provided to improve the rate, the dispersion, and the durability of the catalyst. CONSTITUTION: A pi-pi interaction is formed between a surfactant and crystalline carbon. A hydrophilicity is generated by the hydrophilic functional group of a surfactant. The surfactant is one selected from 1-pyrene carboxylic acid, 9-Anthracene carboxylic acid, Fluorene-1-carboxylic acid, 1-Pyrenebutyric acid, Naphthoic acid, 1-Pyreneacetic acid, Naphtho-2-Aminopyridine-3-carboxylic acid, 1,4-Benzodioxane-6-carboxylic acid, 2-mercaptobenzimidazole, 2-Naphthalenethiol, 1-mercaptopyrene, 6-mercaptobenzopyrene, and 1,4-benzen dithiol. The crystalline carbon is one selected from carbon nano-tube, carbon nano-fiber, carbon nano-coil, and carbon nano-cage.
Abstract translation: 目的：提供增加结晶碳的亲水性的方法和使用该方法制造铂载体催化剂的方法，以提高催化剂的速率，分散性和耐久性。 构成：在表面活性剂和结晶碳之间形成pi-pi相互作用。 亲水性由表面活性剂的亲水性官能团产生。 表面活性剂是选自1-芘羧酸，9-蒽羧酸，芴-1-羧酸，1-芘丁酸，萘甲酸，1-芘乙酸，萘酚-2-氨基吡啶-3-甲酸，1 ，4-苯并二恶烷-6-羧酸，2-巯基苯并咪唑，2-萘硫醇，1-巯基苯乙烯，6-巯基苯并芘和1,4-苯二硫醇。 结晶碳选自碳纳米管，碳纳米纤维，碳纳米线圈和碳纳米笼。
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公开(公告)号：KR101033883B1
公开(公告)日：2011-05-11
申请号：KR1020090056959
申请日：2009-06-25
Inventor： 노범욱
Abstract: 본 발명은 연료전지용 고 비율 백금 담지 촉매 제조방법에 관한 것으로서, 더욱 상세하게는 폴리올 공정을 이용하여 연료전지에 사용되는 결정성 담지체 소재인 선형탄소섬유(CNF)에 백금을 담지시킨 연료전지용 고 비율 백금 담지 촉매 제조방법에 관한 것이다.
이를 위해, 본 발명은 용매이자 환원제 역할을 하는 용매에 NaOH, 백금전구체, 카본(Carbon)을 소정의 비율로 혼합하는 단계와; NaOH, 백금전구체, 카본이 혼합된 용액을 140-180℃ 사이에서 리플럭스 해줌으로써, 에틸렌 글리콜의 산화를 통한 백금전구체의 환원이 이루어지는 단계와; 백금과 담지체간 상호인력을 유발하여 백금이 담지되도록 PH를 조절하는 단계와; 환원백금의 안정화 분위기를 약화시키면서 담지체에 대한 백금 담지 수율을 높이고자 첨가물을 첨가하는 단계와; 촉매를 회수하여 세척 및 열처리를 통하여 불필요한 유기물을 제거하는 단계로 이루어지는 연료전지용 고비율 백금 담지 촉매 제조방법을 제공한다.
연료전지, 첨가물, 디아이 워터, 백금 전구체, 촉매, 담지체, 카본-
公开(公告)号：KR1020140122863A
公开(公告)日：2014-10-21
申请号：KR1020130039835
申请日：2013-04-11
Applicant: 현대자동차주식회사 , 숭실대학교산학협력단
CPC classification number: H01M4/9075 , H01M4/925 , Y02E60/50
Abstract: The present invention relates to a titanium suboxide support for a catalyst electrode for a fuel cell and to a low-temperature synthesis method of the titanium suboxide support. More specifically, the present invention relates to titanium suboxide (Ti_xO_2x-1) nanoparticles which are useful as a support for a catalyst electrode for a fuel cell; and to a method for synthesizing the titanium suboxide (Ti_xO_2x-1) nanoparticles at a low temperature of 600-900°C by using TiO_2, a Co catalyst and hydrogen gas. The titanium suboxide nanoparticles have the advantage of having excellent corrosion resistance to acid, high thermal conductivity and electrical conductivity, and excellent durability. Therefore, the catalyst electrode manufactured by using the titanium suboxide nanoparticles as a support shows high catalytic activity and enhanced oxidation-reduction properties through a fuel cell test.
Abstract translation: 本发明涉及一种用于燃料电池用催化剂电极的低氧化钛载体以及该低硫化钛载体的低温合成方法。 更具体地说，本发明涉及可用作燃料电池用催化剂电极的载体的低氧化钛（Ti_xO_2x-1）纳米粒子， 以及通过使用TiO 2，Co催化剂和氢气，在600-900℃的低温下合成低氧化钛（Ti_xO_2x-1）纳米颗粒的方法。 低氧化钛纳米颗粒具有优异的耐酸腐蚀性，高导热性和导电性，以及优异的耐久性。 因此，通过使用低氧化钛纳米颗粒作为载体制造的催化剂电极通过燃料电池试验显示出高的催化活性和增强的氧化还原性能。
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14.发明授权
公开(公告)号：KR101774706B1
公开(公告)日：2017-09-04
申请号：KR1020160111782
申请日：2016-08-31
CPC classification number: H01M4/926 , H01M4/8652 , H01M4/8803 , H01M4/8828 , H01M4/8882 , H01M4/9083 , H01M8/1004 , H01M8/1018 , H01M2008/1095 , H01M2300/0082 , B01J32/00 , B01J35/1019 , B01J35/1023 , B01J35/1057 , C01B32/168 , C01B32/354 , C01P2006/12 , H01M4/86 , Y02E60/50
Abstract: 본발명은결정성탄소담지체를수증기분위기하에 700℃내지 1100℃의온도범위에서열처리하여상기탄소담지체의비표면적을증가시키는단계; 및상기비표면적이증가된탄소담지체에자기장을인가하여불순물을제거하는단계를포함하는것을특징으로하는촉매담지체의제조방법및 이에의해제조된연료전지용촉매를제공한다. 본발명의일 실시예에따른촉매담지체의제조방법에의하면탄소담지체의표면물성을유지하면서고비표면적및 고결정성을구현할수 있으며, 이로인해촉매의탄소부식내구성및 연료전지의성능을더욱향상시킬수 있다.
Abstract translation: 本发明包括以下步骤：热处理在范围从700至1100的温度℃℃晶体圣诞sodam蒸汽气氛下延迟以增加碳载体的表面面积; 它提供了一种生产包含通过施加磁场来延迟比表面积除去杂质的步骤的催化剂载体被增加，因此含碳所产生的燃料电池用催化剂。 根据用于催化剂载体的制造方法按照本发明的一个实施例中，同时保持所述碳载体的表面特性可以实现高的比表面积和高的结晶度，从而导致进一步提高的催化剂的燃料电池的碳腐蚀耐久性和性能 你可以。
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公开(公告)号：KR101575463B1
公开(公告)日：2015-12-07
申请号：KR1020140035185
申请日：2014-03-26
Applicant: 현대자동차주식회사
CPC classification number: H01M4/921 , C22C5/04 , H01M4/8842 , H01M4/8878 , H01M4/926 , H01M2250/20 , Y02E60/50 , Y02T90/32
Abstract: 본발명은연료전지용합금촉매의제조방법에관한것으로서, 더욱상세하게는연료전지에있어서자동차의운전진행과같은가혹조건에따라환원극탄소담지체촉매가부식되는문제를개선하기위하여환원극탄소담지체촉매에함유된백금에이리듐을합금시킨합금촉매를제조하되특정공정과반응조건으로제조함으로인해탄소표면전하의안정화시간을단축할수 있고금속입자크기를제어하면서금속입자분포가균일하고내구성이우수한고품질의제품을제조할수 있는연료전지용합금촉매의제조방법에관한것이다.
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Patent Agency Ranking
公开(公告)号：KR1020120107397A
公开(公告)日：2012-10-02
申请号：KR1020110025067
申请日：2011-03-21
Applicant: 현대자동차주식회사 , 서울대학교산학협력단
CPC classification number: H01M4/8825 , H01M4/8807 , H01M4/8892 , H01M2008/1095 , Y02E60/50
Abstract: PURPOSE: A manufacturing method of an electrode for a fuel cell is provided to continuously maintain a catalyst layer and a porous structure for operation of a fuel cell, to be able to manufacture a pore structure with various sizes and distributions, and to facilitate control of the catalyst layer and the porous structure. CONSTITUTION: A manufacturing method of a Catalyst layer-combined electrode for a polymer electrolyte membrane fuel cell comprises: a step of providing plate-like porous metal foam(2,2a,2b) or a metal aerogel having a porous structure of nanometer or micron size; a step of manufacturing a catalyst layer-integrated electrode by fixing a catalyst to the metal foam or metal aerogel. The manufacturing method additionally comprises a step of impregnating an ion-conducting material into the catalyst layer-integrated electrode. [Reference numerals] (AA,EE) Gas; (BB,FF) Liquid; (CC) Large pores; (DD) Small pores; (GG,JJ) Electron; (HH, II) Ion
Abstract translation: 目的：提供一种用于燃料电池的电极的制造方法，以连续地维持燃料电池的催化剂层和多孔结构，以能够制造各种尺寸和分布的孔结构，并且有助于控制 催化剂层和多孔结构。 构成：用于聚合物电解质膜燃料电池的催化剂层组合电极的制造方法包括：提供板状多孔金属泡沫（2,2a，2b）或具有纳米或微米多孔结构的金属气凝胶的步骤 尺寸; 通过将催化剂固定到金属泡沫或金属气凝胶来制造催化剂层一体化电极的步骤。 该制造方法还包括将离子传导材料浸渍到催化剂层一体化电极中的步骤。 （标号）（AA，EE）气体; （BB，FF）液体; （CC）大孔; （DD）小孔; （GG，JJ）电子; （HH，II）离子
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公开(公告)号：KR1020040005119A
公开(公告)日：2004-01-16
申请号：KR1020020039419
申请日：2002-07-08
Applicant: 현대자동차주식회사
Inventor： 노범욱
IPC: H01M8/24
Abstract: PURPOSE: A fuel cell stack for an electric automobile is provided, to improve the assembling property and to prevent the loss of electric power by preventing the generated current from flowing along the cooling water. CONSTITUTION: The fuel cell stack comprises a plurality of subassemblies(10) comprising a pair of bipolar plates(11), a pair of gasket members(15) adhered to the inside of the bipolar plates, and an ion exchange member(17) adhered to the inside of the gasket members; a cooling jacket(20) inserted between the subassemblies; and a cooling channel(30) which is placed in the outer side of the subassemblies and supplies the cooling water(31) to the cooling jacket. Preferably the gasket is made of an ABS resin; and the cooling jacket is made of a metallic material.
Abstract translation: 目的：提供一种用于电动汽车的燃料电池堆，以通过防止所产生的电流沿冷却水流动来提高组装性能并防止电力的损失。 构成：燃料电池堆包括多个子组件（10），其包括一对双极板（11），一对密封件（15），粘合到双极板的内部，并且离子交换构件（17）被粘附 到垫圈构件的内部; 插入在所述子组件之间的冷却套（20） 以及冷却通道（30），其被放置在所述子组件的外侧，并将所述冷却水（31）供应到所述冷却套。 优选地，垫圈由ABS树脂制成; 冷却套由金属材料制成。
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公开(公告)号：KR1020040005053A
公开(公告)日：2004-01-16
申请号：KR1020020039343
申请日：2002-07-08
Applicant: 현대자동차주식회사
Inventor： 노범욱
IPC: H01M8/04
Abstract: PURPOSE: An apparatus for simulating the humidification of a fuel cell is provided, to determine the temperature, the pressure and the flow amount of the humidifying water supplied to a fuel cell stack more precisely. CONSTITUTION: The apparatus(100) comprises a housing assembly(10) which has first and second entrance holes(11, 13) at the one side and first and second exit holes(15, 17) at the other side and the hollow inside, and which contains a heat wire member(35) to the length direction and a filtration membrane(19) separating the length direction into an upper part(12) and an under part(14); a flow amount control part(20) which is set on the first path(21) connected with the first entrance hole and control the flow amount of air or hydrogen(16) flown into the upper side of the housing assembly; a humidifying water supply part(30) which is set through the second path connected with the second entrance hole, is provided with a body containing the humidifying water, a heat wire member for heating the humidifying water and a humidifying water display part for displaying the amount of the humidifying water in the body, and supplies the humidifying water(18) to the lower part of the housing assembly; and a pressure gauge(34) which is set on the third path(32) connected with the fuel cell stack by connected to the first exit hole.
Abstract translation: 目的：提供一种用于模拟燃料电池加湿的装置，以更精确地确定供应到燃料电池堆的加湿水的温度，压力和流量。 构成：装置（100）包括壳体组件（10），其在一侧具有第一和第二入口孔（11,13），在另一侧具有第一和第二出口孔（15,17）和中空内部， 并且包括长度方向的热丝构件（35）和将长度方向分隔成上部（12）和下部（14）的过滤膜（19）。 设置在与第一入口孔连接的第一路径（21）上并控制流入壳体组件的上侧的空气或氢气（16）的流量的流量控制部分（20） 通过与第二入口孔连接的第二路径设置的加湿水供给部件（30）设置有容纳加湿水的主体，用于加热加湿水的热丝构件和用于显示加湿水的加湿水显示部 并且将加湿水（18）供给到壳体组件的下部; 以及设置在通过连接到第一出口孔与燃料电池堆连接的第三路径（32）上的压力计（34）。
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公开(公告)号：KR101836721B1
公开(公告)日：2018-03-09
申请号：KR1020160133714
申请日：2016-10-14
IPC: H01M4/88
CPC classification number: H01M4/8875 , H01M4/8882 , Y02E60/50 , Y02P70/56
Abstract: 본발명에의한연료전지용전극제조방법은, 백금-탄소계촉매, 이온전도성고분자바인더, 상기이온전도성고분자바인더보다융점이낮고점도가높은보조바인더를포함하는혼합용액을제조하는제1단계, 상기혼합용액을방사하여나노섬유를제조하고, 이나노섬유를전극형상으로제조하는제2단계및 상기나노섬유를건조환경에서상기이온전도성고분자바인더의융점보다낮은온도로가열하여, 상기나노섬유의표면에서상기보조바인더를제거하여상기백금-탄소계촉매의노출면적을증가시키는제3단계를포함한다.
Abstract translation: 根据本发明，基于铂 - 碳催化剂，离子导电聚合物粘合剂，其包括燃料电池用电极的制造方法，包括：离子导电性低的熔点比该聚合物粘结剂中的第一步骤，制备含有次级粘合剂的混合溶液的粘度高，在混合 通过纺丝生产纳米纤维的溶液，并加热该炉纤维用于第二级和制造电极的形状在干燥环境中在低于所述离子导电聚合物粘合剂的熔点的温度下，纳米纤维，纳米纤维的表面上 第三步除去辅助粘合剂以增加铂碳基催化剂的暴露面积。
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公开(公告)号：KR101500069B1
公开(公告)日：2015-03-06
申请号：KR1020130039835
申请日：2013-04-11
Applicant: 현대자동차주식회사 , 숭실대학교산학협력단
CPC classification number: H01M4/9075 , H01M4/925 , Y02E60/50
Abstract: 본 발명은 연료전지용 촉매전극을 위한 티타늄 서브옥사이드 지지체와 이의 저온 합성방법에 관한 것으로서, 더욱 상세하게는 연료전지의 촉매전극의 지지체로 유용한 티타늄 서브옥사이드(Ti
x O
2x-1 ) 나노입자와, TiO
2 , Co 촉매 및 수소가스를 이용하여 600∼900℃의 낮은 온도에서 상기 티타늄 서브옥사이드(Ti
x O
2x-1 ) 나노입자를 합성하는 방법에 관한 것이다.
상기 티타늄 서브옥사이드 나노입자는 산에 대한 부식저항성이 뛰어나고 열적, 전기적인 전기전도도가 크고, 내구성이 뛰어난 장점을 가지고 있으므로, 이를 지지체로 사용하여 제조된 촉매전극은 연료전지 테스트를 통해 높은 촉매활성과 산화환원 특성이 향상된 효과를 나타낸다.
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