公开(公告)号：AT293118T

公开(公告)日：2005-04-15

申请号：AT02754733

申请日：2002-06-21

Applicant: BASF AG

Inventor： WULFF CHRISTIAN ,  ORSTEN STEFAN ,  OFTRING ALFRED ,  ZEHNER PETER

IPC: C07F9/38 ,  C07F9/40

Abstract: The invention relates to a process for preparing N-phosphono-methylglycine by reacting a hexahydrotriazine compound with a triacyl phosphite in an organic solvent, hydrolyzing the resulting phosphono compound after prior extraction into an aqueous phase and separation from the organic phase. The process avoids decomposition of the organic solvent during hydrolysis.

公开(公告)号：NZ530026A

公开(公告)日：2004-07-30

申请号：NZ53002602

申请日：2002-06-21

Applicant: BASF AG

Inventor： WULFF CHRISTIAN ,  ORSTEN STEFAN ,  OFTRING ALFRED ,  ZEHNER PETER

IPC: C07F9/38 ,  C07F9/40

Abstract: A method is disclosed for producing N-phosphonomethylglycine by reacting a hexahydrotriazine compound with a triacyl phosphite in an organic solvent and the saponification of the phosphono compound that is obtained after previous extraction into an aqueous phase, and separation of the organic phase. This method prevents decomposition of the organic solvent during saponification.

公开(公告)号：AU2003290055A1

公开(公告)日：2004-07-14

申请号：AU2003290055

申请日：2003-12-16

Applicant: BASF AG

Inventor： OFTRING ALFRED ,  BRAUN GEROLD

IPC: C07C253/10 ,  C07C255/46

Abstract: The present invention relates to a process for preparing 3-cyano-3,5,5-trimethylcyclohexanone (isophoronenitrile) by reacting isophorone with hydrogen cyanide in the presence of a base as a catalyst to obtain a crude isophoronenitrile product, and subsequently distilling the crude isophoronenitrile product, with the addition before distillation of at least one specific sulfonic acid or specific carboxylic acid. In addition, the present invention relates to the use of a specific sulfonic acid or of a specific carboxylic acid as a neutralizing agent before distillation of a crude isophoronenitrile product which has been obtained by reacting isophorone with hydrogen cyanide in the presence of a base as a catalyst, in order to avoid precipitates in the neutralization of the base used as a catalyst with an acid.

公开(公告)号：DE10259708A1

公开(公告)日：2004-07-08

申请号：DE10259708

申请日：2002-12-19

Applicant: BASF AG

Inventor： OFTRING ALFRED ,  BRAUN GEROLD

IPC: C07C253/10 ,  C07C255/46 ,  C07C253/34

Abstract: The present invention relates to a process for preparing 3-cyano-3,5,5-trimethylcyclohexanone (isophoronenitrile) by reacting isophorone with hydrogen cyanide in the presence of a base as a catalyst to obtain a crude isophoronenitrile product, and subsequently distilling the crude isophoronenitrile product, with the addition before distillation of at least one specific sulfonic acid or specific carboxylic acid. In addition, the present invention relates to the use of a specific sulfonic acid or of a specific carboxylic acid as a neutralizing agent before distillation of a crude isophoronenitrile product which has been obtained by reacting isophorone with hydrogen cyanide in the presence of a base as a catalyst, in order to avoid precipitates in the neutralization of the base used as a catalyst with an acid.

公开(公告)号：DE10130135A1

公开(公告)日：2003-01-02

申请号：DE10130135

申请日：2001-06-22

Applicant: BASF AG

Inventor： WULFF CHRISTIAN ,  ORSTEN STEFAN ,  OFTRING ALFRED ,  ZEHNER PETER

IPC: C07F9/38 ,  C07F9/40

Abstract: The invention relates to a method for producing N-phosphonomethylglycine by reacting a hexahydrotriazine compound with a triacyle phosphate in an organic solvent and the saponification of the phosphono compound which is obtained after previous extraction into an aqueous phase, and separation of the organic phase. According to the invention, said method prevents decomposition of the organic solvent during saponification.

公开(公告)号：DE59605363D1

公开(公告)日：2000-07-06

申请号：DE59605363

申请日：1996-07-02

Applicant: BASF AG

Inventor： OFTRING ALFRED ,  AUS DEM KAHMEN MARTIN

IPC: C07C231/02 ,  C07C233/47 ,  C07C233/49 ,  C07C303/22 ,  C07C303/32 ,  C07C309/15 ,  C09K23/00

Abstract: PCT No. PCT/EP96/02888 Sec. 371 Date Jan. 13, 1998 Sec. 102(e) Date Jan. 13, 1998 PCT Filed Jul. 2, 1996 PCT Pub. No. WO97/03043 PCT Pub. Date Jan. 30, 1997The process for preparing an N-acylaminocarboxylic or N-acylaminosulfonic acid or an alkali metal salt thereof from an alkali metal aminocarboxylate or aminosulfonate and a carboxylic glyceride comprises (a) preparing a suspension of the solid anhydrous alkali metal aminocarboxylate or aminosulfonate in the carboxylic glyceride, (b) adding a strong base to the suspension to form an alkali metal N-acylaminocarboxylate or N-acylaminosulfonate, and (c) if desired, preparing the free N-acylaminocarboxylic or N-acylaminosulfonic acid therefrom in a conventional manner by adding an acid.

公开(公告)号：DE59506116D1

公开(公告)日：1999-07-08

申请号：DE59506116

申请日：1995-09-12

Applicant: BASF AG

Inventor： STRECKER BEATE ,  OFTRING ALFRED ,  HERTEL DIETER ,  SCHUH GEORG

IPC: C07B61/00 ,  C07C231/02 ,  C07C233/47 ,  C07C303/22 ,  C07C303/32 ,  C07C309/15

Abstract: PCT No. PCT/EP95/03584 Sec. 371 Date Mar. 24, 1997 Sec. 102(e) Date Mar. 24, 1997 PCT Filed Sep. 12, 1995 PCT Pub. No. WO96/09278 PCT Pub. Date Mar. 28, 1996N-acylamino carboxylic acids and N-acylamino sulfonic acids and their alkali metal salts from the technical alkali metal salts of amino carboxylic acids and amino sulfonic acids, respectively, with an active content of 50-95% by weight, based on the solids content of the technical alkali metal salts, and from alkyl carboxylates, are prepared by (a) preparing a suspension of the solid anhydrous technical alkali metal salts of the amino carboxylic acids or amino sulfonic acids in the alkyl carboxylates, (b) reacting this suspension by adding more than 30 to 150 mol % of strong bases to give the alkali metal salts of the N-acylamino carboxylic acids or N-acylamino sulfonic acids, and (c) if required preparing therefrom the free N-acylamino carboxylic acids or N-acylamino sulfonic acids in a conventional way by adding acids.

公开(公告)号：DE59405808D1

公开(公告)日：1998-05-28

申请号：DE59405808

申请日：1994-10-12

Applicant: BASF AG

Inventor： STRECKER BEATE ,  OETTER GUENTER ,  OFTRING ALFRED ,  PERNER JOHANNES ,  BAUR RICHARD ,  SCHWENDEMANN VOLKER ,  AUS DEM KAHMEN MARTIN ,  REIF WOLFGANG

IPC: C11D1/72 ,  A01N25/30 ,  A61K47/18 ,  C07C231/02 ,  C07C233/18 ,  C07C233/20 ,  C09D17/00 ,  C09K8/035 ,  C09K8/28 ,  C09K23/00 ,  C09K23/42 ,  C11D1/52 ,  C23G5/00

Abstract: PCT No. PCT/EP94/03354 Sec. 371 Date Apr. 22, 1996 Sec. 102(e) Date Apr. 22, 1996 PCT Filed Oct. 12, 1994 PCT Pub. No. WO95/11225 PCT Pub. Date Apr. 27, 1995The use of endgroup-capped fatty amide alkoxylates IR1-CO-NH-(CH2)n-O-(AO)x-R2(I)where R1 is C5-C21-alkyl or -alkenyl, R2 is C1-C4-alkyl, A is C2-C4-alkylene, n is 2 or 3, and x has a value from 1 to 6, as nonionic surfactants or emulsifiers in detergents, cleaners or body care compositions, as surface-active substances for industrial applications in electroplating, in the photographic industry, in petroleum production, in the pharmaceutical industry, in plant feeding and in crop protection formulations, and as surface-active substances in the production of emulsions and pigment and plastic dispersions.

公开(公告)号：DE59404645D1

公开(公告)日：1998-01-02

申请号：DE59404645

申请日：1994-08-16

Applicant: BASF AG

Inventor： SCHNEIDER JUERGEN ,  OFTRING ALFRED ,  FREYBERG PETER ,  SCHUMACHER RUDOLF ,  BAUR RICHARD ,  POTTHOFF-KARL BIRGIT ,  KUD ALEXANDER

IPC: C11D3/12 ,  C05D9/02 ,  C05F11/00 ,  C09K3/00 ,  C11D1/10 ,  C11D3/33 ,  C11D3/34 ,  C11D7/32 ,  C11D7/34 ,  D21C9/10 ,  G03C5/305 ,  G03C7/42

公开(公告)号：DE59305905D1

公开(公告)日：1997-04-24

申请号：DE59305905

申请日：1993-10-15

Applicant: BASF AG

Inventor： STRECKER BEATE ,  WOLF HELMUT ,  WOLF GERHARD ,  OFTRING ALFRED ,  BECHTOLSHEIMER HANS-HEINRICH ,  HERTEL DIETER

IPC: C07C231/02 ,  C07C233/18