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公开(公告)号:JP2004107270A
公开(公告)日:2004-04-08
申请号:JP2002272840
申请日:2002-09-19
Inventor: TSUYUTANI SHINJI , SHIBATA KENGO
Abstract: PROBLEM TO BE SOLVED: To provide a method for easily producing an aqueous solution of a phosphoric acid ester salt reduced in odor and discoloration.
SOLUTION: The method for producing the aqueous solution of the phosphoric acid ester salt comprises bringing the original aqueous solution of the phosphoric acid ester salt into contact with an adsorbent.
COPYRIGHT: (C)2004,JPO-
公开(公告)号:JP2003126675A
公开(公告)日:2003-05-07
申请号:JP2001330775
申请日:2001-10-29
Applicant: KAO CORP
Inventor: KIDA KIYOBUMI , SAITO TAKASHI , TANAHASHI SHINICHIRO , SHIBATA KENGO , SHIBATA KEIJI
Abstract: PROBLEM TO BE SOLVED: To provide a fluid distribution apparatus capable of simultaneously distributing fluid such as liquid or powder to any ratio. SOLUTION: The fluid distribution apparatus is composed of a dispersing part 2 that sprinkles a supplied fluid from the center to the approximately circumferential direction radially and uniformly and a dispersing part 3 that is provided with an inner mouth of such size that the dispersing part can be inserted and the first recovering tube having a top flange extending slantly to the axis direction. The fluid is recovered by a first recovering tube 4 that encloses the surrounding of the dispersing part 3 along the approximately circumferential direction at any angle range and a second recovering tube 5 that recovers the fluid which is not recovered by the first recovering tube 4. The recovering tube 4 of which the top flange is constituted slantly moves up and down, so that the angle range enclosing the surrounding of the dispersing part 3 can be altered and the amount of the fluid recovered by both of the recovering tubes 4, 5 can be varied to any extent.
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公开(公告)号:JP2003096088A
公开(公告)日:2003-04-03
申请号:JP2001291848
申请日:2001-09-25
Applicant: KAO CORP
Inventor: SHIBATA KENGO , SAKATA MASARU
Abstract: PROBLEM TO BE SOLVED: To provide a production method of a phosphoric acid ester, which efficiently removes odorous component, produces the phosphoric acid ester with excellent compounding stability in a good yield, and hardly corrodes the device used for the production. SOLUTION: The production method includes: (1) a phosphorylation process to obtain the phosphoric acid ester by reacting an organic hydroxy compound with a phosphorylating agent, (2) a hydrolysis process to hydrolyze a pyrophosphoric acid compound in the phosphoric acid ester obtained in the process (1), (3) a dewatering process to obtain the dewatered phosphoric acid ester by dewatering the hydrolysate of the phosphoric acid ester obtained in the process (2) to at most 3 wt.% in water content, and (4) a deodorization process to obtain the deodorized phosphoric acid ester by removing an odorous component from the dewatered phosphoric acid ester obtained in the process (3).
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公开(公告)号:JP2002363191A
公开(公告)日:2002-12-18
申请号:JP2001165056
申请日:2001-05-31
Applicant: KAO CORP
Inventor: SHIBATA KENGO , MORISHITA MITSUGI
Abstract: PROBLEM TO BE SOLVED: To provide a method for producing a phosphoric acid ester, capable of efficiently and easily reducing an amount of a smelling component of the ester. SOLUTION: This method for producing the phosphoric acid ester comprises (A) making the phosphoric acid ester contact with an inert gas, after heating the phosphoric acid ester, so as to reduce the amount of the smelling component contained in the phosphoric acid ester, and (B) cooling the phosphoric acid ester of which the amount of the smelling component is reduced by the process (A), and further repeating the processes (A) and (B).
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公开(公告)号:JP2001180998A
公开(公告)日:2001-07-03
申请号:JP36110899
申请日:1999-12-20
Applicant: KAO CORP
Inventor: SATO HARUYUKI , IZUMI TATSUO , MINOU SEIYA , SHIMOKAWA YOSHIFUMI , KOYANAGI KOJI , UKIANA TOSHINAO , SHIBATA KENGO
IPC: C04B24/26 , C04B24/32 , C04B28/02 , C04B103/32 , C08F216/12 , C08F220/04 , C08F220/28 , C08F222/02 , C08F222/04 , C08F222/20 , C08F290/06
Abstract: PROBLEM TO BE SOLVED: To provide the concrete admixture which is useful for a high strength concrete and has high fluidity and excellent applicability. SOLUTION: The admixture contains a mixture of copolymers comprising a specific monomer (A) such as ethylenically unsaturated carboxylic acid derivatives with polyoxyalkylene groups, and specific monomer (B) such as (meth)acrylic acid. The molar ratio (A)/(B) is changed at least once during the polymerization process. The concrete containing the admixture is also provided.
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公开(公告)号:JP2000143701A
公开(公告)日:2000-05-26
申请号:JP32012798
申请日:1998-11-11
Applicant: KAO CORP
Inventor: SHIBATA KENGO , SAKATA MASARU , TSUYUTANI SHINJI , UEYAMA NORIO , IWASAKI TOSHIYA
Abstract: PROBLEM TO BE SOLVED: To produce a low viscous aqueous solution of polysaccharide derivative having excellent handleability, especially an operability in an operation of a membrane separation. SOLUTION: This low viscous aqueous solution of polysaccharide derivative is produced by blending 100 pts.wt. of polysaccharide derivative in which a part or all of hydrogen atoms of hydroxyl groups in a molecule are substituted with a hydrophobic substituting group and ionic hydrophilic substituting group and having >=1,000 mPa.s of 1 wt.% of an aqueous solution at 25 deg.C with 10-1,000 pts.wt. of (meth)acrylic acid-based polymer.
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公开(公告)号:JPH11228636A
公开(公告)日:1999-08-24
申请号:JP2692198
申请日:1998-02-09
Applicant: KAO CORP
Inventor: SHIBATA KENGO , MINOU SEIYA , SATO HARUYUKI , HAMADA DAISUKE , KONO YOSHINAO
IPC: C08F220/06 , C08F20/28 , C08F220/28
Abstract: PROBLEM TO BE SOLVED: To produce a (meth)acrylic acid-based polymer suitable as a cement dispersant having a stable quality. SOLUTION: This method for producing a (meth)acrylic acid-based polymer provided with a process 1 for subjecting (meth)acrylic acid and a polyalkyleneglycol monoalkyl ether to an esterification reaction in a molar ratio of 5:1 to 50:1 in the presence of an acid catalyst and a polymerization inhibitor, deactivating the acid catalyst with an alkali agent, and subsequently distilling away the unreacted (meth)acrylic acid to obtain the esterification reaction product containing the (meth)acrylate ester and the unreacted (meth) acrylic acid residue, and with a process 2 for adjusting the esterification product obtained in the process 1 to a pH of 1.5-3.5 and subsequently copolymerizing the (meth)acrylate ester with the unreacted (meth)acrylic acid residue.
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公开(公告)号:JP2003160590A
公开(公告)日:2003-06-03
申请号:JP2001355203
申请日:2001-11-20
Applicant: KAO CORP
Inventor: TSUYUTANI SHINJI , SHIBATA KENGO
IPC: C07F9/11
Abstract: PROBLEM TO BE SOLVED: To provide a manufacture method of a phosphate whose odor is easily and rapidly reduced. SOLUTION: In the manufacture method of the phosphate of an organic hydroxy compound, water is added to the phosphate of the organic hydroxy compound, and water is distilled in vacuo. COPYRIGHT: (C)2003,JPO
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公开(公告)号:JP2003130696A
公开(公告)日:2003-05-08
申请号:JP2001324865
申请日:2001-10-23
Applicant: KAO CORP
Inventor: KIDA KIYOBUMI , SAITO TAKASHI , TANAHASHI SHINICHIRO , SHIBATA KENGO , SHIBATA KEIJI
IPC: G01F1/28
Abstract: PROBLEM TO BE SOLVED: To provide a flowmeter capable of being installed inside a conduit line, which can measure the flow rate of fluid that does not fill the conduit line. SOLUTION: The flow meter which measures the flow rate of the fluid flowing inside conduct lines 5, 6, is provided with a measurement casing 2 which is built in the inside of the system of the conduct lines 5, 6, a displacement means 3 with a body to be detected 16 which is arranged inside the measurement casing 2 and changes its position under the dynamic pressure of the fluid, a biasing means 20 which forces the displacement means toward the initial position, and a noncontacting-type displacement sensor 17 which is mounted on outside surface of the measuring casing 2. The displacement means 3 receives the dynamic pressure corresponding to the flow rate of the fluid and changes its position based on the displacement value corresponding to the dynamic pressure of the fluid against the force of the biasing means 20, and the displacement sensor 17 detects the displacement value of the body to be detected 16 and measures the flow rate.
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公开(公告)号:JP2002363190A
公开(公告)日:2002-12-18
申请号:JP2001165040
申请日:2001-05-31
Applicant: KAO CORP
Inventor: SHIBATA KENGO , AIZAWA KAZUNORI , MORISHITA MITSUGI
Abstract: PROBLEM TO BE SOLVED: To provide a method for producing a phosphoric acid ester, capable of easily and rapidly reducing an amount of a smelling component of the ester and capable of giving a good color to the ester. SOLUTION: This method for producing the phosphoric acid ester comprises making the phosphoric acid ester of 100-160 deg.C contact with an inert gas in a packed tower, so that the amount of the smelling component is reduced.
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